3,3-\u4e8c\u6c1f-4-\u54cc\u5576\u7532\u9187\u76d0\u9178\u76d0\u4ea7\u54c1\u8bf4\u660e\u4e66<\/p>\n
\u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u5316\u5b66\u540d\u79f0\u4e3a(3,3-Difluoro-4-piperidinyl)methanol hydrochloride (1:1)\uff0c\u662f\u4e00\u79cd\u542b\u6c1f\u54cc\u5576\u884d\u751f\u7269\uff0cCAS\u53f7\u4e3a1783945-29-8\u3002\u5176\u5206\u5b50\u5f0f\u4e3aC6H12ClF2NO\uff0c\u5206\u5b50\u91cf187.615\uff0c\u5916\u89c2\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\u3002\u8be5\u5316\u5408\u7269\u5728\u7ed3\u6784\u4e2d\u540c\u65f6\u5177\u5907\u54cc\u5576\u73af\u3001\u4e8c\u6c1f\u53d6\u4ee3\u57fa\u53ca\u7f9f\u7532\u57fa\u5b98\u80fd\u56e2\uff0c\u4f7f\u5176\u517c\u5177\u4eb2\u6c34\u6027\u548c\u4eb2\u8102\u6027\uff0c\u6613\u6eb6\u4e8e\u6781\u6027\u6709\u673a\u6eb6\u5242\u5982\u7532\u9187\u3001DMSO\u7b49\u3002\u4ea7\u54c1\u7ecfHPLC\u68c0\u6d4b\u7eaf\u5ea6>96%\uff0c\u7b26\u5408\u751f\u5316\u8bd5\u5242\u6807\u51c6\u3002<\/p>\n
\u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u54cc\u5576\u7c7b\u5316\u5408\u7269\u7684\u6c1f\u4ee3\u884d\u751f\u7269\uff0c\u5176\u5206\u5b50\u4e2d\u7684\u4e8c\u6c1f\u53d6\u4ee3\u53ef\u663e\u8457\u6539\u53d8\u7535\u5b50\u4e91\u5206\u5e03\uff0c\u589e\u5f3a\u4ee3\u8c22\u7a33\u5b9a\u6027\u3002\u7f9f\u7532\u57fa\u7684\u5f15\u5165\u63d0\u4f9b\u4e86\u91cd\u8981\u7684\u5206\u5b50\u4fee\u9970\u4f4d\u70b9\uff0c\u4f7f\u5176\u6210\u4e3a\u5408\u6210\u591a\u79cd\u751f\u7269\u6d3b\u6027\u5206\u5b50\u7684\u5173\u952e\u4e2d\u95f4\u4f53\u3002\u8be5\u7ed3\u6784\u7279\u5f81\u4f7f\u5176\u5728\u8c03\u8282\u5316\u5408\u7269\u8102\u6eb6\u6027\u548c\u6c22\u952e\u5f62\u6210\u80fd\u529b\u65b9\u9762\u5177\u6709\u72ec\u7279\u4f18\u52bf\uff0c\u5bf9\u836f\u7269\u5206\u5b50\u7684\u8840\u8111\u5c4f\u969c\u7a7f\u900f\u6027\u548c\u9776\u6807\u7ed3\u5408\u4eb2\u548c\u529b\u5177\u6709\u91cd\u8981\u5f71\u54cd\u3002<\/p>\n
\u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n1. \u533b\u836f\u7814\u53d1\u9886\u57df\uff1a\u4f5c\u4e3a\u6838\u5fc3\u9aa8\u67b6\u7528\u4e8e\u795e\u7ecf\u7cfb\u7edf\u836f\u7269\u3001\u9547\u75db\u5242\u53ca\u6297\u80bf\u7624\u836f\u7269\u7684\u5408\u6210
\n2. \u6750\u6599\u79d1\u5b66\uff1a\u7528\u4e8e\u5236\u5907\u542b\u6c1f\u529f\u80fd\u6750\u6599\u7684\u524d\u4f53\u5316\u5408\u7269
\n3. \u751f\u5316\u7814\u7a76\uff1a\u4f5c\u4e3a\u9176\u6291\u5236\u5242\u6216\u53d7\u4f53\u8c03\u8282\u5242\u7684\u7ed3\u6784\u6a21\u5757
\n4. \u519c\u836f\u5f00\u53d1\uff1a\u4f5c\u4e3a\u65b0\u578b\u542b\u6c1f\u519c\u836f\u7684\u4e2d\u95f4\u4f53
\n\u5178\u578b\u5e94\u7528\u5305\u62ec\u4f46\u4e0d\u9650\u4e8e\uff1a\u86cb\u767d\u6fc0\u9176\u6291\u5236\u5242\u7684\u7ed3\u6784\u4f18\u5316\u3001G\u86cb\u767d\u5076\u8054\u53d7\u4f53\u914d\u4f53\u7684\u5408\u6210\u3001\u4ee5\u53caPET\u663e\u5f71\u5242\u7684\u5f00\u53d1\u3002<\/p>\n
\u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u672c\u54c1\u5e94\u5bc6\u5c01\u4fdd\u5b58\u4e8e-20\u2103\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u907f\u514d\u5149\u7167\u548c\u6f6e\u6e7f\u3002\u5f00\u5c01\u540e\u5efa\u8bae\u5145\u6c2e\u4fdd\u62a4\uff0c\u5e76\u4e8e6\u4e2a\u6708\u5185\u4f7f\u7528\u5b8c\u6bd5\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u60f0\u6027\u6c14\u4f53\u73af\u5883\u4e0b\u64cd\u4f5c\uff0c\u5efa\u8bae\u4f69\u6234\u9632\u62a4\u624b\u5957\u548c\u62a4\u76ee\u955c\u3002\u6eb6\u89e3\u65f6\u53ef\u5148\u7528\u5c11\u91cfDMSO\u52a9\u6eb6\uff0c\u518d\u7528\u7f13\u51b2\u6db2\u7a00\u91ca\u81f3\u5de5\u4f5c\u6d53\u5ea6\u3002\u907f\u514d\u4e0e\u5f3a\u6c27\u5316\u5242\u63a5\u89e6\u3002<\/p>\n
\u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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