Boc-(+\/-)-trans-4-(4-isopropyl-phenyl)-pyrrolidine-3-carboxylic acid\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u662f\u4e00\u79cd\u9ad8\u7eaf\u5ea6\u6709\u673a\u5316\u5408\u7269\uff0c\u5316\u5b66\u540d\u79f0\u4e3aBoc-(+\/-)-trans-4-(4-isopropyl-phenyl)-pyrrolidine-3-carboxylic acid\uff0cCAS\u53f7\u4e3a1394827-14-5\u3002\u5176\u5206\u5b50\u5f0f\u4e3aC19H27NO4\uff0c\u5206\u5b50\u91cf\u4e3a333.42198\uff0c\u7eaf\u5ea6\u8d85\u8fc796%\u3002\u8be5\u5316\u5408\u7269\u5c5e\u4e8e\u5421\u54af\u70f7\u7fa7\u9178\u884d\u751f\u7269\uff0c\u7ed3\u6784\u4e2d\u5305\u542bBoc\uff08\u53d4\u4e01\u6c27\u7fb0\u57fa\uff09\u4fdd\u62a4\u57fa\u548c\u5f02\u4e19\u57fa\u82ef\u57fa\u56e2\uff0c\u5177\u6709\u7279\u5b9a\u7684\u7acb\u4f53\u6784\u578b\uff08trans-\u6784\u578b\uff09\u3002\u5176\u5316\u5b66\u6027\u8d28\u7a33\u5b9a\uff0c\u9002\u5408\u4f5c\u4e3a\u4e2d\u95f4\u4f53\u7528\u4e8e\u6709\u673a\u5408\u6210\u548c\u836f\u7269\u7814\u53d1\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u5728\u751f\u7269\u5316\u5b66\u9886\u57df\u5177\u6709\u91cd\u8981\u4ef7\u503c\uff0c\u5176\u7ed3\u6784\u4e2d\u7684\u5421\u54af\u70f7\u73af\u548c\u7fa7\u9178\u57fa\u56e2\u4f7f\u5176\u6210\u4e3a\u591a\u80bd\u5408\u6210\u548c\u836f\u7269\u5206\u5b50\u8bbe\u8ba1\u7684\u5173\u952e\u4e2d\u95f4\u4f53\u3002Boc\u4fdd\u62a4\u57fa\u7684\u5b58\u5728\u589e\u5f3a\u4e86\u5176\u5728\u9178\u6027\u6761\u4ef6\u4e0b\u7684\u7a33\u5b9a\u6027\uff0c\u4fbf\u4e8e\u540e\u7eed\u8131\u4fdd\u62a4\u548c\u5b98\u80fd\u56e2\u4fee\u9970\u3002\u6b64\u5916\uff0c\u5f02\u4e19\u57fa\u82ef\u57fa\u56e2\u7684\u5f15\u5165\u53ef\u80fd\u5f71\u54cd\u5316\u5408\u7269\u7684\u758f\u6c34\u6027\u548c\u751f\u7269\u6d3b\u6027\uff0c\u4f7f\u5176\u5728\u9776\u5411\u836f\u7269\u5f00\u53d1\u4e2d\u5177\u6709\u6f5c\u5728\u5e94\u7528\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u533b\u836f\u7814\u53d1\u548c\u6709\u673a\u5408\u6210\u9886\u57df\uff0c\u5177\u4f53\u7528\u9014\u5305\u62ec\u4f46\u4e0d\u9650\u4e8e\u4ee5\u4e0b\u65b9\u9762\uff1a\u4f5c\u4e3a\u624b\u6027\u780c\u5757\u7528\u4e8e\u975e\u5929\u7136\u6c28\u57fa\u9178\u7684\u5408\u6210\uff1b\u4f5c\u4e3a\u4e2d\u95f4\u4f53\u53c2\u4e0e\u591a\u80bd\u7c7b\u836f\u7269\u7684\u5236\u5907\uff1b\u7528\u4e8e\u6784\u5efa\u5177\u6709\u751f\u7269\u6d3b\u6027\u7684\u5c0f\u5206\u5b50\u5316\u5408\u7269\u5e93\u3002\u6b64\u5916\uff0c\u5176\u7ed3\u6784\u7279\u6027\u4f7f\u5176\u5728\u9176\u6291\u5236\u5242\u548c\u53d7\u4f53\u8c03\u8282\u5242\u7684\u7814\u7a76\u4e2d\u5177\u6709\u4e00\u5b9a\u6f5c\u529b\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5c06\u672c\u54c1\u7f6e\u4e8e-20\u00b0C\u7684\u5e72\u71e5\u73af\u5883\u4e2d\u907f\u5149\u4fdd\u5b58\uff0c\u957f\u671f\u50a8\u5b58\u9700\u5145\u5165\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u4ee5\u4fdd\u6301\u7a33\u5b9a\u6027\u3002\u4f7f\u7528\u65f6\u5e94\u5728\u5e72\u71e5\u60f0\u6027\u6c14\u6c1b\uff08\u5982\u6c29\u6c14\u6216\u6c2e\u6c14\uff09\u4e0b\u64cd\u4f5c\uff0c\u907f\u514d\u63a5\u89e6\u5f3a\u9178\u3001\u5f3a\u78b1\u6216\u6c27\u5316\u5242\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u8868\u660e\uff0c\u8be5\u5316\u5408\u7269\u53ef\u6eb6\u4e8e\u4e8c\u7532\u57fa\u4e9a\u781c\uff08DMSO\uff09\u3001\u4e8c\u6c2f\u7532\u70f7\u7b49\u6709\u673a\u6eb6\u5242\uff0c\u4f46\u5728\u6c34\u4e2d\u7684\u6eb6\u89e3\u5ea6\u8f83\u4f4e\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u901a\u8fc7\u9ad8\u6548\u6db2\u76f8\u8272\u8c31\uff08HPLC\uff09\u548c\u6838\u78c1\u5171\u632f\uff08NMR\uff09\u8fdb\u884c\u4e25\u683c\u8d28\u91cf\u63a7\u5236\uff0c\u786e\u4fdd\u7eaf\u5ea6\u9ad8\u4e8e96%\u3002\u4f7f\u7528\u65f6\u5e94\u7a7f\u6234\u9002\u5f53\u7684\u9632\u62a4\u88c5\u5907\uff08\u5982\u624b\u5957\u3001\u62a4\u76ee\u955c\u548c\u5b9e\u9a8c\u670d\uff09\uff0c\u907f\u514d\u5438\u5165\u7c89\u5c18\u6216\u76f4\u63a5\u63a5\u89e6\u76ae\u80a4\u3002\u5982\u4e0d\u614e\u63a5\u89e6\uff0c\u5e94\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u672c\u4ea7\u54c1\u4ec5\u9650\u79d1\u7814\u7528\u9014\uff0c\u4e0d\u53ef\u7528\u4e8e\u4eba\u4f53\u6216\u52a8\u7269\u5b9e\u9a8c\u3002\u5e9f\u5f03\u7269\u5904\u7f6e\u9700\u7b26\u5408\u5f53\u5730\u73af\u4fdd\u6cd5\u89c4\u3002 <\/p>\n
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