7-\u6eb4\u55b9\u5511\u5549-4(3H)-\u916e\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n7-\u6eb4\u55b9\u5511\u5549-4(3H)-\u916e\uff087-bromo-1h-quinazolin-4-one\uff09\u662f\u4e00\u79cd\u542b\u6eb4\u53d6\u4ee3\u57fa\u7684\u55b9\u5511\u5549\u916e\u7c7b\u5316\u5408\u7269\uff0c\u5316\u5b66\u5f0f\u4e3aC8H5BrN2O\uff0c\u5206\u5b50\u91cf225.042\uff0cCAS\u767b\u8bb0\u53f7194851-16-6\u3002\u8be5\u5316\u5408\u7269\u4e3a\u767d\u8272\u81f3\u6de1\u9ec4\u8272\u7ed3\u6676\u6027\u7c89\u672b\uff0c\u7eaf\u5ea6\u9ad8\u4e8e96%\uff0c\u5177\u6709\u5178\u578b\u7684\u55b9\u5511\u5549\u916e\u9aa8\u67b6\u7ed3\u6784\uff0c\u5176\u6eb4\u539f\u5b50\u53d6\u4ee3\u4f4d\u70b9\uff08C-7\uff09\u8d4b\u4e88\u5206\u5b50\u72ec\u7279\u7684\u53cd\u5e94\u6d3b\u6027\uff0c\u9002\u7528\u4e8e\u8fdb\u4e00\u6b65\u5b98\u80fd\u56e2\u5316\u4fee\u9970\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u55b9\u5511\u5549\u916e\u884d\u751f\u7269\uff0c\u8be5\u5316\u5408\u7269\u662f\u6784\u5efa\u590d\u6742\u751f\u7269\u6d3b\u6027\u5206\u5b50\u7684\u5173\u952e\u4e2d\u95f4\u4f53\u3002\u55b9\u5511\u5549\u916e\u7c7b\u7ed3\u6784\u5e7f\u6cdb\u5b58\u5728\u4e8e\u836f\u7269\u5206\u5b50\u4e2d\uff0c\u5177\u6709\u6297\u83cc\u3001\u6297\u80bf\u7624\u53ca\u6fc0\u9176\u6291\u5236\u7b49\u6f5c\u529b\u30027-\u4f4d\u6eb4\u539f\u5b50\u7684\u5f15\u5165\u53ef\u589e\u5f3a\u5206\u5b50\u4eb2\u7535\u6027\uff0c\u4fbf\u4e8e\u901a\u8fc7\u5076\u8054\u53cd\u5e94\uff08\u5982Suzuki\u3001Buchwald-Hartwig\u53cd\u5e94\uff09\u5f15\u5165\u82b3\u57fa\u6216\u6742\u73af\u57fa\u56e2\uff0c\u662f\u5f00\u53d1\u65b0\u578bEGFR\u6291\u5236\u5242\u6216PARP\u62ee\u6297\u5242\u7684\u91cd\u8981\u524d\u4f53\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u533b\u836f\u7814\u53d1\u548c\u6709\u673a\u5408\u6210\u9886\u57df\u3002\u5728\u836f\u7269\u5316\u5b66\u4e2d\uff0c\u53ef\u4f5c\u4e3a\u5148\u5bfc\u5316\u5408\u7269\u4f18\u5316\u4e2d\u7684\u6838\u5fc3\u9aa8\u67b6\uff0c\u7528\u4e8e\u6297\u80bf\u7624\u6216\u6297\u708e\u836f\u7269\u7684\u7ed3\u6784\u4fee\u9970\u3002\u5728\u6750\u6599\u79d1\u5b66\u4e2d\uff0c\u5176\u521a\u6027\u5e73\u9762\u7ed3\u6784\u53ef\u7528\u4e8e\u5236\u5907\u8367\u5149\u63a2\u9488\u6216\u5149\u7535\u6750\u6599\u3002\u5177\u4f53\u5b9e\u9a8c\u7528\u9014\u5305\u62ec\uff1a\u6fc0\u9176\u6291\u5236\u5242\u5e93\u6784\u5efa\u3001DNA\u635f\u4f24\u4fee\u590d\u673a\u5236\u7814\u7a76\uff0c\u4ee5\u53ca\u4f5c\u4e3aHPLC\u6807\u51c6\u54c1\u7528\u4e8e\u5206\u6790\u65b9\u6cd5\u5f00\u53d1\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5bc6\u5c01\u4fdd\u5b58\u4e8e-20\u2103\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u907f\u514d\u5149\u7167\u53ca\u6f6e\u6e7f\u3002\u5f00\u5c01\u540e\u9700\u5145\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u4ee5\u5ef6\u957f\u7a33\u5b9a\u6027\u3002\u4f7f\u7528\u524d\u9700\u6062\u590d\u81f3\u5ba4\u6e29\u5e76\u77ed\u6682\u79bb\u5fc3\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u8868\u660e\uff0c\u8be5\u5316\u5408\u7269\u6613\u6eb6\u4e8eDMSO\uff0850 mg\/mL\uff09\uff0c\u5fae\u6eb6\u4e8e\u7532\u9187\uff0c\u4e0d\u6eb6\u4e8e\u6c34\u3002\u5b9e\u9a8c\u64cd\u4f5c\u5efa\u8bae\u5728\u901a\u98ce\u6a71\u4e2d\u8fdb\u884c\uff0c\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u76ae\u80a4\u6216\u5438\u5165\u7c89\u5c18\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u7ecfHPLC\u9a8c\u8bc1\u7eaf\u5ea6\uff1e96%\uff0c\u6838\u78c1\u5171\u632f\uff081H NMR\uff09\u53ca\u8d28\u8c31\uff08MS\uff09\u786e\u8ba4\u7ed3\u6784\u3002\u5b89\u5168\u6570\u636e\u8868\u660e\uff0c\u8be5\u5316\u5408\u7269\u53ef\u80fd\u5f15\u8d77\u773c\u775b\u548c\u76ae\u80a4\u523a\u6fc0\uff0c\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u9632\u62a4\u773c\u955c\u53ca\u4e01\u8148\u624b\u5957\u3002\u5982\u610f\u5916\u63a5\u89e6\uff0c\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5904\u7f6e\u9700\u7b26\u5408\u5f53\u5730\u5371\u9669\u5316\u5b66\u54c1\u7ba1\u7406\u6cd5\u89c4\uff0c\u7981\u6b62\u76f4\u63a5\u6392\u5165\u4e0b\u6c34\u9053\u3002 <\/p>\n
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