1-(\u53d4\u4e01\u6c27\u7fb0\u57fa)-2-\u7532\u57fa\u54cc\u5576-4-\u7fa7\u9178\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u5316\u5b66\u540d\u79f0\u4e3a1-(tert-Butoxycarbonyl)-2-methylpiperidine-4-carboxylic acid\uff0cCAS\u53f7\u4e3a193085-98-2\uff0c\u5206\u5b50\u5f0f\u4e3aC12H21NO4\uff0c\u5206\u5b50\u91cf\u4e3a243.299\u3002\u8be5\u5316\u5408\u7269\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\uff0c\u7eaf\u5ea6>96%\uff0c\u5c5e\u4e8e\u54cc\u5576\u7c7b\u884d\u751f\u7269\uff0c\u5177\u6709\u53d4\u4e01\u6c27\u7fb0\u57fa\uff08Boc\uff09\u4fdd\u62a4\u57fa\u56e2\u548c\u7fa7\u9178\u6d3b\u6027\u5b98\u80fd\u56e2\u3002\u5176\u7ed3\u6784\u4e2d\u7684Boc\u57fa\u56e2\u5728\u9178\u6027\u6761\u4ef6\u4e0b\u53ef\u8131\u4fdd\u62a4\uff0c\u800c\u7fa7\u9178\u57fa\u56e2\u53ef\u8fdb\u4e00\u6b65\u53c2\u4e0e\u7f29\u5408\u6216\u4fee\u9970\u53cd\u5e94\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u54cc\u5576\u73af\u7ed3\u6784\u7684\u4fee\u9970\u7269\uff0c\u8be5\u5316\u5408\u7269\u5728\u6709\u673a\u5408\u6210\u548c\u836f\u7269\u5316\u5b66\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002Boc\u4fdd\u62a4\u57fa\u80fd\u6709\u6548\u5c4f\u853d\u6c28\u57fa\u7684\u6d3b\u6027\uff0c\u5728\u80bd\u7c7b\u5316\u5408\u7269\u548c\u591a\u6b65\u5408\u6210\u4e2d\u63d0\u4f9b\u9009\u62e9\u6027\u4fdd\u62a4\u3002\u7fa7\u9178\u57fa\u56e2\u53ef\u901a\u8fc7\u916f\u5316\u3001\u9170\u80fa\u5316\u7b49\u53cd\u5e94\u5f15\u5165\u7279\u5b9a\u836f\u6548\u56e2\uff0c\u662f\u6784\u5efa\u4e2d\u67a2\u795e\u7ecf\u7cfb\u7edf\u836f\u7269\u3001\u6297\u708e\u5242\u53ca\u6297\u83cc\u5242\u7684\u5173\u952e\u4e2d\u95f4\u4f53\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u5e7f\u6cdb\u5e94\u7528\u4e8e\u533b\u836f\u7814\u53d1\u548c\u7cbe\u7ec6\u5316\u5de5\u9886\u57df\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a1\uff09\u4f5c\u4e3a\u624b\u6027\u5408\u6210\u5b50\u7528\u4e8e\u975e\u5929\u7136\u6c28\u57fa\u9178\u5236\u5907\uff1b2\uff09\u53c2\u4e0e\u6297\u80bf\u7624\u836f\u7269\uff08\u5982\u6fc0\u9176\u6291\u5236\u5242\uff09\u7684\u9aa8\u67b6\u6784\u5efa\uff1b3\uff09\u7528\u4e8e\u795e\u7ecf\u9012\u8d28\u7c7b\u4f3c\u7269\u7684\u5408\u6210\uff0c\u5982GABA\u53d7\u4f53\u8c03\u8282\u5242\uff1b4\uff09\u4f5c\u4e3a\u4fdd\u62a4\u578b\u4e2d\u95f4\u4f53\u7528\u4e8e\u56fa\u76f8\u80bd\u5408\u6210\uff08SPPS\uff09\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u4e0b\u907f\u5149\u5e72\u71e5\u50a8\u5b58\uff0c\u957f\u671f\u4fdd\u5b58\u9700\u5145\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u3002\u5f00\u5c01\u540e\u9700\u5bc6\u5c01\u9632\u6f6e\uff0c\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u73af\u5883\u4e0b\u64cd\u4f5c\uff0c\u82e5\u7528\u4e8e\u80bd\u5408\u6210\uff0c\u5efa\u8bae\u9884\u5148\u7528DCM\u6216DMF\u6eb6\u89e3\u3002\u6ce8\u610fBoc\u57fa\u56e2\u5bf9\u5f3a\u9178\u654f\u611f\uff0c\u8131\u4fdd\u62a4\u65f6\u5e94\u63a7\u5236\u4e09\u6c1f\u4e59\u9178\uff08TFA\uff09\u7528\u91cf\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u7ecfHPLC\u68c0\u6d4b\u7eaf\u5ea6>96%\uff0cMS\u548cNMR\u9a8c\u8bc1\u7ed3\u6784\u3002\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u9632\u62a4\u624b\u5957\u53ca\u62a4\u76ee\u955c\uff0c\u907f\u514d\u5438\u5165\u7c89\u5c18\u6216\u63a5\u89e6\u76ae\u80a4\u3002\u5982\u610f\u5916\u63a5\u89e6\uff0c\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5316\u5b66\u5e9f\u5f03\u7269\u5e94\u6309\u7167\u5371\u9669\u6709\u673a\u7269\u89c4\u8303\u5904\u7f6e\u3002\u5b89\u5168\u6570\u636e\u8868\uff08SDS\uff09\u53ef\u968f\u8d27\u63d0\u4f9b\u6216\u53e6\u884c\u7d22\u53d6\u3002 <\/p>\n
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