\u4ea7\u54c1\u8bf4\u660e <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\nFmoc-N-Me-Asp(OtBu)-OH\uff0c\u4e2d\u6587\u540d\u79f0\u4e3aFmoc-N-\u7532\u57fa-L-\u5929\u51ac\u6c28\u9178 4-\u53d4\u4e01\u916f\uff0c\u662f\u4e00\u79cd\u91cd\u8981\u7684\u6c28\u57fa\u9178\u884d\u751f\u7269\uff0cCAS\u53f7\u4e3a152548-66-8\u3002\u5176\u5206\u5b50\u5f0f\u4e3aC24H27NO6\uff0c\u5206\u5b50\u91cf\u4e3a425.474\uff0c\u7eaf\u5ea6\u901a\u5e38\u9ad8\u4e8e96%\u3002\u8be5\u5316\u5408\u7269\u7ed3\u6784\u4e2d\u542b\u6709Fmoc\uff089-\u82b4\u7532\u6c27\u7fb0\u57fa\uff09\u4fdd\u62a4\u57fa\u56e2\u3001N-\u7532\u57fa\u5316\u4fee\u9970\u4ee5\u53ca\u5929\u51ac\u6c28\u9178\u4fa7\u94fe\u7684\u53d4\u4e01\u916f\u4fdd\u62a4\u57fa\u56e2\uff0c\u4f7f\u5176\u5728\u56fa\u76f8\u591a\u80bd\u5408\u6210\uff08SPPS\uff09\u4e2d\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u7a33\u5b9a\u6027\u548c\u53cd\u5e94\u9009\u62e9\u6027\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\nFmoc-N-Me-Asp(OtBu)-OH\u662fN-\u7532\u57fa\u5316\u6c28\u57fa\u9178\u7684\u5178\u578b\u4ee3\u8868\uff0cN-\u7532\u57fa\u5316\u4fee\u9970\u53ef\u663e\u8457\u6539\u53d8\u80bd\u94fe\u7684\u6784\u8c61\u548c\u751f\u7269\u6d3b\u6027\uff0c\u589e\u5f3a\u5176\u4ee3\u8c22\u7a33\u5b9a\u6027\u548c\u819c\u901a\u900f\u6027\u3002\u8fd9\u7c7b\u4fee\u9970\u5728\u5929\u7136\u4ea7\u7269\u548c\u836f\u7269\u8bbe\u8ba1\u4e2d\u5c24\u4e3a\u91cd\u8981\uff0c\u4f8b\u5982\u7528\u4e8e\u5f00\u53d1\u6297\u83cc\u80bd\u3001\u6297\u80bf\u7624\u80bd\u53ca\u795e\u7ecf\u6d3b\u6027\u80bd\u7b49\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u56fa\u76f8\u591a\u80bd\u5408\u6210\uff0c\u7279\u522b\u9002\u7528\u4e8e\u9700\u8981\u5f15\u5165N-\u7532\u57fa\u5316\u5929\u51ac\u6c28\u9178\u6b8b\u57fa\u7684\u80bd\u94fe\u6784\u5efa\u3002\u5176\u53d4\u4e01\u916f\u4fdd\u62a4\u57fa\u56e2\u53ef\u5728\u9178\u6027\u6761\u4ef6\u4e0b\u9009\u62e9\u6027\u8131\u9664\uff0c\u800cFmoc\u57fa\u56e2\u53ef\u901a\u8fc7\u78b1\u6027\u6761\u4ef6\uff08\u5982\u54cc\u5576\uff09\u8131\u4fdd\u62a4\uff0c\u517c\u5bb9\u6807\u51c6\u7684Fmoc\u5408\u6210\u7b56\u7565\u3002\u6b64\u5916\uff0c\u5b83\u8fd8\u5e7f\u6cdb\u5e94\u7528\u4e8e\u836f\u7269\u7814\u53d1\u3001\u751f\u7269\u63a2\u9488\u5236\u5907\u53ca\u7ed3\u6784\u751f\u7269\u5b66\u7814\u7a76\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5c06\u4ea7\u54c1\u5bc6\u5c01\u4fdd\u5b58\u4e8e-20\u00b0C\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u907f\u514d\u5149\u7167\u548c\u6f6e\u6e7f\u3002\u4f7f\u7528\u524d\u9700\u6062\u590d\u81f3\u5ba4\u6e29\u5e76\u4fdd\u6301\u5e72\u71e5\uff0c\u4ee5\u9632\u6b62\u5438\u6e7f\u964d\u89e3\u3002\u6eb6\u89e3\u65f6\u63a8\u8350\u4f7f\u7528\u6781\u6027\u6709\u673a\u6eb6\u5242\uff08\u5982DMF\u6216DCM\uff09\uff0c\u5e76\u5728\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u4e0b\u64cd\u4f5c\u4ee5\u7ef4\u6301\u7a33\u5b9a\u6027\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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