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3-\u6c1f-4-((\u7532\u57fa\u78fa\u9170\u6c27\u57fa)\u7532\u57fa)\u54cc\u5576-1-\u7532\u9178\u53d4\u4e01\u916f\u4ea7\u54c1\u8bf4\u660e <\/p>\n

1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u54c1\u5316\u5b66\u540d\u79f0\u4e3atert-butyl 3-fluoro-4-((methylsulfonyloxy)methyl)piperidine-1-carboxylate\uff0c\u4e2d\u6587\u540d\u79f0\u4e3a3-\u6c1f-4-((\u7532\u57fa\u78fa\u9170\u6c27\u57fa)\u7532\u57fa)\u54cc\u5576-1-\u7532\u9178\u53d4\u4e01\u916f\uff0cCAS\u53f7\u4e3a1824168-69-5\uff0c\u5206\u5b50\u5f0f\u4e3aC12H22FNO5S\uff0c\u5206\u5b50\u91cf\u4e3a311.37\u3002\u8be5\u5316\u5408\u7269\u662f\u4e00\u79cd\u54cc\u5576\u884d\u751f\u7269\uff0c\u5177\u6709\u53d4\u4e01\u6c27\u7fb0\u57fa\uff08Boc\uff09\u4fdd\u62a4\u57fa\u548c\u7532\u57fa\u78fa\u9170\u6c27\u57fa\uff08MsO\uff09\u6d3b\u6027\u57fa\u56e2\uff0c\u7eaf\u5ea6\u9ad8\u4e8e96%\uff0c\u901a\u5e38\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u56fa\u4f53\u6216\u6cb9\u72b6\u7269\uff0c\u5177\u6709\u8f83\u9ad8\u7684\u5316\u5b66\u7a33\u5b9a\u6027\u3002 <\/p>\n

2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u54cc\u5576\u7c7b\u5316\u5408\u7269\u7684\u884d\u751f\u7269\uff0c\u8be5\u4ea7\u54c1\u5728\u6709\u673a\u5408\u6210\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002\u5176\u7ed3\u6784\u4e2d\u7684Boc\u4fdd\u62a4\u57fa\u53ef\u9009\u62e9\u6027\u8131\u9664\uff0c\u800c\u7532\u57fa\u78fa\u9170\u6c27\u57fa\u4f5c\u4e3a\u826f\u597d\u7684\u79bb\u53bb\u57fa\u56e2\uff0c\u6613\u4e8e\u53c2\u4e0e\u4eb2\u6838\u53d6\u4ee3\u53cd\u5e94\u3002\u6c1f\u539f\u5b50\u7684\u5f15\u5165\u53ef\u8c03\u8282\u5206\u5b50\u7684\u7535\u5b50\u6548\u5e94\u548c\u8102\u6eb6\u6027\uff0c\u4f7f\u5176\u5728\u836f\u7269\u5316\u5b66\u4e2d\u6210\u4e3a\u5173\u952e\u7684\u4e2d\u95f4\u4f53\uff0c\u5c24\u5176\u9002\u7528\u4e8e\u9776\u5411\u5206\u5b50\u7684\u7ed3\u6784\u4fee\u9970\u4e0e\u4f18\u5316\u3002 <\/p>\n

3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u54c1\u4e3b\u8981\u7528\u4e8e\u533b\u836f\u7814\u53d1\u548c\u7cbe\u7ec6\u5316\u5de5\u9886\u57df\uff0c\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a
\n– \u4f5c\u4e3a\u5173\u952e\u4e2d\u95f4\u4f53\u7528\u4e8e\u5408\u6210\u542b\u6c1f\u54cc\u5576\u7ed3\u6784\u7684\u6d3b\u6027\u836f\u7269\u6210\u5206\uff08API\uff09\uff0c\u5982\u795e\u7ecf\u7cfb\u7edf\u836f\u7269\u6216\u6297\u611f\u67d3\u836f\u7269\u3002
\n– \u5728\u5076\u8054\u53cd\u5e94\u6216\u5b98\u80fd\u56e2\u8f6c\u5316\u4e2d\u4f5c\u4e3a\u524d\u4f53\uff0c\u7528\u4e8e\u6784\u5efa\u590d\u6742\u6742\u73af\u5316\u5408\u7269\u3002
\n– \u5e94\u7528\u4e8e\u653e\u5c04\u6027\u6807\u8bb0\u6216\u63a2\u9488\u5206\u5b50\u7684\u5408\u6210\uff0c\u52a9\u529b\u751f\u7269\u533b\u5b66\u7814\u7a76\u3002 <\/p>\n

4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u81f34\u00b0C\u7684\u5e72\u71e5\u73af\u5883\u4e2d\u907f\u5149\u4fdd\u5b58\uff0c\u957f\u671f\u50a8\u5b58\u9700\u5145\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u60f0\u6027\u6c14\u6c1b\uff08\u5982\u6c2e\u6c14\u6216\u6c29\u6c14\uff09\u4e0b\u64cd\u4f5c\uff0c\u907f\u514d\u63a5\u89e6\u6c34\u5206\u6216\u5f3a\u9178\u5f3a\u78b1\u3002\u5f00\u5c01\u540e\u5e94\u5c3d\u5feb\u4f7f\u7528\uff0c\u5269\u4f59\u7269\u6599\u9700\u4e25\u683c\u5bc6\u5c01\u3002 <\/p>\n

5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u901a\u8fc7HPLC\u3001NMR\u548c\u8d28\u8c31\u8fdb\u884c\u8d28\u91cf\u63a7\u5236\uff0c\u786e\u4fdd\u7eaf\u5ea6\u4e0e\u7ed3\u6784\u7b26\u5408\u6807\u51c6\u3002\u5b89\u5168\u4fe1\u606f\u5982\u4e0b\uff1a
\n– \u53ef\u80fd\u5bf9\u76ae\u80a4\u3001\u773c\u775b\u548c\u547c\u5438\u9053\u6709\u523a\u6fc0\u6027\uff0c\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u9632\u62a4\u624b\u5957\u3001\u62a4\u76ee\u955c\u53ca\u9632\u5c18\u53e3\u7f69\u3002
\n– \u82e5\u4e0d\u614e\u63a5\u89e6\uff0c\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002
\n– \u5e9f\u5f03\u7269\u5e94\u6309\u7167\u5371\u9669\u5316\u5b66\u54c1\u89c4\u8303\u5904\u7f6e\uff0c\u907f\u514d\u73af\u5883\u6c61\u67d3\u3002 <\/p>\n

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