2-(4-\u6eb4-2-\u6c2f\u82ef\u57fa)\u4e19-2-\u80fa\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u4e3a2-(4-\u6eb4-2-\u6c2f\u82ef\u57fa)\u4e19-2-\u80fa\uff0c\u5316\u5b66\u5f0f\u4e3aC9H11BrClN\uff0c\u5206\u5b50\u91cf248.547\uff0cCAS\u53f71314740-58-3\u3002\u8be5\u5316\u5408\u7269\u662f\u4e00\u79cd\u542b\u5364\u7d20\u53d6\u4ee3\u7684\u82ef\u4e19\u80fa\u884d\u751f\u7269\uff0c\u7eaf\u5ea6>96%\uff0c\u5e38\u6e29\u4e0b\u5448\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6216\u7c89\u672b\u72b6\u3002\u5176\u7ed3\u6784\u4e2d\u6eb4\u548c\u6c2f\u539f\u5b50\u7684\u5f15\u5165\u663e\u8457\u589e\u5f3a\u4e86\u5206\u5b50\u7684\u7535\u5b50\u6548\u5e94\u548c\u7a7a\u95f4\u4f4d\u963b\uff0c\u4f7f\u5176\u5728\u6709\u673a\u5408\u6210\u548c\u836f\u7269\u5316\u5b66\u4e2d\u5177\u6709\u72ec\u7279\u53cd\u5e94\u6d3b\u6027\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u82b3\u9999\u80fa\u7c7b\u5316\u5408\u7269\uff0c\u8be5\u5206\u5b50\u53ef\u901a\u8fc7\u6c28\u57fa\u4e0e\u7fa7\u57fa\u6216\u7fb0\u57fa\u7684\u7f29\u5408\u53cd\u5e94\u53c2\u4e0e\u6742\u73af\u6784\u5efa\uff0c\u5176\u82ef\u73af\u4e0a\u7684\u5364\u7d20\u4f4d\u70b9\uff08\u6eb4\u3001\u6c2f\uff09\u4e3a\u540e\u7eed Suzuki\u5076\u8054\u3001Buchwald-Hartwig\u80fa\u5316\u7b49\u4ea4\u53c9\u5076\u8054\u53cd\u5e94\u63d0\u4f9b\u5173\u952e\u4fee\u9970\u4f4d\u70b9\u3002\u5728\u795e\u7ecf\u836f\u7406\u5b66\u7814\u7a76\u4e2d\uff0c\u6b64\u7c7b\u7ed3\u6784\u53ef\u80fd\u4f5c\u4e3a\u591a\u5df4\u80fa\/5-\u7f9f\u8272\u80fa\u53d7\u4f53\u8c03\u8282\u5242\u7684\u4e2d\u95f4\u4f53\uff0c\u4f46\u9700\u6ce8\u610f\u5176\u672a\u7ecf\u6279\u51c6\u7528\u4e8e\u4eba\u4f53\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u4ea7\u54c1\u4e3b\u8981\u5e94\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a
\n(1) \u533b\u836f\u7814\u53d1\uff1a\u4f5c\u4e3a\u6fc0\u9176\u6291\u5236\u5242\u6216G\u86cb\u767d\u5076\u8054\u53d7\u4f53\u914d\u4f53\u7684\u5408\u6210\u780c\u5757
\n(2) \u6750\u6599\u79d1\u5b66\uff1a\u7528\u4e8e\u5236\u5907\u542b\u5364\u7d20\u529f\u80fd\u56e2\u7684\u6709\u673a\u5149\u7535\u6750\u6599\u524d\u4f53
\n(3) \u5b66\u672f\u7814\u7a76\uff1a\u5728\u91d1\u5c5e\u50ac\u5316\u53cd\u5e94\u673a\u7406\u7814\u7a76\u4e2d\u4f5c\u4e3a\u6a21\u578b\u5e95\u7269 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u50a8\u5b58\u4e8e-20\u2103\u907f\u5149\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u5145\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u4ee5\u5ef6\u957f\u7a33\u5b9a\u6027\u3002\u5f00\u5c01\u540e\u5efa\u8bae\u5206\u88c5\u4f7f\u7528\uff0c\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002\u5b9e\u9a8c\u64cd\u4f5c\u9700\u5728\u901a\u98ce\u6a71\u4e2d\u8fdb\u884c\uff0c\u4f69\u6234\u9632\u5316\u624b\u5957\u53ca\u62a4\u76ee\u955c\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u8868\u660e\u5176\u6613\u6eb6\u4e8e\u4e8c\u6c2f\u7532\u70f7\u3001THF\u7b49\u6709\u673a\u6eb6\u5242\uff0c\u6c34\u6eb6\u6027\u8f83\u5dee\uff08<0.1 mg\/mL\uff09\u3002 \n\n5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f \n\u901a\u8fc7HPLC\uff08C18\u67f1\uff0c\u4e59\u8148\/\u6c34\u68af\u5ea6\u6d17\u8131\uff09\u786e\u4fdd\u7eaf\u5ea6>96%\uff0cGC-MS\u9a8c\u8bc1\u65e0\u91cd\u91d1\u5c5e\u6b8b\u7559\u3002\u6839\u636eGHS\u5206\u7c7b\uff0c\u8be5\u4ea7\u54c1\u53ef\u80fd\u9020\u6210\u76ae\u80a4\u523a\u6fc0\uff08\u7c7b\u522b2\uff09\u548c\u773c\u635f\u4f24\uff08\u7c7b\u522b1\uff09\uff0c\u5b89\u5168\u6570\u636e\u8868\uff08SDS\uff09\u5df2\u5907\u6848\u3002\u8fd0\u8f93\u65f6\u9700\u7b26\u5408UN2811\u5371\u9669\u54c1\u89c4\u8303\uff0c\u4e25\u7981\u4e0e\u5f3a\u6c27\u5316\u5242\u5171\u5b58\u3002\u5e9f\u5f03\u7269\u5904\u7f6e\u5e94\u9075\u5faa\u5f53\u5730\u6cd5\u89c4\uff0c\u5efa\u8bae\u91c7\u7528\u4e13\u4e1a\u5371\u5e9f\u5904\u7406\u516c\u53f8\u56de\u6536\u3002 <\/p>\n
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