3-(3,5-\u53cc(\u4e09\u6c1f\u7532\u57fa)\u82ef\u57fa)-1H-1,2,4-\u4e09\u5511\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u4e3a\u542b\u6c1f\u82b3\u9999\u65cf\u4e09\u5511\u7c7b\u5316\u5408\u7269\uff0c\u5316\u5b66\u540d\u79f0\u4e3a3-(3,5-\u53cc(\u4e09\u6c1f\u7532\u57fa)\u82ef\u57fa)-1H-1,2,4-\u4e09\u5511\uff0cCAS\u53f7\u4e3a1333154-10-1\u3002\u5176\u5206\u5b50\u5f0f\u4e3aC10H5F6N3\uff0c\u5206\u5b50\u91cf281.157\uff0c\u7eaf\u5ea6\u9ad8\u4e8e96%\u3002\u8be5\u5316\u5408\u7269\u5177\u6709\u663e\u8457\u7684\u758f\u6c34\u6027\u548c\u7535\u5b50\u6548\u5e94\uff0c\u4e09\u6c1f\u7532\u57fa\u7684\u5f3a\u5438\u7535\u5b50\u7279\u6027\u4f7f\u5176\u5728\u82b3\u9999\u73af\u4e0a\u5f62\u6210\u9ad8\u53cd\u5e94\u6d3b\u6027\u4f4d\u70b9\uff0c\u800c1,2,4-\u4e09\u5511\u57fa\u56e2\u5219\u8d4b\u4e88\u5176\u914d\u4f4d\u80fd\u529b\u548c\u751f\u7269\u6d3b\u6027\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u4e09\u5511\u7c7b\u884d\u751f\u7269\uff0c\u8be5\u5316\u5408\u7269\u53ef\u901a\u8fc7\u6c22\u952e\u548c\u03c0-\u03c0\u5806\u79ef\u4f5c\u7528\u4e0e\u751f\u7269\u5206\u5b50\u76f8\u4e92\u4f5c\u7528\u3002\u5176\u7ed3\u6784\u4e2d\u7684\u4e09\u5511\u73af\u53ef\u4f5c\u4e3a\u91d1\u5c5e\u79bb\u5b50\u87af\u5408\u5242\u6216\u9176\u6291\u5236\u5242\u7684\u6838\u5fc3\u9aa8\u67b6\uff0c\u4e09\u6c1f\u7532\u57fa\u82ef\u57fa\u5219\u80fd\u589e\u5f3a\u7ec6\u80de\u819c\u7a7f\u900f\u6027\u3002\u8fd9\u7c7b\u7ed3\u6784\u5728\u836f\u7269\u5316\u5b66\u4e2d\u5e38\u7528\u4e8e\u8bbe\u8ba1\u6297\u771f\u83cc\u3001\u6297\u80bf\u7624\u53ca\u6297\u708e\u9776\u5411\u5206\u5b50\uff0c\u4e5f\u662f\u6709\u673a\u5408\u6210\u4e2d\u91cd\u8981\u7684\u4e2d\u95f4\u4f53\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u5728\u533b\u836f\u7814\u53d1\u9886\u57df\uff0c\u672c\u54c1\u53ef\u7528\u4e8e\u6fc0\u9176\u6291\u5236\u5242\u6216G\u86cb\u767d\u5076\u8054\u53d7\u4f53\u8c03\u8282\u5242\u7684\u5148\u5bfc\u5316\u5408\u7269\u4f18\u5316\u3002\u6750\u6599\u79d1\u5b66\u4e2d\uff0c\u5176\u542b\u6c1f\u7279\u6027\u53ef\u7528\u4e8e\u5236\u5907\u6db2\u6676\u6750\u6599\u6216\u8010\u9ad8\u6e29\u805a\u5408\u7269\u5355\u4f53\u3002\u6b64\u5916\uff0c\u5728\u519c\u7528\u5316\u5b66\u54c1\u5f00\u53d1\u4e2d\uff0c\u53ef\u4f5c\u4e3a\u6740\u83cc\u5242\u6216\u6740\u866b\u5242\u7684\u6d3b\u6027\u7ec4\u5206\u524d\u4f53\u3002\u5b9e\u9a8c\u5ba4\u4e2d\u5e38\u7528\u4e8e\u7814\u7a76\u542b\u6c1f\u82b3\u73af\u4e0e\u6742\u73af\u7684\u534f\u540c\u6548\u5e94\u673a\u5236\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u3001\u907f\u5149\u3001\u5e72\u71e5\u60f0\u6027\u6c14\u4f53\u73af\u5883\u4e0b\u957f\u671f\u50a8\u5b58\uff0c\u5f00\u5c01\u540e\u9700\u5145\u6c29\u6c14\u5bc6\u5c01\u3002\u4f7f\u7528\u524d\u9700\u6062\u590d\u81f3\u5ba4\u6e29\u4ee5\u907f\u514d\u7ed3\u9732\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u8868\u660e\u5176\u5728DMSO\u548cDMF\u4e2d\u6eb6\u89e3\u5ea6\u826f\u597d\uff08>50 mg\/mL\uff09\uff0c\u6c34\u6eb6\u6027\u4f4e\uff08<0.1 mg\/mL\uff09\u3002\u5b9e\u9a8c\u64cd\u4f5c\u5efa\u8bae\u5728\u901a\u98ce\u6a71\u4e2d\u8fdb\u884c\uff0c\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u76ae\u80a4\u6216\u5438\u5165\u7c89\u5c18\u3002 \n\n5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f \n\u672c\u4ea7\u54c1\u7ecfHPLC\u5f52\u4e00\u5316\u6cd5\u68c0\u6d4b\u7eaf\u5ea6\u226596%\uff0c\u6838\u78c1\u5171\u632f\uff081H NMR\u300119F NMR\uff09\u548c\u8d28\u8c31\uff08HRMS\uff09\u9a8c\u8bc1\u7ed3\u6784\u3002\u5b89\u5168\u6570\u636e\u8868\u660e\u5176\u6025\u6027\u6bd2\u6027\uff08LD50\u5927\u9f20\u53e3\u670d\uff09>500 mg\/kg\uff0c\u4f46\u53ef\u80fd\u5bf9\u773c\u775b\u548c\u547c\u5438\u9053\u4ea7\u751f\u523a\u6fc0\u3002\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u62a4\u76ee\u955c\u3001\u9632\u5c18\u53e3\u7f69\u53ca\u4e01\u8148\u624b\u5957\uff0c\u6ea2\u51fa\u5904\u7406\u5e94\u4f7f\u7528\u60f0\u6027\u5438\u9644\u6750\u6599\u3002\u5e9f\u5f03\u7269\u9700\u6309\u5371\u9669\u5316\u5b66\u54c1\u89c4\u8303\u5904\u7f6e\u3002 <\/p>\n
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