N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-2,3-dimethyl-L-phenylalanine \u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u662f\u4e00\u79cd\u5177\u6709\u7279\u5b9a\u4fdd\u62a4\u57fa\u56e2\u7684\u4fee\u9970\u6c28\u57fa\u9178\u884d\u751f\u7269\uff0c\u5316\u5b66\u540d\u79f0\u4e3aN-[(9H-Fluoren-9-ylmethoxy)carbonyl]-2,3-dimethyl-L-phenylalanine\uff0c\u7b80\u79f0Fmoc-2,3-dimethyl-L-phenylalanine\u3002\u5176CAS\u53f7\u4e3a1270295-08-3\uff0c\u5206\u5b50\u5f0f\u4e3aC26H25NO4\uff0c\u5206\u5b50\u91cf\u4e3a415.481\u3002\u8be5\u5316\u5408\u7269\u7eaf\u5ea6\u9ad8\u4e8e96%\uff0c\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\uff0c\u53ef\u6eb6\u4e8e\u5e38\u89c1\u6709\u673a\u6eb6\u5242\u5982\u4e8c\u7532\u57fa\u7532\u9170\u80fa\uff08DMF\uff09\u548c\u4e8c\u6c2f\u7532\u70f7\uff08DCM\uff09\uff0c\u4f46\u5728\u6c34\u4e2d\u6eb6\u89e3\u5ea6\u8f83\u4f4e\u3002\u5176\u7ed3\u6784\u4e2d\u7684Fmoc\u57fa\u56e2\uff089-\u82b4\u7532\u6c27\u7fb0\u57fa\uff09\u4e3a\u9178\u654f\u611f\u6027\u4fdd\u62a4\u57fa\uff0c\u5e38\u7528\u4e8e\u591a\u80bd\u56fa\u76f8\u5408\u6210\u4e2d\u7684\u6c28\u57fa\u4fdd\u62a4\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\nFmoc-2,3-dimethyl-L-phenylalanine\u662f\u4eba\u5de5\u8bbe\u8ba1\u7684\u975e\u5929\u7136\u6c28\u57fa\u9178\u884d\u751f\u7269\uff0c\u5176\u4fa7\u94fe\u76842,3-\u4e8c\u7532\u57fa\u82ef\u57fa\u7ed3\u6784\u53ef\u8d4b\u4e88\u591a\u80bd\u7279\u6b8a\u7684\u7a7a\u95f4\u4f4d\u963b\u548c\u758f\u6c34\u6027\u3002\u5728\u80bd\u94fe\u5408\u6210\u4e2d\uff0cFmoc\u57fa\u56e2\u53ef\u901a\u8fc7\u78b1\u6027\u6761\u4ef6\uff08\u5982\u54cc\u5576\/DMF\uff09\u9ad8\u6548\u8131\u9664\uff0c\u800c2,3-\u4e8c\u7532\u57fa\u82ef\u57fa\u7684\u5f15\u5165\u80fd\u589e\u5f3a\u80bd\u94fe\u7684\u6784\u8c61\u7a33\u5b9a\u6027\u6216\u4e0e\u9776\u86cb\u767d\u7684\u7279\u5f02\u6027\u7ed3\u5408\u80fd\u529b\u3002\u8fd9\u7c7b\u4fee\u9970\u6c28\u57fa\u9178\u5728\u836f\u7269\u7814\u53d1\u4e2d\u5c24\u4e3a\u91cd\u8981\uff0c\u53ef\u7528\u4e8e\u4f18\u5316\u80bd\u7c7b\u836f\u7269\u7684\u4ee3\u8c22\u7a33\u5b9a\u6027\u548c\u751f\u7269\u6d3b\u6027\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u4e3b\u8981\u5e94\u7528\u4e8e\u591a\u80bd\u836f\u7269\u5f00\u53d1\u3001\u7ed3\u6784\u751f\u7269\u5b66\u7814\u7a76\u548c\u751f\u7269\u5171\u8f6d\u5316\u5b66\u9886\u57df\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a1\uff09\u4f5c\u4e3aFmoc\u4fdd\u62a4\u7684\u5355\u4f53\u7528\u4e8e\u56fa\u76f8\u591a\u80bd\u5408\u6210\uff08SPPS\uff09\uff0c\u6784\u5efa\u5177\u6709\u7279\u5b9a\u758f\u6c34\u6838\u5fc3\u6216\u7ed3\u5408\u4f4d\u70b9\u7684\u80bd\u6bb5\uff1b2\uff09\u4f5c\u4e3a\u5206\u5b50\u63a2\u9488\u524d\u4f53\uff0c\u7814\u7a76\u86cb\u767d\u8d28-\u914d\u4f53\u76f8\u4e92\u4f5c\u7528\u673a\u5236\uff1b3\uff09\u5728\u65b0\u578b\u6297\u4f53\u5076\u8054\u836f\u7269\uff08ADC\uff09\u5f00\u53d1\u4e2d\uff0c\u4f5c\u4e3a\u8fde\u63a5\u5b50\u6216\u8f7d\u836f\u6a21\u5757\u7684\u4fee\u9970\u5355\u5143\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u3001\u907f\u5149\u3001\u5e72\u71e5\u6761\u4ef6\u4e0b\u957f\u671f\u50a8\u5b58\uff0c\u77ed\u671f\u4f7f\u7528\u53ef\u7f6e\u4e8e4\u00b0C\u73af\u5883\u3002\u5f00\u5c01\u540e\u9700\u5145\u5165\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u5bc6\u5c01\u4fdd\u5b58\uff0c\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u73af\u5883\u4e2d\u64cd\u4f5c\uff0c\u6eb6\u89e3\u5efa\u8bae\u91c7\u7528DMF\u6216DCM\u6eb6\u5242\uff0c\u5e76\u907f\u514d\u63a5\u89e6\u5f3a\u6c27\u5316\u5242\u6216\u5f3a\u9178\u3002\u5b9e\u9a8c\u8fc7\u7a0b\u4e2d\u5efa\u8bae\u4f69\u6234\u9632\u62a4\u624b\u5957\u548c\u62a4\u76ee\u955c\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u7ecfHPLC\u68c0\u6d4b\u7eaf\u5ea6\u226596%\uff0c\u6279\u6b21\u95f4\u4e00\u81f4\u6027\u4e25\u683c\u628a\u63a7\u3002\u5b89\u5168\u6570\u636e\u8868\u660e\uff0c\u8be5\u5316\u5408\u7269\u53ef\u80fd\u5bf9\u773c\u775b\u548c\u76ae\u80a4\u6709\u8f7b\u5fae\u523a\u6fc0\u6027\uff0c\u64cd\u4f5c\u65f6\u5e94\u9075\u5b88\u5b9e\u9a8c\u5ba4\u5b89\u5168\u89c4\u8303\u3002\u5982\u610f\u5916\u63a5\u89e6\uff0c\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u9700\u6309\u6709\u673a\u6709\u5bb3\u7269\u8d28\u5904\u7406\uff0c\u7981\u6b62\u76f4\u63a5\u6392\u653e\u81f3\u73af\u5883\u4e2d\u3002\u5982\u9700\u8fdb\u4e00\u6b65\u6bd2\u7406\u5b66\u6570\u636e\uff0c\u8bf7\u53c2\u9605\u968f\u9644\u7684\u5b89\u5168\u6280\u672f\u8bf4\u660e\u4e66\uff08MSDS\uff09\u3002<\/p>\n","protected":false},"featured_media":25541,"template":"","meta":{"_acf_changed":false,"_kad_blocks_custom_css":"","_kad_blocks_head_custom_js":"","_kad_blocks_body_custom_js":"","_kad_blocks_footer_custom_js":"","_kadence_starter_templates_imported_post":false,"_kad_post_transparent":"","_kad_post_title":"","_kad_post_layout":"","_kad_post_sidebar_id":"","_kad_post_content_style":"","_kad_post_vertical_padding":"","_kad_post_feature":"","_kad_post_feature_position":"","_kad_post_header":false,"_kad_post_footer":false,"_kad_post_classname":""},"product_category":[25],"class_list":["post-54901","chemical-product","type-chemical-product","status-publish","has-post-thumbnail","hentry","product_category-25"],"acf":[],"taxonomy_info":{"product_category":[{"value":25,"label":"\u5b9e\u9a8c\u836f\u54c1"}]},"featured_image_src_large":["https:\/\/bio-get.com\/wp-content\/uploads\/2026\/04\/1270295-08-3.jpg",464,464,false],"author_info":[],"comment_info":"","_links":{"self":[{"href":"https:\/\/bio-get.com\/index.php?rest_route=\/wp\/v2\/chemical-product\/54901","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/bio-get.com\/index.php?rest_route=\/wp\/v2\/chemical-product"}],"about":[{"href":"https:\/\/bio-get.com\/index.php?rest_route=\/wp\/v2\/types\/chemical-product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/bio-get.com\/index.php?rest_route=\/wp\/v2\/media\/25541"}],"wp:attachment":[{"href":"https:\/\/bio-get.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=54901"}],"wp:term":[{"taxonomy":"product_category","embeddable":true,"href":"https:\/\/bio-get.com\/index.php?rest_route=%2Fwp%2Fv2%2Fproduct_category&post=54901"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}