\u4ea7\u54c1\u8bf4\u660e <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n2-([1,1′-\u8054\u82ef]-4-\u57fa)-2,2-\u4e8c\u6c1f\u4e59\u70f7-1-\u9187\uff08CAS\u53f7\uff1a1889025-63-1\uff09\u662f\u4e00\u79cd\u6709\u673a\u6c1f\u5316\u5408\u7269\uff0c\u5206\u5b50\u5f0f\u4e3aC14H12F2O\uff0c\u5206\u5b50\u91cf\u4e3a234.241\u3002\u8be5\u5316\u5408\u7269\u4ee5\u8054\u82ef\u7ed3\u6784\u4e3a\u6838\u5fc3\uff0c\u5e76\u5728\u4e59\u70f7\u94fe\u4e0a\u5f15\u5165\u4e8c\u6c1f\u53d6\u4ee3\u57fa\u548c\u7f9f\u57fa\uff0c\u4f7f\u5176\u517c\u5177\u82b3\u9999\u6027\u548c\u6781\u6027\u5b98\u80fd\u56e2\u7279\u6027\u3002\u5176\u7eaf\u5ea6\u9ad8\u4e8e96%\uff0c\u5916\u89c2\u901a\u5e38\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u56fa\u4f53\u6216\u7c89\u672b\uff0c\u53ef\u6eb6\u4e8e\u5e38\u89c1\u6709\u673a\u6eb6\u5242\u5982\u7532\u9187\u3001\u4e59\u9187\u548c\u4e8c\u7532\u57fa\u4e9a\u781c\uff08DMSO\uff09\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u56e0\u5176\u72ec\u7279\u7684\u4e8c\u6c1f\u4e59\u57fa\u7ed3\u6784\uff0c\u5728\u751f\u7269\u5316\u5b66\u7814\u7a76\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002\u4e8c\u6c1f\u53d6\u4ee3\u57fa\u53ef\u663e\u8457\u6539\u53d8\u5206\u5b50\u7684\u7535\u5b50\u5206\u5e03\u548c\u4ee3\u8c22\u7a33\u5b9a\u6027\uff0c\u4f7f\u5176\u6210\u4e3a\u836f\u7269\u5316\u5b66\u4e2d\u5e38\u89c1\u7684\u836f\u6548\u56e2\u4fee\u9970\u7b56\u7565\u3002\u7f9f\u57fa\u7684\u5b58\u5728\u8fdb\u4e00\u6b65\u589e\u5f3a\u4e86\u5176\u53c2\u4e0e\u6c22\u952e\u5f62\u6210\u7684\u80fd\u529b\uff0c\u9002\u7528\u4e8e\u4f5c\u4e3a\u4e2d\u95f4\u4f53\u6216\u914d\u4f53\u7528\u4e8e\u9176\u6291\u5236\u7814\u7a76\u3001\u53d7\u4f53\u7ed3\u5408\u5b9e\u9a8c\u7b49\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n2-([1,1′-\u8054\u82ef]-4-\u57fa)-2,2-\u4e8c\u6c1f\u4e59\u70f7-1-\u9187\u5e7f\u6cdb\u5e94\u7528\u4e8e\u533b\u836f\u7814\u53d1\u548c\u6750\u6599\u79d1\u5b66\u9886\u57df\u3002\u5728\u836f\u7269\u5316\u5b66\u4e2d\uff0c\u5b83\u53ef\u4f5c\u4e3a\u5173\u952e\u4e2d\u95f4\u4f53\u7528\u4e8e\u5408\u6210\u6297\u80bf\u7624\u3001\u6297\u708e\u6216\u4e2d\u67a2\u795e\u7ecf\u7cfb\u7edf\u836f\u7269\u3002\u6b64\u5916\uff0c\u5176\u8054\u82ef\u7ed3\u6784\u4e5f\u4f7f\u5176\u6210\u4e3a\u6db2\u6676\u6750\u6599\u6216\u6709\u673a\u5149\u7535\u6750\u6599\u7684\u6f5c\u5728\u6784\u5efa\u5355\u5143\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\u4f46\u4e0d\u9650\u4e8e\uff1a
\n– \u4f5c\u4e3a\u6c1f\u5316\u4fee\u9970\u7684\u5206\u5b50\u63a2\u9488
\n– \u7528\u4e8e\u9ad8\u901a\u91cf\u7b5b\u9009\u4e2d\u7684\u6d3b\u6027\u5316\u5408\u7269\u5e93\u6784\u5efa
\n– \u6709\u673a\u5408\u6210\u4e2d\u7684\u624b\u6027\u62c6\u5206\u6216\u50ac\u5316\u53cd\u5e94\u5e95\u7269 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u4e3a\u786e\u4fdd\u4ea7\u54c1\u7a33\u5b9a\u6027\uff0c\u5efa\u8bae\u5728-20\u00b0C\u4e0b\u907f\u5149\u4fdd\u5b58\uff0c\u957f\u671f\u50a8\u5b58\u9700\u7f6e\u4e8e\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u73af\u5883\u4e2d\u3002\u5f00\u5c01\u540e\u5e94\u907f\u514d\u53cd\u590d\u51bb\u878d\uff0c\u5e76\u4e25\u683c\u9632\u6f6e\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u73af\u5883\u4e0b\u64cd\u4f5c\uff0c\u4f69\u6234\u9632\u62a4\u624b\u5957\u548c\u62a4\u76ee\u955c\u3002\u6eb6\u89e3\u5efa\u8bae\u91c7\u7528\u65e0\u6c34\u6eb6\u5242\uff0c\u5e76\u5728\u4f7f\u7528\u524d\u901a\u8fc7\u6838\u78c1\u5171\u632f\uff08NMR\uff09\u6216\u9ad8\u6548\u6db2\u76f8\u8272\u8c31\uff08HPLC\uff09\u9a8c\u8bc1\u7eaf\u5ea6\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u901a\u8fc7HPLC\u548c\u8d28\u8c31\uff08MS\uff09\u53cc\u91cd\u68c0\u6d4b\uff0c\u786e\u4fdd\u7eaf\u5ea6>96%\u3002\u6f5c\u5728\u98ce\u9669\u5305\u62ec\u5bf9\u76ae\u80a4\u3001\u773c\u775b\u548c\u547c\u5438\u9053\u7684\u8f7b\u5fae\u523a\u6fc0\u6027\uff0c\u64cd\u4f5c\u65f6\u5e94\u9075\u5b88\u5b9e\u9a8c\u5ba4\u5b89\u5168\u89c4\u8303\u3002\u5b89\u5168\u6570\u636e\u8868\uff08SDS\uff09\u4e2d\u5df2\u6807\u660e\u5176\u6025\u6027\u6bd2\u6027\uff08\u5982LD50\uff09\u548c\u751f\u6001\u6bd2\u6027\u4fe1\u606f\uff0c\u5e9f\u5f03\u5904\u7406\u9700\u7b26\u5408\u5f53\u5730\u6cd5\u89c4\u3002 <\/p>\n
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