1-(Azetidin-3-yl)-4,4-difluoropiperidine\u4ea7\u54c1\u8bf4\u660e\u4e66<\/p>\n
\u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n1-(Azetidin-3-yl)-4,4-difluoropiperidine\u662f\u4e00\u79cd\u542b\u6c2e\u6742\u73af\u5316\u5408\u7269\uff0cCAS\u53f7\u4e3a1257293-83-6\uff0c\u5206\u5b50\u5f0f\u4e3aC8H14F2N2\uff0c\u5206\u5b50\u91cf\u4e3a176.207\u3002\u8be5\u5316\u5408\u7269\u7531\u54cc\u5576\u73af\u548c\u6c2e\u6742\u73af\u4e01\u70f7\u7ed3\u6784\u5355\u5143\u7ec4\u6210\uff0c\u5176\u4e2d\u54cc\u5576\u73af\u76844\u4f4d\u88ab\u4e24\u4e2a\u6c1f\u539f\u5b50\u53d6\u4ee3\uff0c\u5f62\u6210\u72ec\u7279\u76844,4-\u4e8c\u6c1f\u54cc\u5576\u7ed3\u6784\u3002\u4ea7\u54c1\u7eaf\u5ea6\u7ecfHPLC\u9a8c\u8bc1\u5927\u4e8e96%\uff0c\u5448\u65e0\u8272\u81f3\u6de1\u9ec4\u8272\u6db2\u4f53\uff0c\u5177\u6709\u78b1\u6027\u7279\u5f81\uff0c\u6613\u6eb6\u4e8e\u5e38\u89c1\u6709\u673a\u6eb6\u5242\u5982\u7532\u9187\u3001\u4e59\u8148\u548c\u4e8c\u6c2f\u7532\u70f7\u3002<\/p>\n
\u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u4f5c\u4e3a\u91cd\u8981\u7684\u533b\u836f\u4e2d\u95f4\u4f53\uff0c\u5176\u5206\u5b50\u7ed3\u6784\u4e2d\u7684\u6c2e\u6742\u73af\u4e01\u70f7\u548c4,4-\u4e8c\u6c1f\u54cc\u5576\u57fa\u56e2\u4f7f\u5176\u5177\u6709\u7279\u6b8a\u7684\u7a7a\u95f4\u6784\u578b\u548c\u7535\u5b50\u6548\u5e94\u3002\u4e8c\u6c1f\u53d6\u4ee3\u53ef\u663e\u8457\u6539\u53d8\u5206\u5b50\u7684\u8102\u6eb6\u6027\u548c\u4ee3\u8c22\u7a33\u5b9a\u6027\uff0c\u800c\u6c2e\u6742\u73af\u4e01\u70f7\u5219\u63d0\u4f9b\u4e86\u826f\u597d\u7684\u6c22\u952e\u53d7\u4f53\u7279\u6027\u3002\u8fd9\u4e9b\u7ed3\u6784\u7279\u70b9\u4f7f\u5176\u5728\u836f\u7269\u8bbe\u8ba1\u4e2d\u53ef\u7528\u4e8e\u8c03\u8282\u5206\u5b50\u7684\u751f\u7269\u6d3b\u6027\u3001\u6539\u5584\u836f\u4ee3\u52a8\u529b\u5b66\u6027\u8d28\uff0c\u5e76\u589e\u5f3a\u4e0e\u9776\u6807\u86cb\u767d\u7684\u76f8\u4e92\u4f5c\u7528\u80fd\u529b\u3002<\/p>\n
\u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n1. \u533b\u836f\u7814\u53d1\u9886\u57df\uff1a\u4f5c\u4e3a\u5173\u952e\u4e2d\u95f4\u4f53\u7528\u4e8e\u5408\u6210\u591a\u79cd\u751f\u7269\u6d3b\u6027\u5206\u5b50\uff0c\u7279\u522b\u662f\u4e2d\u67a2\u795e\u7ecf\u7cfb\u7edf\u836f\u7269\u548c\u6297\u611f\u67d3\u836f\u7269\u7684\u5f00\u53d1\u3002
\n2. \u836f\u7269\u5316\u5b66\u7814\u7a76\uff1a\u7528\u4e8e\u6784\u6548\u5173\u7cfb\u7814\u7a76\uff0c\u63a2\u7d22\u6c1f\u539f\u5b50\u53d6\u4ee3\u5bf9\u836f\u7269\u6d3b\u6027\u7684\u5f71\u54cd\u3002
\n3. \u751f\u7269\u63a2\u9488\u5408\u6210\uff1a\u53ef\u4f5c\u4e3a\u6807\u8bb0\u5316\u5408\u7269\u7684\u6784\u5efa\u6a21\u5757\uff0c\u7528\u4e8e\u751f\u7269\u5206\u5b50\u76f8\u4e92\u4f5c\u7528\u7814\u7a76\u3002
\n4. \u6750\u6599\u79d1\u5b66\uff1a\u5728\u7279\u6b8a\u529f\u80fd\u6750\u6599\u5f00\u53d1\u4e2d\u4f5c\u4e3a\u542b\u6c1f\u7ed3\u6784\u5355\u5143\u4f7f\u7528\u3002<\/p>\n
\u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u672c\u4ea7\u54c1\u5e94\u5728-20\u00b0C\u4e0b\u907f\u5149\u4fdd\u5b58\uff0c\u7f6e\u4e8e\u5e72\u71e5\u3001\u60f0\u6027\u6c14\u6c1b\uff08\u5982\u6c2e\u6c14\uff09\u73af\u5883\u4e2d\u3002\u5f00\u5c01\u540e\u5efa\u8bae\u5c3d\u5feb\u4f7f\u7528\uff0c\u672a\u7528\u5b8c\u7684\u8bd5\u5242\u5e94\u91cd\u65b0\u5bc6\u5c01\u5e76\u5145\u5165\u4fdd\u62a4\u6c14\u4f53\u3002\u4f7f\u7528\u65f6\u5e94\u5728\u901a\u98ce\u826f\u597d\u7684\u5316\u5b66\u901a\u98ce\u6a71\u4e2d\u64cd\u4f5c\uff0c\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u76ae\u80a4\u548c\u773c\u775b\u3002\u5efa\u8bae\u4f7f\u7528\u73bb\u7483\u6216\u805a\u56db\u6c1f\u4e59\u70ef\u6750\u8d28\u7684\u5bb9\u5668\u8fdb\u884c\u50a8\u5b58\u548c\u8f6c\u79fb\u3002<\/p>\n
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