1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u4e3amethyl (+\/-)-(3aR)-2-(phenylmethyl)hexahydrocyclopenta[c]pyrrole-3a(1H)-carboxylate\uff0c\u5316\u5b66\u5f0f\u4e3aC16H21NO2\uff0c\u5206\u5b50\u91cf259.343\uff0cCAS\u53f7\u4e3a885958-43-0\u3002\u8be5\u5316\u5408\u7269\u662f\u4e00\u79cd\u5177\u6709\u7279\u5b9a\u7acb\u4f53\u6784\u578b\u7684\u6742\u73af\u884d\u751f\u7269\uff0c\u7eaf\u5ea6\u9ad8\u4e8e96%\uff0c\u5916\u89c2\u901a\u5e38\u4e3a\u65e0\u8272\u81f3\u6de1\u9ec4\u8272\u6db2\u4f53\u6216\u56fa\u4f53\u3002\u5176\u7ed3\u6784\u5305\u542b\u82ef\u7532\u57fa\u548c\u516d\u6c22\u73af\u620a\u5e76[c]\u5421\u54af\u73af\uff0c\u7fa7\u9178\u7532\u916f\u57fa\u56e2\u8d4b\u4e88\u5176\u826f\u597d\u7684\u6eb6\u89e3\u6027\u548c\u53cd\u5e94\u6d3b\u6027\uff0c\u9002\u7528\u4e8e\u6709\u673a\u5408\u6210\u53ca\u836f\u7269\u5316\u5b66\u7814\u7a76\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u4f5c\u4e3a\u624b\u6027\u4e2d\u95f4\u4f53\uff0c\u5728\u751f\u7269\u6d3b\u6027\u5206\u5b50\u6784\u5efa\u4e2d\u5177\u6709\u91cd\u8981\u4f5c\u7528\u3002\u5176\u73af\u620a\u5e76\u5421\u54af\u9aa8\u67b6\u5e38\u89c1\u4e8e\u591a\u79cd\u5929\u7136\u4ea7\u7269\u548c\u836f\u7269\u5206\u5b50\u4e2d\uff0c\u80fd\u591f\u53c2\u4e0e\u7acb\u4f53\u9009\u62e9\u6027\u5408\u6210\uff0c\u5c24\u5176\u9002\u7528\u4e8e\u795e\u7ecf\u6d3b\u6027\u5316\u5408\u7269\u6216\u9176\u6291\u5236\u5242\u7684\u7814\u53d1\u3002\u82ef\u7532\u57fa\u7684\u5f15\u5165\u53ef\u8c03\u8282\u8102\u6eb6\u6027\u548c\u9776\u6807\u7ed3\u5408\u80fd\u529b\uff0c\u4f7f\u5176\u5728\u836f\u7269\u5148\u5bfc\u7269\u4f18\u5316\u4e2d\u5177\u6709\u6f5c\u5728\u4ef7\u503c\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u533b\u836f\u7814\u53d1\u548c\u7cbe\u7ec6\u5316\u5de5\u9886\u57df\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a\u4f5c\u4e3a\u624b\u6027\u780c\u5757\u7528\u4e8e\u4e0d\u5bf9\u79f0\u5408\u6210\uff1b\u53c2\u4e0e\u591a\u80bd\u6a21\u62df\u7269\u7684\u6784\u5efa\uff1b\u7528\u4e8e\u5f00\u53d1G\u86cb\u767d\u5076\u8054\u53d7\u4f53\uff08GPCR\uff09\u8c03\u8282\u5242\u6216\u4e2d\u67a2\u795e\u7ecf\u7cfb\u7edf\u836f\u7269\u3002\u6b64\u5916\uff0c\u5728\u50ac\u5316\u53cd\u5e94\u4e2d\u53ef\u4f5c\u4e3a\u914d\u4f53\u524d\u4f53\u6216\u8f85\u52a9\u5242\uff0c\u63d0\u5347\u53cd\u5e94\u6548\u7387\u548c\u9009\u62e9\u6027\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u4e0b\u907f\u5149\u5bc6\u5c01\u4fdd\u5b58\uff0c\u957f\u671f\u50a8\u5b58\u9700\u5145\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u3002\u5f00\u5c01\u540e\u5e94\u5c3d\u5feb\u4f7f\u7528\uff0c\u907f\u514d\u53cd\u590d\u51bb\u878d\u6216\u66b4\u9732\u4e8e\u6f6e\u6e7f\u73af\u5883\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u60f0\u6027\u6c14\u6c1b\uff08\u5982\u6c2e\u6c14\uff09\u4e0b\u64cd\u4f5c\uff0c\u6eb6\u4e8e\u4e8c\u6c2f\u7532\u70f7\u6216THF\u7b49\u6709\u673a\u6eb6\u5242\u524d\u9700\u5145\u5206\u5e73\u8861\u81f3\u5ba4\u6e29\u3002\u5b9e\u9a8c\u4eba\u5458\u5e94\u4f69\u6234\u9632\u62a4\u624b\u5957\u53ca\u62a4\u76ee\u955c\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u54c1\u901a\u8fc7HPLC\u548cNMR\u4e25\u683c\u68c0\u6d4b\uff0c\u786e\u4fdd\u7eaf\u5ea6>96%\u3002\u5b89\u5168\u6570\u636e\u8868\u660e\uff0c\u8be5\u5316\u5408\u7269\u53ef\u80fd\u5bf9\u773c\u775b\u548c\u76ae\u80a4\u6709\u523a\u6fc0\u6027\uff0c\u64cd\u4f5c\u65f6\u9700\u5728\u901a\u98ce\u6a71\u4e2d\u8fdb\u884c\u3002\u82e5\u4e0d\u614e\u63a5\u89e6\uff0c\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5e94\u4f5c\u4e3a\u6709\u5bb3\u5316\u5b66\u54c1\u5904\u7406\uff0c\u9075\u5b88\u5f53\u5730\u73af\u4fdd\u6cd5\u89c4\u3002\u8fd0\u8f93\u65f6\u5f52\u7c7b\u4e3a\u975e\u5371\u9669\u54c1\uff0c\u4f46\u9700\u907f\u514d\u9ad8\u6e29\u548c\u5267\u70c8\u9707\u52a8\u3002 <\/p>\n
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