(2R)-2,3-\u53cc[(2H27)\u5341\u56db\u70f7\u9170\u6c27\u57fa]\u4e19\u57fa-2-(\u4e09\u7532\u57fa\u94f5)\u4e59\u57fa\u78f7\u9178\u916f\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u4e3a\u6c18\u4ee3\u78f7\u8102\u884d\u751f\u7269\uff0c\u5316\u5b66\u540d\u79f0(2R)-2,3-\u53cc[(2H27)\u5341\u56db\u70f7\u9170\u6c27\u57fa]\u4e19\u57fa-2-(\u4e09\u7532\u57fa\u94f5)\u4e59\u57fa\u78f7\u9178\u916f\uff0cCAS\u53f778415-49-3\uff0c\u5206\u5b50\u5f0fC36H18D54NO8P\uff0c\u5206\u5b50\u91cf732.265\u3002\u5176\u7ed3\u6784\u7279\u70b9\u4e3a\u7518\u6cb9\u9aa8\u67b6\u76841,2\u4f4d\u8fde\u63a5\u5168\u6c18\u4ee3\u5341\u56db\u70f7\u9170\u94fe\uff082H27\uff09\uff0c3\u4f4d\u901a\u8fc7\u78f7\u9178\u4e8c\u916f\u952e\u4e0e\u80c6\u78b1\u7c7b\u4f3c\u7269\u7ed3\u5408\u3002\u6c18\u4ee3\u7387\u226598%\uff0c\u7eaf\u5ea6\u7ecfHPLC\u9a8c\u8bc1\uff1e96%\uff0c\u5448\u767d\u8272\u81f3\u7c7b\u767d\u8272\u56fa\u4f53\u5f62\u6001\uff0c\u6613\u6eb6\u4e8e\u6c2f\u4eff\u3001\u7532\u9187\u7b49\u6709\u673a\u6eb6\u5242\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u6c18\u6807\u8bb0\u7684\u78f7\u8102\u7c7b\u4f3c\u7269\uff0c\u8be5\u5316\u5408\u7269\u5728\u819c\u751f\u7269\u5b66\u7814\u7a76\u4e2d\u5177\u6709\u72ec\u7279\u4ef7\u503c\uff1a\u6c18\u4ee3\u9170\u57fa\u94fe\u53ef\u663e\u8457\u964d\u4f4e\u6838\u78c1\u5171\u632f\uff08NMR\uff09\u68c0\u6d4b\u80cc\u666f\u566a\u58f0\uff0c\u63d0\u9ad8\u4fe1\u53f7\u5206\u8fa8\u7387\uff1b\u5176\u7ed3\u6784\u4e0e\u5929\u7136\u78f7\u8102\u9170\u80c6\u78b1\u9ad8\u5ea6\u76f8\u4f3c\uff0c\u80fd\u6a21\u62df\u7ec6\u80de\u819c\u53cc\u5c42\u73af\u5883\uff0c\u9002\u7528\u4e8e\u819c\u86cb\u767d\u76f8\u4e92\u4f5c\u7528\u3001\u8102\u7b4f\u5f62\u6210\u53ca\u8de8\u819c\u8f6c\u8fd0\u673a\u5236\u7814\u7a76\u3002\u6c18\u6807\u8bb0\u7279\u6027\u4f7f\u5176\u6210\u4e3aFTIR\u3001\u8d28\u8c31\u7b49\u5206\u6790\u6280\u672f\u7684\u7406\u60f3\u5185\u6807\u7269\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n3.1 \u751f\u7269\u7269\u7406\u7814\u7a76\uff1a\u7528\u4e8e\u6784\u5efa\u6c18\u4ee3\u8102\u8d28\u4f53\uff0c\u901a\u8fc7\u4e2d\u5b50\u6563\u5c04\u6216\u56fa\u6001NMR\u89e3\u6790\u819c\u7ed3\u6784\u52a8\u529b\u5b66
\n3.2 \u836f\u7269\u5f00\u53d1\uff1a\u4f5c\u4e3a\u8f7d\u4f53\u6750\u6599\u7814\u7a76\u8102\u8d28\u7eb3\u7c73\u9897\u7c92\uff08LNP\uff09\u7684\u5305\u5c01\u7387\u4e0e\u91ca\u653e\u7279\u6027
\n3.3 \u4ee3\u8c22\u8ffd\u8e2a\uff1a\u6c18\u6807\u8bb0\u53ef\u5b9e\u73b0\u8102\u8d28\u4ee3\u8c22\u9014\u5f84\u7684\u7a33\u5b9a\u540c\u4f4d\u7d20\u793a\u8e2a
\n3.4 \u5206\u6790\u6807\u51c6\u54c1\uff1a\u4f5c\u4e3aLC-MS\/MS\u5b9a\u91cf\u5206\u6790\u78f7\u8102\u4ee3\u8c22\u7269\u7684\u53c2\u6bd4\u7269\u8d28 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u50a8\u5b58\u4e8e-20\u2103\u907f\u5149\u5e72\u71e5\u73af\u5883\uff0c\u5f00\u5c01\u540e\u9700\u5145\u60f0\u6027\u6c14\u4f53\u5bc6\u5c01\u4fdd\u5b58\u3002\u5efa\u8bae\u6eb6\u89e3\u65f6\u5148\u4ee5\u6c2f\u4eff\u9884\u6eb6\uff0c\u518d\u7528\u7f13\u51b2\u6db2\u7a00\u91ca\u3002\u5de5\u4f5c\u6d53\u5ea6\u9700\u6839\u636e\u5b9e\u9a8c\u4f53\u7cfb\u4f18\u5316\uff0c\u5178\u578b\u4f7f\u7528\u6d53\u5ea6\u4e3a10-100 \u03bcM\u3002\u907f\u514d\u53cd\u590d\u51bb\u878d\uff0c\u6eb6\u6db2\u72b6\u6001\u5efa\u8bae\u73b0\u914d\u73b0\u7528\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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