1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u54c1\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\uff0c\u5316\u5b66\u540d\u79f0\u4e3a(E)4-((\u809f\u57fa)\u7532\u57fa)-\u82c4\u57fa(\u7532\u57fa)\u6c28\u57fa\u7532\u9178\u53d4\u4e01\u916f\uff08Carbamic acid, N-[[4-[(hydroxyimino)methyl]phenyl]methyl]-N-methyl-, 1,1-dimethylethyl ester\uff09\uff0cCAS\u53f71349198-30-6\uff0c\u5206\u5b50\u5f0fC14H20N2O3\uff0c\u5206\u5b50\u91cf264.32\u3002\u5176\u7ed3\u6784\u4e2d\u542b\u809f\u57fa\uff08-CH=NOH\uff09\u4e0e\u53d4\u4e01\u6c27\u7fb0\u57fa\uff08Boc\uff09\u4fdd\u62a4\u57fa\u56e2\uff0c\u8d4b\u4e88\u5176\u826f\u597d\u7684\u5316\u5b66\u7a33\u5b9a\u6027\u4e0e\u53cd\u5e94\u9009\u62e9\u6027\u3002\u7eaf\u5ea6\u7ecfHPLC\u9a8c\u8bc1\u226596%\uff0c\u6613\u6eb6\u4e8e\u6709\u673a\u6eb6\u5242\u5982DMSO\u3001\u7532\u9187\uff0c\u5fae\u6eb6\u4e8e\u6c34\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u4f5c\u4e3a\u6c28\u57fa\u4fdd\u62a4\u57fa\u56e2\u884d\u751f\u7269\uff0c\u5728\u80bd\u5408\u6210\u4e0e\u836f\u7269\u8bbe\u8ba1\u4e2d\u5177\u6709\u5173\u952e\u4f5c\u7528\u3002\u809f\u57fa\u53ef\u53c2\u4e0e\u751f\u7269\u6b63\u4ea4\u53cd\u5e94\uff0c\u800cBoc\u57fa\u56e2\u5728\u9178\u6027\u6761\u4ef6\u4e0b\u53ef\u9006\u8131\u4fdd\u62a4\uff0c\u5e7f\u6cdb\u5e94\u7528\u4e8e\u591a\u80bd\u56fa\u76f8\u5408\u6210\u3001\u86cb\u767d\u8d28\u4fee\u9970\u53ca\u5c0f\u5206\u5b50\u6291\u5236\u5242\u5f00\u53d1\u3002\u5176\u9ad8\u7eaf\u5ea6\u7279\u6027\u786e\u4fdd\u4e86\u751f\u5316\u53cd\u5e94\u7684\u91cd\u590d\u6027\u4e0e\u4ea7\u7269\u6536\u7387\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u4e3b\u8981\u5e94\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a
\n(1) \u836f\u7269\u7814\u53d1\uff1a\u4f5c\u4e3a\u4e2d\u95f4\u4f53\u7528\u4e8e\u6fc0\u9176\u6291\u5236\u5242\u3001\u6297\u80bf\u7624\u836f\u7269\u7684\u5408\u6210\uff1b
\n(2) \u86cb\u767d\u8d28\u5de5\u7a0b\uff1a\u901a\u8fc7\u809f\u952e\u5f62\u6210\u5b9e\u73b0\u5b9a\u70b9\u5076\u8054\uff0c\u7528\u4e8e\u6297\u4f53-\u836f\u7269\u5076\u8054\u7269\uff08ADC\uff09\u5f00\u53d1\uff1b
\n(3) \u6750\u6599\u79d1\u5b66\uff1a\u4fee\u9970\u9ad8\u5206\u5b50\u6750\u6599\u8868\u9762\u4ee5\u5f15\u5165\u529f\u80fd\u6027\u57fa\u56e2\u3002\u5178\u578b\u5b9e\u9a8c\u5305\u62ecBoc\u4fdd\u62a4\u6c28\u57fa\u7684\u8131\u4fdd\u62a4\u53cd\u5e94\uff08\u5982TFA\u5904\u7406\uff09\u53ca\u809f\u57fa\u4e0e\u919b\/\u916e\u7684\u7f29\u5408\u53cd\u5e94\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5bc6\u5c01\u4fdd\u5b58\u4e8e-20\u00b0C\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u907f\u514d\u5149\u7167\u4e0e\u6f6e\u6e7f\u3002\u5f00\u5c01\u540e\u9700\u5145\u6c2e\u4fdd\u62a4\u4ee5\u5ef6\u957f\u7a33\u5b9a\u6027\u3002\u4f7f\u7528\u65f6\u9700\u5728\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c29\u6c14\uff09\u73af\u5883\u4e0b\u64cd\u4f5c\uff0c\u6eb6\u89e3\u63a8\u8350\u4f7f\u7528\u65e0\u6c34DMSO\uff08\u6d53\u5ea6\u226410 mM\uff09\uff0c\u5de5\u4f5c\u6db2\u73b0\u914d\u73b0\u7528\u3002\u957f\u671f\u50a8\u5b58\u5efa\u8bae\u5206\u88c5\u4ee5\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u54c1\u7ecf\u8d28\u8c31\uff08MS\uff09\u4e0e\u6838\u78c1\u5171\u632f\uff08NMR\uff09\u786e\u8bc1\u7ed3\u6784\uff0cHPLC\u68c0\u6d4b\u5355\u4e00\u4e3b\u5cf0\u226596%\u3002\u5b89\u5168\u6570\u636e\uff1a
\n– \u5371\u5bb3\u63d0\u793a\uff1a\u53ef\u80fd\u5f15\u8d77\u76ae\u80a4\/\u773c\u775b\u523a\u6fc0\uff0c\u5438\u5165\u6216\u8bef\u98df\u6709\u5bb3\uff1b
\n– \u9632\u62a4\u63aa\u65bd\uff1a\u64cd\u4f5c\u65f6\u4f69\u6234\u62a4\u76ee\u955c\u3001\u9632\u5c18\u53e3\u7f69\u53ca\u4e01\u8148\u624b\u5957\uff1b
\n– \u5e94\u6025\u5904\u7406\uff1a\u63a5\u89e6\u76ae\u80a4\u7acb\u5373\u7528\u80a5\u7682\u6c34\u51b2\u6d17\uff0c\u6e85\u5165\u773c\u775b\u9700\u7528\u751f\u7406\u76d0\u6c34\u51b2\u6d1715\u5206\u949f\u5e76\u5c31\u533b\u3002
\n\u5e9f\u5f03\u7269\u5e94\u4f5c\u4e3a\u6709\u5bb3\u5316\u5b66\u54c1\u5904\u7f6e\uff0c\u9075\u5b88\u5f53\u5730\u6cd5\u89c4\u3002 <\/p>\n
\u6ce8\uff1a\u5177\u4f53\u5b9e\u9a8c\u65b9\u6848\u9700\u7ed3\u5408\u6587\u732e\u4f18\u5316\uff0c\u5efa\u8bae\u53c2\u8003\u6587\u732eDOI: 10.1021\/acs.joc.xxxxxxx\uff08\u793a\u4f8b\uff09\u4ee5\u83b7\u53d6\u8be6\u7ec6\u5e94\u7528\u6848\u4f8b\u3002<\/p>\n","protected":false},"featured_media":26037,"template":"","meta":{"_acf_changed":false,"_kad_blocks_custom_css":"","_kad_blocks_head_custom_js":"","_kad_blocks_body_custom_js":"","_kad_blocks_footer_custom_js":"","_kadence_starter_templates_imported_post":false,"_kad_post_transparent":"","_kad_post_title":"","_kad_post_layout":"","_kad_post_sidebar_id":"","_kad_post_content_style":"","_kad_post_vertical_padding":"","_kad_post_feature":"","_kad_post_feature_position":"","_kad_post_header":false,"_kad_post_footer":false,"_kad_post_classname":""},"product_category":[25],"class_list":["post-55094","chemical-product","type-chemical-product","status-publish","has-post-thumbnail","hentry","product_category-25"],"acf":[],"taxonomy_info":{"product_category":[{"value":25,"label":"\u5b9e\u9a8c\u836f\u54c1"}]},"featured_image_src_large":["https:\/\/bio-get.com\/wp-content\/uploads\/2026\/04\/1349198-30-6.jpg",464,464,false],"author_info":[],"comment_info":"","_links":{"self":[{"href":"https:\/\/bio-get.com\/index.php?rest_route=\/wp\/v2\/chemical-product\/55094","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/bio-get.com\/index.php?rest_route=\/wp\/v2\/chemical-product"}],"about":[{"href":"https:\/\/bio-get.com\/index.php?rest_route=\/wp\/v2\/types\/chemical-product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/bio-get.com\/index.php?rest_route=\/wp\/v2\/media\/26037"}],"wp:attachment":[{"href":"https:\/\/bio-get.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=55094"}],"wp:term":[{"taxonomy":"product_category","embeddable":true,"href":"https:\/\/bio-get.com\/index.php?rest_route=%2Fwp%2Fv2%2Fproduct_category&post=55094"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}