\u4ea7\u54c1\u8bf4\u660e <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u5316\u5b66\u540d\u79f0\u4e3a4,5-PyriMidinediaMine, 6-chloro-N4-[(3aS,4R,6S,6aR)-6-[2-[[(1,1-diMethylethyl)diMethylsilyl]oxy]ethoxy]tetrahydro-2,2-diMethyl-4H-cyclopenta-1,3-dioxol-4-yl]-2-(propylthio)-\uff0c\u4e2d\u6587\u540d\u79f0\u4e3aN4-((3AS,4R,6S,6AR)-6-(2-((\u53d4\u4e01\u57fa\u4e8c\u7532\u57fa\u7845\u70f7\u57fa)\u6c27\u57fa)\u4e59\u6c27\u57fa)-2\u3002\u5176CAS\u53f7\u4e3a1400665-91-9\uff0c\u5206\u5b50\u5f0f\u4e3aC23H41ClN4O4SSi\uff0c\u5206\u5b50\u91cf\u4e3a533.2\uff0c\u7eaf\u5ea6\u9ad8\u4e8e96%\u3002\u8be5\u5316\u5408\u7269\u662f\u4e00\u79cd\u5177\u6709\u590d\u6742\u7ed3\u6784\u7684\u5627\u5576\u884d\u751f\u7269\uff0c\u542b\u6709\u53d4\u4e01\u57fa\u4e8c\u7532\u57fa\u7845\u70f7\u57fa\uff08TBDMS\uff09\u4fdd\u62a4\u57fa\u56e2\u548c\u786b\u4ee3\u4e19\u57fa\u5b98\u80fd\u56e2\uff0c\u5177\u6709\u8f83\u9ad8\u7684\u5316\u5b66\u7a33\u5b9a\u6027\u548c\u7279\u5b9a\u7684\u751f\u7269\u6d3b\u6027\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u5728\u6838\u82f7\u9178\u7c7b\u4f3c\u7269\u5408\u6210\u4e2d\u5177\u6709\u91cd\u8981\u5e94\u7528\uff0c\u53ef\u4f5c\u4e3a\u4e2d\u95f4\u4f53\u7528\u4e8e\u4fee\u9970\u6838\u9178\u7ed3\u6784\u3002\u5176\u5627\u5576\u9aa8\u67b6\u548c\u786b\u4ee3\u4e19\u57fa\u7ed3\u6784\u4f7f\u5176\u80fd\u591f\u53c2\u4e0e\u6838\u82f7\u9178\u4ee3\u8c22\u9014\u5f84\u7684\u8c03\u63a7\uff0c\u5e76\u5728\u6297\u75c5\u6bd2\u6216\u6297\u80bf\u7624\u836f\u7269\u7684\u7814\u53d1\u4e2d\u53d1\u6325\u5173\u952e\u4f5c\u7528\u3002\u6b64\u5916\uff0cTBDMS\u4fdd\u62a4\u57fa\u56e2\u7684\u5f15\u5165\u589e\u5f3a\u4e86\u5316\u5408\u7269\u7684\u7a33\u5b9a\u6027\uff0c\u4fbf\u4e8e\u5728\u590d\u6742\u5408\u6210\u53cd\u5e94\u4e2d\u4fdd\u6301\u7ed3\u6784\u5b8c\u6574\u6027\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u533b\u836f\u7814\u53d1\u9886\u57df\uff0c\u7279\u522b\u662f\u6838\u82f7\u9178\u7c7b\u4f3c\u7269\u548c\u6297\u75c5\u6bd2\u836f\u7269\u7684\u5408\u6210\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a
\n– \u4f5c\u4e3a\u5173\u952e\u4e2d\u95f4\u4f53\u7528\u4e8e\u5408\u6210\u5177\u6709\u751f\u7269\u6d3b\u6027\u7684\u6838\u82f7\u9178\u884d\u751f\u7269\uff1b
\n– \u7528\u4e8e\u7814\u7a76\u6838\u82f7\u9178\u4ee3\u8c22\u9014\u5f84\u53ca\u5f00\u53d1\u65b0\u578b\u6297\u75c5\u6bd2\u6216\u6297\u80bf\u7624\u836f\u7269\uff1b
\n– \u5728\u6709\u673a\u5408\u6210\u4e2d\u4f5c\u4e3a\u4fdd\u62a4\u57fa\u56e2\u4fee\u9970\u7684\u53c2\u8003\u5316\u5408\u7269\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5c06\u672c\u54c1\u7f6e\u4e8e-20\u00b0C\u4ee5\u4e0b\u5e72\u71e5\u3001\u907f\u5149\u7684\u73af\u5883\u4e2d\u4fdd\u5b58\uff0c\u4ee5\u786e\u4fdd\u5176\u957f\u671f\u7a33\u5b9a\u6027\u3002\u4f7f\u7528\u65f6\u9700\u5728\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u4fdd\u62a4\u4e0b\u64cd\u4f5c\uff0c\u907f\u514d\u66b4\u9732\u4e8e\u6f6e\u6e7f\u7a7a\u6c14\u6216\u5f3a\u6c27\u5316\u5242\u3002\u6eb6\u89e3\u5efa\u8bae\u4f7f\u7528\u65e0\u6c34\u6709\u673a\u6eb6\u5242\uff08\u5982DMSO\u6216DMF\uff09\uff0c\u5e76\u5728\u4f7f\u7528\u524d\u8fdb\u884c\u7eaf\u5ea6\u9a8c\u8bc1\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u901a\u8fc7HPLC\u548c\u8d28\u8c31\u5206\u6790\u786e\u4fdd\u7eaf\u5ea6\u9ad8\u4e8e96%\u3002\u4f7f\u7528\u65f6\u9700\u7a7f\u6234\u9002\u5f53\u7684\u9632\u62a4\u88c5\u5907\uff08\u5982\u624b\u5957\u3001\u62a4\u76ee\u955c\u548c\u5b9e\u9a8c\u670d\uff09\uff0c\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u76ae\u80a4\u6216\u5438\u5165\u7c89\u5c18\u3002\u5982\u4e0d\u614e\u63a5\u89e6\uff0c\u8bf7\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u672c\u4ea7\u54c1\u4ec5\u9650\u79d1\u7814\u7528\u9014\uff0c\u4e0d\u53ef\u7528\u4e8e\u4eba\u4f53\u6216\u52a8\u7269\u5b9e\u9a8c\u3002 <\/p>\n
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