1-Boc-4-\u7532\u57fa-\u54cc\u5576\u7532\u9170\u80fa\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u5316\u5b66\u540d\u79f0\u4e3atert-butyl 4-carbamoyl-4-methylpiperidine-1-carboxylate\uff08CAS\u53f7\uff1a343788-67-0\uff09\uff0c\u4e2d\u6587\u547d\u540d\u4e3a1-Boc-4-\u7532\u57fa-\u54cc\u5576\u7532\u9170\u80fa\uff0c\u662f\u4e00\u79cd\u9ad8\u7eaf\u5ea6\u6709\u673a\u5408\u6210\u4e2d\u95f4\u4f53\u3002\u5176\u5206\u5b50\u5f0f\u4e3aC12H22N2O3\uff0c\u5206\u5b50\u91cf\u4e3a242.315\uff0c\u5916\u89c2\u901a\u5e38\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\u3002\u8be5\u5316\u5408\u7269\u5728Boc\uff08\u53d4\u4e01\u6c27\u7fb0\u57fa\uff09\u4fdd\u62a4\u57fa\u548c\u9170\u80fa\u57fa\u56e2\u7684\u5171\u540c\u4f5c\u7528\u4e0b\uff0c\u8868\u73b0\u51fa\u826f\u597d\u7684\u5316\u5b66\u7a33\u5b9a\u6027\uff0c\u53ef\u6eb6\u4e8e\u5e38\u89c1\u6709\u673a\u6eb6\u5242\u5982\u4e8c\u6c2f\u7532\u70f7\u3001DMF\u548cTHF\uff0c\u4f46\u5728\u6c34\u4e2d\u6eb6\u89e3\u5ea6\u8f83\u4f4e\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u54cc\u5576\u7c7b\u884d\u751f\u7269\uff0c\u8be5\u5206\u5b50\u5728\u836f\u7269\u5316\u5b66\u4e2d\u5177\u6709\u5173\u952e\u4f5c\u7528\u3002Boc\u4fdd\u62a4\u57fa\u53ef\u9009\u62e9\u6027\u8131\u9664\uff0c\u4e3a\u540e\u7eed\u5b98\u80fd\u56e2\u4fee\u9970\u63d0\u4f9b\u4fbf\u5229\uff1b\u800c4\u4f4d\u7532\u57fa\u548c\u7532\u9170\u80fa\u7ed3\u6784\u80fd\u663e\u8457\u5f71\u54cd\u5206\u5b50\u7684\u7a7a\u95f4\u6784\u8c61\u548c\u6c22\u952e\u7ed3\u5408\u80fd\u529b\uff0c\u4f7f\u5176\u6210\u4e3a\u6784\u5efa\u6fc0\u9176\u6291\u5236\u5242\u3001\u795e\u7ecf\u9012\u8d28\u8c03\u8282\u5242\u7b49\u6d3b\u6027\u5206\u5b50\u7684\u91cd\u8981\u9aa8\u67b6\u3002\u5176\u9ad8\u7eaf\u5ea6\u7279\u6027\uff08>96%\uff09\u786e\u4fdd\u4e86\u53cd\u5e94\u7684\u53ef\u91cd\u590d\u6027\u548c\u4ea7\u7269\u6536\u7387\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u5e7f\u6cdb\u5e94\u7528\u4e8e\u533b\u836f\u7814\u53d1\u548c\u7cbe\u7ec6\u5316\u5de5\u9886\u57df\uff0c\u5177\u4f53\u5305\u62ec\uff1a1\uff09\u4f5c\u4e3a\u6297\u80bf\u7624\u836f\u7269\uff08\u5982PARP\u6291\u5236\u5242\uff09\u5408\u6210\u4e2d\u7684\u5173\u952e\u4e2d\u95f4\u4f53\uff1b2\uff09\u7528\u4e8e\u6784\u5efa\u4e2d\u67a2\u795e\u7ecf\u7cfb\u7edf\u836f\u7269\uff08\u5982\u9547\u75db\u5242\u6216\u6297\u6291\u90c1\u5242\uff09\u7684\u54cc\u5576\u73af\u7ed3\u6784\uff1b3\uff09\u5728\u4e0d\u5bf9\u79f0\u50ac\u5316\u53cd\u5e94\u4e2d\u4f5c\u4e3a\u624b\u6027\u914d\u4f53\u7684\u524d\u4f53\u3002\u5b9e\u9a8c\u8868\u660e\uff0c\u5176\u884d\u751f\u7269\u53ef\u663e\u8457\u589e\u5f3a\u9776\u6807\u86cb\u767d\u7684\u7ed3\u5408\u4eb2\u548c\u529b\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u81f34\u00b0C\u7684\u5e72\u71e5\u73af\u5883\u4e2d\u907f\u5149\u4fdd\u5b58\uff0c\u957f\u671f\u50a8\u5b58\u9700\u5145\u5165\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u3002\u5f00\u5c01\u540e\u5e94\u907f\u514d\u53cd\u590d\u51bb\u878d\uff0c\u5efa\u8bae\u5206\u88c5\u4f7f\u7528\u3002\u5b9e\u9a8c\u64cd\u4f5c\u65f6\u9700\u5728\u901a\u98ce\u6a71\u4e2d\u8fdb\u884c\uff0c\u4f69\u6234\u9632\u62a4\u624b\u5957\u548c\u62a4\u76ee\u955c\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u63a8\u8350\u5148\u4ee5\u5c11\u91cfDMSO\u52a9\u6eb6\uff0c\u518d\u7a00\u91ca\u81f3\u76ee\u6807\u6eb6\u5242\u4f53\u7cfb\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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