\u4ee5\u4e0b\u662f\u6839\u636e\u60a8\u7684\u8981\u6c42\u64b0\u5199\u7684\u4e13\u4e1a\u4ea7\u54c1\u8bf4\u660e\uff1a<\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u4e3aMethyl 5-[(3aR,4R,6aS)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl]pentanoate\uff0c\u4e2d\u6587\u540d\u79f0\u4e3a\u7532\u57fa5-[(3aR,4R,6aS)-2-\u6c27\u4ee3\u516d\u6c22-1H-\u567b\u5429\u5e76[3,4-d]\u54aa\u5511-4-\u57fa]\u620a\u9178\u916f\uff0cCAS\u53f7\u4e3a60562-11-0\u3002\u5176\u5206\u5b50\u5f0f\u4e3aC11H18N2O3S\uff0c\u5206\u5b50\u91cf\u4e3a258.337\uff0c\u7eaf\u5ea6\u7ecfHPLC\u68c0\u6d4b\u786e\u8ba4\u5927\u4e8e96%\u3002\u8be5\u5316\u5408\u7269\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\uff0c\u5177\u6709\u7279\u5b9a\u7684\u7acb\u4f53\u6784\u578b\uff083aR,4R,6aS\uff09\uff0c\u5728\u6709\u673a\u6eb6\u5242\u5982\u7532\u9187\u3001\u4e59\u9187\u4e2d\u5177\u6709\u4e2d\u7b49\u6eb6\u89e3\u6027\uff0c\u6c34\u6eb6\u6027\u8f83\u4f4e\u3002<\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5206\u5b50\u7ed3\u6784\u4e2d\u542b\u6709\u567b\u5429\u5e76\u54aa\u5511\u916e\u6838\u5fc3\u548c\u620a\u9178\u916f\u4fa7\u94fe\uff0c\u4f7f\u5176\u6210\u4e3a\u751f\u7269\u7d20\u4ee3\u8c22\u9014\u5f84\u4e2d\u7684\u91cd\u8981\u4e2d\u95f4\u4f53\u3002\u5176\u7acb\u4f53\u7279\u5f02\u6027\u7ed3\u6784\u5728\u9176\u4fc3\u53cd\u5e94\u4e2d\u8868\u73b0\u51fa\u663e\u8457\u7684\u9009\u62e9\u6027\uff0c\u53ef\u4f5c\u4e3a\u751f\u7269\u7d20\u5408\u6210\u9176\u7684\u5e95\u7269\u7c7b\u4f3c\u7269\u6216\u6291\u5236\u5242\u3002\u5728\u8f85\u9176A\u7fa7\u5316\u53cd\u5e94\u7814\u7a76\u4e2d\uff0c\u8be5\u5316\u5408\u7269\u80fd\u6a21\u62df\u751f\u7269\u7d20-\u7fa7\u57fa\u8f7d\u4f53\u86cb\u767d\u7684\u529f\u80fd\uff0c\u5bf9\u7814\u7a76\u7ef4\u751f\u7d20H\u4ee3\u8c22\u673a\u5236\u5177\u6709\u7279\u6b8a\u4ef7\u503c\u3002<\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u54c1\u4e3b\u8981\u5e94\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a\u4f5c\u4e3a\u751f\u7269\u5316\u5b66\u7814\u7a76\u7684\u6807\u51c6\u54c1\u7528\u4e8eHPLC\u5b9a\u91cf\u5206\u6790\uff1b\u5728\u836f\u7269\u7814\u53d1\u4e2d\u4f5c\u4e3a\u751f\u7269\u7d20\u62ee\u6297\u5242\u7684\u5408\u6210\u524d\u4f53\uff1b\u5728\u9176\u5b66\u7814\u7a76\u4e2d\u7528\u4e8e\u7fa7\u5316\u9176\u6291\u5236\u5b9e\u9a8c\u3002\u5177\u4f53\u53ef\u7528\u4e8e\uff1a\u5fae\u751f\u7269\u57f9\u517b\u5b9e\u9a8c\u4e2d\u751f\u7269\u7d20\u4ee3\u8c22\u9014\u5f84\u7684\u8c03\u63a7\uff1b\u5f00\u53d1\u65b0\u578b\u6297\u80bf\u7624\u836f\u7269\u9776\u70b9\u7814\u7a76\uff1b\u4f5c\u4e3a\u8bca\u65ad\u8bd5\u5242\u7ec4\u5206\u7528\u4e8e\u67d0\u4e9b\u9057\u4f20\u6027\u751f\u7269\u7d20\u4ee3\u8c22\u7f3a\u9677\u75be\u75c5\u7684\u68c0\u6d4b\u3002<\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u50a8\u5b58\u4e8e-20\u2103\u7684\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u907f\u5149\u4fdd\u5b58\u4e8e\u5bc6\u5c01\u5bb9\u5668\u5185\u3002\u5f00\u5c01\u540e\u5efa\u8bae\u5145\u5165\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u3002\u4f7f\u7528\u65f6\u9700\u6062\u590d\u81f3\u5ba4\u6e29\u518d\u5f00\u5c01\uff0c\u907f\u514d\u51b7\u51dd\u6c34\u5f71\u54cd\u3002\u5de5\u4f5c\u6eb6\u6db2\u5efa\u8bae\u73b0\u914d\u73b0\u7528\uff0c\u6eb6\u5242\u9996\u9009\u65e0\u6c34DMSO\u6216\u4e59\u9187\u3002\u5b9e\u9a8c\u64cd\u4f5c\u5e94\u5728\u901a\u98ce\u6a71\u4e2d\u8fdb\u884c\uff0c\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u76ae\u80a4\u548c\u773c\u775b\u3002<\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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