3,4-\u5417\u5549\u4e8c\u7532\u9178-3-\u4e59\u57fa-4-(1,1-\u4e8c\u7532\u57fa\u4e59\u57fa)\u916f\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u662f\u4e00\u79cd\u9ad8\u7eaf\u5ea6\u6709\u673a\u5316\u5408\u7269\uff0c\u5316\u5b66\u540d\u79f0\u4e3a3,4-\u5417\u5549\u4e8c\u7532\u9178-3-\u4e59\u57fa-4-(1,1-\u4e8c\u7532\u57fa\u4e59\u57fa)\u916f\uff0c\u4e2d\u6587\u522b\u540dN-Boc-3-\u4e59\u57fa\u5417\u5549-3-\u7532\u9178\u3002\u5176CAS\u53f7\u4e3a1205749-44-5\uff0c\u5206\u5b50\u5f0f\u4e3aC12H21NO5\uff0c\u5206\u5b50\u91cf\u4e3a259.299\u3002\u8be5\u5316\u5408\u7269\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u7c89\u672b\uff0c\u7eaf\u5ea6\u7ecf\u9ad8\u6548\u6db2\u76f8\u8272\u8c31\uff08HPLC\uff09\u9a8c\u8bc1\u5927\u4e8e96%\uff0c\u5177\u6709\u660e\u786e\u7684\u5316\u5b66\u7ed3\u6784\u548c\u7a33\u5b9a\u7684\u7406\u5316\u6027\u8d28\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u5417\u5549\u73af\u884d\u751f\u7269\uff0c\u8be5\u5316\u5408\u7269\u5728\u6709\u673a\u5408\u6210\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002\u5176\u7ed3\u6784\u4e2d\u7684Boc\u4fdd\u62a4\u57fa\uff08\u53d4\u4e01\u6c27\u7fb0\u57fa\uff09\u53ef\u9009\u62e9\u6027\u4fdd\u62a4\u6c28\u57fa\uff0c\u800c\u4e59\u57fa\u548c\u916f\u57fa\u7684\u5f15\u5165\u589e\u5f3a\u4e86\u5206\u5b50\u7684\u758f\u6c34\u6027\u548c\u53cd\u5e94\u591a\u6837\u6027\u3002\u8fd9\u7c7b\u7ed3\u6784\u5355\u5143\u5e7f\u6cdb\u5e94\u7528\u4e8e\u836f\u7269\u4e2d\u95f4\u4f53\u5408\u6210\uff0c\u5c24\u5176\u5728\u6784\u5efa\u5177\u6709\u751f\u7269\u6d3b\u6027\u7684\u6742\u73af\u5316\u5408\u7269\u65f6\u8868\u73b0\u51fa\u663e\u8457\u4f18\u52bf\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u4e3b\u8981\u5e94\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a
\n3.1 \u533b\u836f\u7814\u53d1\uff1a\u4f5c\u4e3a\u5173\u952e\u4e2d\u95f4\u4f53\u7528\u4e8e\u5408\u6210\u6297\u80bf\u7624\u3001\u6297\u75c5\u6bd2\u53ca\u4e2d\u67a2\u795e\u7ecf\u7cfb\u7edf\u836f\u7269\u3002
\n3.2 \u6750\u6599\u79d1\u5b66\uff1a\u7528\u4e8e\u5236\u5907\u529f\u80fd\u5316\u9ad8\u5206\u5b50\u6750\u6599\u7684\u5355\u4f53\u3002
\n3.3 \u5b66\u672f\u7814\u7a76\uff1a\u5728\u4e0d\u5bf9\u79f0\u5408\u6210\u3001\u50ac\u5316\u5242\u8bbe\u8ba1\u7b49\u6709\u673a\u5316\u5b66\u7814\u7a76\u4e2d\u4f5c\u4e3a\u91cd\u8981\u780c\u5757\u3002
\n\u5178\u578b\u53cd\u5e94\u5305\u62ec\u9170\u80fa\u5316\u3001\u916f\u4ea4\u6362\u53ca\u4eb2\u6838\u53d6\u4ee3\u53cd\u5e94\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u50a8\u5b58\u6761\u4ef6\uff1a\u5e94\u5bc6\u5c01\u4fdd\u5b58\u4e8e-20\u00b0C\u81f34\u00b0C\u7684\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u907f\u514d\u5149\u7167\u548c\u6f6e\u6e7f\u3002\u957f\u671f\u50a8\u5b58\u5efa\u8bae\u5145\u5165\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u3002
\n\u4f7f\u7528\u5efa\u8bae\uff1a
\n4.1 \u4f7f\u7528\u524d\u9700\u6062\u590d\u81f3\u5ba4\u6e29\u4ee5\u907f\u514d\u7ed3\u9732\u3002
\n4.2 \u5efa\u8bae\u5728\u901a\u98ce\u6a71\u4e2d\u64cd\u4f5c\uff0c\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u76ae\u80a4\u548c\u773c\u775b\u3002
\n4.3 \u6eb6\u89e3\u6027\u6d4b\u8bd5\u663e\u793a\u6613\u6eb6\u4e8e\u4e8c\u6c2f\u7532\u70f7\u3001THF\u7b49\u6709\u673a\u6eb6\u5242\uff0c\u5fae\u6eb6\u4e8e\u6c34\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u8d28\u91cf\u63a7\u5236\uff1a\u6bcf\u6279\u6b21\u4ea7\u54c1\u5747\u63d0\u4f9bHPLC\u7eaf\u5ea6\u62a5\u544a\u3001\u6838\u78c1\u5171\u632f\uff08NMR\uff09\u53ca\u8d28\u8c31\uff08MS\uff09\u8868\u5f81\u6570\u636e\u3002
\n\u5b89\u5168\u4fe1\u606f\uff1a
\n5.1 \u5b89\u5168\u6807\u8bc6\uff1aGHS\u5206\u7c7b\u4e3a\u523a\u6fc0\u6027\u7269\u8d28\uff08\u7c7b\u522b2\uff09\uff0c\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u9632\u62a4\u624b\u5957\u548c\u62a4\u76ee\u955c\u3002
\n5.2 \u5e94\u6025\u5904\u7406\uff1a\u5982\u63a5\u89e6\u76ae\u80a4\uff0c\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\uff1b\u82e5\u5438\u5165\uff0c\u8f6c\u79fb\u81f3\u7a7a\u6c14\u65b0\u9c9c\u5904\u3002
\n5.3 \u5e9f\u5f03\u7269\u5904\u7406\uff1a\u6309\u5371\u9669\u5316\u5b66\u54c1\u89c4\u8303\u5904\u7f6e\uff0c\u4e0d\u53ef\u76f4\u63a5\u6392\u5165\u4e0b\u6c34\u9053\u3002 <\/p>\n
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