{"id":68667,"date":"2026-04-27T10:58:08","date_gmt":"2026-04-27T02:58:08","guid":{"rendered":"http:\/\/111.62.156.167\/?chemical-product=n-acetyl-d-ul-13c6glucosamine"},"modified":"2026-04-27T10:58:08","modified_gmt":"2026-04-27T02:58:08","slug":"n-acetyl-d-ul-13c6glucosamine","status":"publish","type":"chemical-product","link":"https:\/\/bio-get.com\/?chemical-product=n-acetyl-d-ul-13c6glucosamine","title":{"rendered":"N-Acetyl-D-[UL-13C6]glucosamine"},"content":{"rendered":"

\u4ea7\u54c1\u8bf4\u660e
\nN-\u4e59\u9170\u57fa-D-[UL-13C6]\u8461\u8404\u7cd6\u80fa\u4ea7\u54c1\u8bf4\u660e\u4e66
\n1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u54c1\u4e3a\u7a33\u5b9a\u540c\u4f4d\u7d20\u6807\u8bb0\u7684N-\u4e59\u9170\u8461\u8404\u7cd6\u80fa\u884d\u751f\u7269\uff0c\u5316\u5b66\u540d\u79f0N-Acetyl-D-[UL-13C6]glucosamine\uff0cCAS\u53f7127959-06-2\u3002\u5206\u5b50\u5f0f\u4e3a\u00b9\u00b3C6C2H15NO6\uff0c\u5206\u5b50\u91cf227.21 g\/mol\uff0c\u7eaf\u5ea6\u7ecfHPLC\u9a8c\u8bc1>96%\u3002\u4ea7\u54c1\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u7c89\u672b\uff0c\u6613\u6eb6\u4e8e\u6c34\u53ca\u6781\u6027\u6709\u673a\u6eb6\u5242\u3002\u7ed3\u6784\u4e2d\u7684\u516d\u4e2a\u78b3\u539f\u5b50\u5747\u88ab13C\u540c\u4f4d\u7d20\u6807\u8bb0\uff08UL-13C6\uff09\uff0c\u6807\u8bb0\u7387\u226599%\uff0c\u662f\u7cd6\u4ee3\u8c22\u7814\u7a76\u548c\u793a\u8e2a\u5b9e\u9a8c\u7684\u9ad8\u7eaf\u5ea6\u6807\u51c6\u54c1\u3002
\n2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u6c28\u57fa\u7cd6\u7c7b\u5173\u952e\u4ee3\u8c22\u4e2d\u95f4\u4f53\uff0c\u672c\u54c1\u662f\u900f\u660e\u8d28\u9178\u3001\u51e0\u4e01\u8d28\u7b49\u591a\u7cd6\u751f\u7269\u5408\u6210\u7684\u76f4\u63a5\u524d\u4f53\u7269\u8d28\u300213C\u6807\u8bb0\u7279\u6027\u4f7f\u5176\u6210\u4e3a\u7cd6\u80fa\u805a\u7cd6\u4ee3\u8c22\u901a\u8def\u7814\u7a76\u7684\u7406\u60f3\u793a\u8e2a\u5242\uff0c\u53ef\u901a\u8fc7\u8d28\u8c31\u6216NMR\u6280\u672f\u7cbe\u51c6\u8ffd\u8e2a\u7ec6\u80de\u5185\u7cd6\u57fa\u5316\u4fee\u9970\u3001\u86cb\u767d\u8d28O-GlcNAc\u5316\u7b49\u8fc7\u7a0b\uff0c\u4e3a\u7cd6\u751f\u7269\u5b66\u3001\u80bf\u7624\u4ee3\u8c22\u91cd\u7f16\u7a0b\u7b49\u7814\u7a76\u63d0\u4f9b\u5206\u5b50\u5de5\u5177\u3002
\n3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\uff081\uff09\u4ee3\u8c22\u7ec4\u5b66\u7814\u7a76\uff1a\u7528\u4e8e\u5b9a\u91cf\u5206\u6790\u7cd6\u9175\u89e3-HBP\u901a\u8def\u901a\u91cf
\n\uff082\uff09\u836f\u7269\u5f00\u53d1\uff1a\u4f5c\u4e3a\u7cd6\u57fa\u5316\u6291\u5236\u5242\u7b5b\u9009\u7684\u53c2\u7167\u5316\u5408\u7269
\n\uff083\uff09\u75be\u75c5\u673a\u5236\u7814\u7a76\uff1a\u793a\u8e2a\u7cd6\u5c3f\u75c5\u3001\u764c\u75c7\u7b49\u75be\u75c5\u4e2d\u7684\u5f02\u5e38\u7cd6\u4ee3\u8c22
\n\uff084\uff09\u8d28\u8c31\u5185\u6807\uff1a\u4f5c\u4e3aLC-MS\/MS\u6cd5\u5b9a\u91cf\u68c0\u6d4b\u7ec4\u7ec7\/\u4f53\u6db2\u4e2dN-\u4e59\u9170\u8461\u8404\u7cd6\u80fa\u7684\u6821\u6b63\u6807\u51c6
\n4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u957f\u671f\u50a8\u5b58\u9700\u7f6e\u4e8e-20\u2103\u5e72\u71e5\u907f\u5149\u73af\u5883\uff0c\u5f00\u5c01\u540e\u5efa\u8bae\u5206\u88c5\u4fdd\u5b58\u3002\u5de5\u4f5c\u6db2\u9700\u73b0\u914d\u73b0\u7528\uff0c\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002\u4f7f\u7528\u65f6\u9700\u5728\u751f\u7269\u5b89\u5168\u67dc\u4e2d\u64cd\u4f5c\uff0c\u5efa\u8bae\u6d53\u5ea6\u8303\u56f40.1-10 mM\uff08\u6839\u636e\u5b9e\u9a8c\u4f53\u7cfb\u4f18\u5316\uff09\u3002\u4e0e\u5f3a\u6c27\u5316\u5242\u4e0d\u76f8\u5bb9\uff0c\u6eb6\u89e3\u63a8\u8350\u4f7f\u7528PBS\u7f13\u51b2\u6db2\uff08pH 7.4\uff09\u6216\u65e0\u83cc\u6c34\u3002
\n5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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