1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u53cc\u73af[4.1.0]\u5e9a\u57fa-7-\u6c28\u57fa\u7532\u9178\u53d4\u4e01\u916f\uff08tert-butyl bicyclo[4.1.0]heptan-7-ylcarbamate\uff09\u662f\u4e00\u79cd\u6709\u673a\u5316\u5408\u7269\uff0cCAS\u53f7\u4e3a1870325-81-7\uff0c\u5206\u5b50\u5f0f\u4e3aC12H21NO2\uff0c\u5206\u5b50\u91cf\u4e3a211.3\u3002\u8be5\u5316\u5408\u7269\u4ee5\u53cc\u73af\u5e9a\u70f7\u4e3a\u6838\u5fc3\u7ed3\u6784\uff0c\u901a\u8fc7\u53d4\u4e01\u6c27\u7fb0\u57fa\uff08Boc\uff09\u4fdd\u62a4\u6c28\u57fa\uff0c\u5177\u6709\u8f83\u9ad8\u7684\u5316\u5b66\u7a33\u5b9a\u6027\u548c\u53cd\u5e94\u9009\u62e9\u6027\u3002\u5176\u7eaf\u5ea6\u5927\u4e8e96%\uff0c\u9002\u5408\u4f5c\u4e3a\u4e2d\u95f4\u4f53\u7528\u4e8e\u6709\u673a\u5408\u6210\u4e0e\u836f\u7269\u7814\u53d1\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u5728\u751f\u7269\u5316\u5b66\u9886\u57df\u4e3b\u8981\u7528\u4e8e\u6c28\u57fa\u4fdd\u62a4\u57fa\u56e2\u7684\u5f15\u5165\u4e0e\u8131\u4fdd\u62a4\u53cd\u5e94\u3002Boc\u57fa\u56e2\u5728\u9178\u6027\u6761\u4ef6\u4e0b\u53ef\u9009\u62e9\u6027\u8131\u9664\uff0c\u56e0\u6b64\u5728\u591a\u80bd\u5408\u6210\u3001\u86cb\u767d\u8d28\u4fee\u9970\u53ca\u5c0f\u5206\u5b50\u836f\u7269\u5f00\u53d1\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002\u5176\u53cc\u73af\u7ed3\u6784\u8fd8\u53ef\u80fd\u8d4b\u4e88\u5206\u5b50\u72ec\u7279\u7684\u7a7a\u95f4\u6784\u578b\uff0c\u4e3a\u836f\u7269\u8bbe\u8ba1\u63d0\u4f9b\u66f4\u591a\u53ef\u80fd\u6027\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u53cc\u73af[4.1.0]\u5e9a\u57fa-7-\u6c28\u57fa\u7532\u9178\u53d4\u4e01\u916f\u5e7f\u6cdb\u5e94\u7528\u4e8e\u533b\u836f\u7814\u53d1\u548c\u6709\u673a\u5408\u6210\u9886\u57df\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a\u4f5c\u4e3a\u5173\u952e\u4e2d\u95f4\u4f53\u7528\u4e8e\u6784\u5efa\u590d\u6742\u6742\u73af\u5316\u5408\u7269\uff1b\u5728\u6297\u764c\u3001\u6297\u75c5\u6bd2\u836f\u7269\u7814\u53d1\u4e2d\u4f5c\u4e3a\u9aa8\u67b6\u7ed3\u6784\uff1b\u5728\u6750\u6599\u79d1\u5b66\u4e2d\u7528\u4e8e\u529f\u80fd\u6027\u5206\u5b50\u7684\u4fee\u9970\u3002\u5176\u9ad8\u7eaf\u5ea6\u7279\u6027\u786e\u4fdd\u4e86\u5b9e\u9a8c\u7ed3\u679c\u7684\u53ef\u9760\u6027\u548c\u91cd\u590d\u6027\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5c06\u672c\u54c1\u7f6e\u4e8e\u5e72\u71e5\u3001\u907f\u5149\u7684\u73af\u5883\u4e2d\uff0c\u50a8\u5b58\u6e29\u5ea6\u8303\u56f4\u4e3a2-8\u2103\u3002\u5f00\u5c01\u540e\u9700\u5145\u5165\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u4fdd\u62a4\uff0c\u4ee5\u907f\u514d\u5438\u6e7f\u6216\u6c27\u5316\u3002\u4f7f\u7528\u65f6\u9700\u5728\u901a\u98ce\u6a71\u4e2d\u64cd\u4f5c\uff0c\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u76ae\u80a4\u6216\u773c\u775b\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u8868\u660e\uff0c\u8be5\u5316\u5408\u7269\u6613\u6eb6\u4e8e\u6709\u673a\u6eb6\u5242\uff08\u5982\u4e8c\u6c2f\u7532\u70f7\u3001\u56db\u6c22\u544b\u5583\uff09\uff0c\u4f46\u5728\u6c34\u4e2d\u6eb6\u89e3\u5ea6\u8f83\u4f4e\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u901a\u8fc7HPLC\u68c0\u6d4b\uff0c\u7eaf\u5ea6\u4e25\u683c\u63a7\u5236\u572896%\u4ee5\u4e0a\u3002\u5b89\u5168\u6570\u636e\u8868\u660e\uff0c\u8be5\u5316\u5408\u7269\u53ef\u80fd\u5bf9\u773c\u775b\u548c\u76ae\u80a4\u6709\u523a\u6fc0\u6027\uff0c\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u9632\u62a4\u624b\u5957\u548c\u62a4\u76ee\u955c\u3002\u82e5\u4e0d\u614e\u63a5\u89e6\uff0c\u5e94\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5e94\u6309\u7167\u5f53\u5730\u6cd5\u89c4\u5904\u7406\uff0c\u907f\u514d\u73af\u5883\u6c61\u67d3\u3002 <\/p>\n
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