2-\u6c28\u57fa-5-[2-(1,1,1,2,3,3,3-\u4e03\u6c18\u4ee3\u4e19-2-\u57fa\u6c28\u57fa)-1-\u7f9f\u57fa\u4e59\u57fa]\u82ef\u7532\u8148\uff08\u6c18\u4ee3\u897f\u9a6c\u7279\u7f57\uff09\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u4e3a\u6c18\u4ee3\u897f\u9a6c\u7279\u7f57\u7684\u7a33\u5b9a\u540c\u4f4d\u7d20\u6807\u8bb0\u5316\u5408\u7269\uff0c\u5316\u5b66\u540d\u79f0\u5982\u6807\u9898\u6240\u793a\uff0cCAS\u53f7\u4e3a1228182-44-2\uff0c\u5206\u5b50\u5f0f\u4e3aC12H10D7N3O\uff0c\u5206\u5b50\u91cf226.326\u3002\u5176\u7ed3\u6784\u5728\u5929\u7136\u897f\u9a6c\u7279\u7f57\u57fa\u7840\u4e0a\u5f15\u51657\u4e2a\u6c18\u539f\u5b50\uff0c\u663e\u8457\u63d0\u9ad8\u4ee3\u8c22\u7a33\u5b9a\u6027\uff0c\u540c\u65f6\u4fdd\u7559\u539f\u5316\u5408\u7269\u7684\u751f\u7269\u6d3b\u6027\u3002\u5e38\u6e29\u4e0b\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u7c89\u672b\uff0c\u7eaf\u5ea6\u7ecfHPLC\u9a8c\u8bc1\u5927\u4e8e96%\uff0c\u7b26\u5408\u540c\u4f4d\u7d20\u6807\u8bb0\u8bd5\u5242\u7684\u56fd\u9645\u6807\u51c6\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u6c18\u4ee3\u897f\u9a6c\u7279\u7f57\u4f5c\u4e3a\u03b22-\u80be\u4e0a\u817a\u7d20\u53d7\u4f53\u6fc0\u52a8\u5242\u7684\u6c18\u4ee3\u884d\u751f\u7269\uff0c\u901a\u8fc7\u9009\u62e9\u6027\u6fc0\u6d3b\u547c\u5438\u9053\u5e73\u6ed1\u808c\u53d7\u4f53\u53d1\u6325\u652f\u6c14\u7ba1\u6269\u5f20\u4f5c\u7528\u3002\u6c18\u539f\u5b50\u53d6\u4ee3\u663e\u8457\u964d\u4f4e\u78b3-\u6c18\u952e\u65ad\u88c2\u901f\u7387\uff0c\u5ef6\u957f\u836f\u7269\u534a\u8870\u671f\u5e76\u51cf\u5c11\u4ee3\u8c22\u4ea7\u7269\u5e72\u6270\uff0c\u4f7f\u5176\u6210\u4e3a\u836f\u7269\u4ee3\u8c22\u7814\u7a76\uff08DMPK\uff09\u548c\u5b9a\u91cf\u8d28\u8c31\u5206\u6790\u4e2d\u7684\u5173\u952e\u5185\u6807\u7269\u8d28\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a
\n3.1 \u836f\u7269\u7814\u53d1\uff1a\u4f5c\u4e3a\u897f\u9a6c\u7279\u7f57\u53ca\u5176\u7c7b\u4f3c\u7269\u7684\u540c\u4f4d\u7d20\u5185\u6807\uff0c\u7528\u4e8eLC-MS\/MS\u6cd5\u8fdb\u884c\u836f\u4ee3\u52a8\u529b\u5b66\u7814\u7a76\u3002
\n3.2 \u5174\u594b\u5242\u68c0\u6d4b\uff1a\u4f53\u80b2\u7ade\u6280\u4e2d\u03b22-\u6fc0\u52a8\u5242\u6ee5\u7528\u7684\u68c0\u6d4b\u65b9\u6cd5\u5f00\u53d1\u4e0e\u9a8c\u8bc1\u3002
\n3.3 \u4ee3\u8c22\u901a\u8def\u7814\u7a76\uff1a\u901a\u8fc7\u8ffd\u8e2a\u6c18\u6807\u8bb0\u4f4d\u7f6e\u89e3\u6790\u836f\u7269\u4ee3\u8c22\u9176\u7684\u4f5c\u7528\u673a\u5236\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n4.1 \u50a8\u5b58\u6761\u4ef6\uff1a\u5efa\u8bae-20\u2103\u907f\u5149\u4fdd\u5b58\u4e8e\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u5f00\u5c01\u540e\u9700\u5145\u60f0\u6027\u6c14\u4f53\u5bc6\u5c01\u3002
\n4.2 \u6eb6\u89e3\u6027\uff1a\u6613\u6eb6\u4e8eDMSO\uff0850mg\/mL\uff09\uff0c\u7532\u9187\u4e2d\u6eb6\u89e3\u5ea6\u7ea6\u4e3a10mg\/mL\uff0c\u6c34\u6eb6\u6027\u8f83\u5dee\u3002
\n4.3 \u4f7f\u7528\u6ce8\u610f\uff1a\u914d\u5236\u5de5\u4f5c\u6db2\u65f6\u9700\u91c7\u7528\u73bb\u7483\u5bb9\u5668\u4ee5\u51cf\u5c11\u5438\u9644\uff0c\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n5.1 \u8d28\u91cf\u63a7\u5236\uff1a\u6bcf\u6279\u6b21\u63d0\u4f9bCOA\u62a5\u544a\uff0c\u5305\u542bHPLC\u7eaf\u5ea6\u3001\u540c\u4f4d\u7d20\u4e30\u5ea6\uff08\u226599% D\uff09\u3001\u6c34\u5206\u53ca\u6b8b\u7559\u6eb6\u5242\u6570\u636e\u3002
\n5.2 \u5b89\u5168\u8b66\u793a\uff1a\u672c\u54c1\u5c5e\u4e8e\u5371\u9669\u5316\u5b66\u54c1\uff0c\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u9632\u62a4\u88c5\u5907\uff0c\u907f\u514d\u5438\u5165\u6216\u76ae\u80a4\u63a5\u89e6\u3002
\n5.3 \u5904\u7f6e\u65b9\u6cd5\uff1a\u5e9f\u5f03\u7269\u6599\u5e94\u4f5c\u4e3a\u6709\u5bb3\u5e9f\u7269\u5904\u7406\uff0c\u7b26\u5408\u5f53\u5730\u73af\u4fdd\u6cd5\u89c4\u3002 <\/p>\n
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