\u4ea7\u54c1\u8bf4\u660e <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u4e3a(4,4-\u4e8c\u6c1f-1-{[(2-\u7532\u57fa-2-\u4e19\u70f7\u57fa)\u6c27\u57fa]\u7fb0\u57fa}-3-\u54cc\u5576\u57fa)\u4e59\u9178\uff0c\u5316\u5b66\u540d\u79f0\uff1a(4,4-Difluoro-1-{[(2-methyl-2-propanyl)oxy]carbonyl}-3-piperidinyl)acetic acid\uff0cCAS\u53f7\uff1a1334417-29-6\u3002\u5176\u5206\u5b50\u5f0f\u4e3aC12H19F2NO4\uff0c\u5206\u5b50\u91cf\u4e3a279.28\uff0c\u7eaf\u5ea6\u9ad8\u4e8e96%\u3002\u8be5\u5316\u5408\u7269\u662f\u4e00\u79cd\u542b\u6c1f\u54cc\u5576\u884d\u751f\u7269\uff0c\u5177\u6709\u72ec\u7279\u7684\u7ed3\u6784\u7279\u5f81\uff0c\u5305\u62ec\u4e8c\u6c1f\u53d6\u4ee3\u7684\u54cc\u5576\u73af\u548c\u53d4\u4e01\u6c27\u7fb0\u57fa\uff08Boc\uff09\u4fdd\u62a4\u57fa\u56e2\uff0c\u4ee5\u53ca\u672b\u7aef\u7fa7\u9178\u5b98\u80fd\u56e2\uff0c\u4f7f\u5176\u5728\u6709\u673a\u5408\u6210\u548c\u836f\u7269\u5316\u5b66\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u4f5c\u4e3a\u54cc\u5576\u7c7b\u884d\u751f\u7269\uff0c\u5176\u7ed3\u6784\u4e2d\u7684\u4e8c\u6c1f\u53d6\u4ee3\u548cBoc\u4fdd\u62a4\u57fa\u56e2\u8d4b\u4e88\u5176\u826f\u597d\u7684\u5316\u5b66\u7a33\u5b9a\u6027\u548c\u53cd\u5e94\u6d3b\u6027\u3002\u7fa7\u9178\u5b98\u80fd\u56e2\u4f7f\u5176\u6613\u4e8e\u4e0e\u5176\u4ed6\u5206\u5b50\u5f62\u6210\u9170\u80fa\u952e\u6216\u916f\u952e\uff0c\u9002\u7528\u4e8e\u591a\u79cd\u751f\u7269\u5076\u8054\u53cd\u5e94\u3002\u5728\u836f\u7269\u7814\u53d1\u4e2d\uff0c\u6b64\u7c7b\u7ed3\u6784\u5e38\u4f5c\u4e3a\u4e2d\u95f4\u4f53\u7528\u4e8e\u6784\u5efa\u5177\u6709\u751f\u7269\u6d3b\u6027\u7684\u5206\u5b50\uff0c\u5c24\u5176\u662f\u9776\u5411\u9176\u6216\u53d7\u4f53\u7684\u6291\u5236\u5242\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u533b\u836f\u7814\u53d1\u548c\u6709\u673a\u5408\u6210\u9886\u57df\uff0c\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a
\n– \u4f5c\u4e3a\u5173\u952e\u4e2d\u95f4\u4f53\u7528\u4e8e\u5408\u6210\u542b\u6c1f\u54cc\u5576\u7c7b\u836f\u7269\u5206\u5b50\uff0c\u5982\u86cb\u767d\u9176\u6291\u5236\u5242\u6216\u795e\u7ecf\u9012\u8d28\u8c03\u8282\u5242\u3002
\n– \u5728\u80bd\u7c7b\u5316\u5408\u7269\u4fee\u9970\u4e2d\uff0c\u901a\u8fc7\u7fa7\u9178\u5b98\u80fd\u56e2\u4e0e\u5176\u4ed6\u6c28\u57fa\u5316\u5408\u7269\u5076\u8054\uff0c\u6269\u5c55\u5206\u5b50\u591a\u6837\u6027\u3002
\n– \u7528\u4e8e\u6c1f\u5316\u5316\u5408\u7269\u7684\u7814\u7a76\uff0c\u63a2\u7d22\u5176\u751f\u7269\u6d3b\u6027\u4e0e\u4ee3\u8c22\u7a33\u5b9a\u6027\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5c06\u672c\u54c1\u7f6e\u4e8e\u5e72\u71e5\u3001\u907f\u5149\u7684\u73af\u5883\u4e2d\uff0c\u50a8\u5b58\u6e29\u5ea6\u4e3a-20\u00b0C\uff0c\u4ee5\u4fdd\u6301\u5176\u957f\u671f\u7a33\u5b9a\u6027\u3002\u4f7f\u7528\u65f6\u9700\u5728\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u4fdd\u62a4\u4e0b\u64cd\u4f5c\uff0c\u907f\u514d\u66b4\u9732\u4e8e\u6f6e\u6e7f\u7a7a\u6c14\u6216\u5f3a\u9178\u5f3a\u78b1\u6761\u4ef6\u3002\u6eb6\u89e3\u5efa\u8bae\u4f7f\u7528\u6781\u6027\u6709\u673a\u6eb6\u5242\uff08\u5982DMF\u6216DMSO\uff09\uff0c\u5e76\u6839\u636e\u5b9e\u9a8c\u9700\u6c42\u8fdb\u4e00\u6b65\u7a00\u91ca\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u7ecfHPLC\u68c0\u6d4b\uff0c\u7eaf\u5ea6>96%\uff0c\u7b26\u5408\u79d1\u7814\u7ea7\u6807\u51c6\u3002\u4f7f\u7528\u65f6\u9700\u7a7f\u6234\u9632\u62a4\u88c5\u5907\uff08\u5982\u624b\u5957\u3001\u62a4\u76ee\u955c\uff09\uff0c\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u76ae\u80a4\u6216\u5438\u5165\u7c89\u5c18\u3002\u5982\u4e0d\u614e\u63a5\u89e6\uff0c\u5e94\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5e94\u6309\u7167\u6709\u673a\u5316\u5b66\u54c1\u5904\u7406\u89c4\u8303\u5904\u7f6e\u3002 <\/p>\n
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