\u4ee5\u4e0b\u662f\u4e13\u4e1a\u7684\u4ea7\u54c1\u8bf4\u660e\u6587\u6863\uff1a<\/p>\n
\u4ea7\u54c1\u540d\u79f0\uff1aheptakis(6-deoxy-6-azido)\u03b2-CD
\nCAS\u53f7\uff1a53958-47-7
\n\u5206\u5b50\u5f0f\uff1aC42H63N21O28
\n\u5206\u5b50\u91cf\uff1a1310.07 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\nheptakis(6-deoxy-6-azido)\u03b2-CD\u662f\u4e00\u79cd\u7ecf\u8fc7\u5316\u5b66\u4fee\u9970\u7684\u03b2-\u73af\u7cca\u7cbe\u884d\u751f\u7269\uff0c\u5176\u7ed3\u6784\u4e2d\u6240\u67097\u4e2a\u8461\u8404\u7cd6\u5355\u5143\u76846\u4f4d\u7f9f\u57fa\u5747\u88ab\u53e0\u6c2e\u57fa\u56e2\u53d6\u4ee3\u3002\u8be5\u5316\u5408\u7269\u4fdd\u7559\u4e86\u03b2-\u73af\u7cca\u7cbe\u7684\u7ecf\u5178\u7a7a\u8154\u7ed3\u6784\uff08\u5185\u5f84\u7ea60.78 nm\uff09\uff0c\u540c\u65f6\u56e0\u53e0\u6c2e\u57fa\u56e2\u7684\u5f15\u5165\u800c\u663e\u8457\u589e\u5f3a\u4e86\u53cd\u5e94\u6d3b\u6027\u3002\u5176\u5206\u5b50\u91cf\u4e3a1310.07\uff0c\u5e38\u6e29\u4e0b\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7c89\u672b\uff0c\u7eaf\u5ea6\u7ecfHPLC\u9a8c\u8bc1\u5927\u4e8e96%\uff0c\u6613\u6eb6\u4e8eDMSO\u3001DMF\u7b49\u6781\u6027\u6709\u673a\u6eb6\u5242\uff0c\u5fae\u6eb6\u4e8e\u6c34\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u70b9\u51fb\u5316\u5b66\u7684\u5173\u952e\u4e2d\u95f4\u4f53\uff0c\u8be5\u4ea7\u54c1\u53ef\u901a\u8fc7CuAAC\u53cd\u5e94\uff08\u94dc\u50ac\u5316\u53e0\u6c2e-\u7094\u73af\u52a0\u6210\uff09\u9ad8\u6548\u8fde\u63a5\u7094\u57fa\u5316\u5206\u5b50\u3002\u5176\u7a7a\u8154\u7ed3\u6784\u53ef\u5305\u5408\u758f\u6c34\u6027\u5206\u5b50\uff0c\u5b9e\u73b0\u836f\u7269\u8f7d\u4f53\u529f\u80fd\uff1b\u53e0\u6c2e\u57fa\u56e2\u5219\u4e3a\u751f\u7269\u5076\u8054\u63d0\u4f9b\u591a\u4f4d\u70b9\u4fee\u9970\u5e73\u53f0\u3002\u5728\u5206\u5b50\u8bc6\u522b\u9886\u57df\uff0c\u5176\u4fee\u9970\u540e\u7684\u7a7a\u8154\u5bf9\u82b3\u9999\u65cf\u5316\u5408\u7269\u5177\u6709\u7279\u5f02\u6027\u7ed3\u5408\u80fd\u529b\uff0c\u8fd9\u79cd\u53cc\u91cd\u7279\u6027\u4f7f\u5176\u6210\u4e3a\u8d85\u5206\u5b50\u5316\u5b66\u7814\u7a76\u7684\u91cd\u8981\u5de5\u5177\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n3.1 \u836f\u7269\u9012\u9001\u7cfb\u7edf\uff1a\u4f5c\u4e3a\u667a\u80fd\u8f7d\u4f53\u7528\u4e8e\u6297\u764c\u836f\u7269\uff08\u5982\u7d2b\u6749\u9187\uff09\u7684\u589e\u6eb6\u4e0e\u9776\u5411\u4fee\u9970
\n3.2 \u751f\u7269\u6807\u8bb0\uff1a\u901a\u8fc7\u70b9\u51fb\u5316\u5b66\u5076\u8054\u8367\u5149\u63a2\u9488\uff0c\u7528\u4e8e\u6d3b\u7ec6\u80de\u6210\u50cf\u7814\u7a76
\n3.3 \u6750\u6599\u79d1\u5b66\uff1a\u5236\u5907\u529f\u80fd\u6027\u9ad8\u5206\u5b50\u6750\u6599\uff08\u5982\u81ea\u4fee\u590d\u6c34\u51dd\u80f6\uff09\u7684\u4ea4\u8054\u5242
\n3.4 \u5206\u6790\u5316\u5b66\uff1a\u624b\u6027\u5206\u79bb\u67f1\u7684\u4fee\u9970\u586b\u6599\uff0c\u7279\u522b\u9002\u7528\u4e8e\u82b3\u9999\u65cf\u5f02\u6784\u4f53\u62c6\u5206 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u2103\u3001\u907f\u5149\u3001\u5e72\u71e5\u6761\u4ef6\u4e0b\u4fdd\u5b58\uff0c\u5f00\u5c01\u540e\u9700\u5145\u6c2e\u6c14\u5bc6\u5c01\u3002\u4f7f\u7528\u65f6\u5e94\u907f\u514d\u63a5\u89e6\u8fd8\u539f\u6027\u7269\u8d28\uff0c\u53cd\u5e94\u4f53\u7cfb\u4e2d\u5efa\u8bae\u63a7\u5236pH\u57286-8\u8303\u56f4\u5185\u3002\u6eb6\u89e3\u65f6\u4f18\u5148\u9009\u7528\u9884\u8131\u6c14\u7684DMSO\u6eb6\u6db2\uff08\u6d53\u5ea6\u226410 mM\uff09\uff0c\u5982\u9700\u6c34\u76f8\u53cd\u5e94\uff0c\u5efa\u8bae\u52a0\u51655-10%\u52a9\u6eb6\u5242\u63d0\u9ad8\u6eb6\u89e3\u5ea6\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u7ecf\u8d28\u8c31\uff08MS\uff09\u548c\u6838\u78c1\uff081H NMR\uff09\u9a8c\u8bc1\u7ed3\u6784\uff0cHPLC\u68c0\u6d4b\u663e\u793a\u5355\u4e00\u4e3b\u5cf0\u3002\u5b89\u5168\u6ce8\u610f\u4e8b\u9879\uff1a\u53e0\u6c2e\u57fa\u56e2\u5728\u9ad8\u6e29\/\u5f3a\u51b2\u51fb\u4e0b\u53ef\u80fd\u7206\u70b8\uff0c\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u9632\u62a4\u88c5\u5907\uff1b\u907f\u514d\u4e0e\u91cd\u91d1\u5c5e\u63a5\u89e6\u4ee5\u9632\u751f\u6210\u7206\u70b8\u6027\u53e0\u6c2e\u91d1\u5c5e\u76d0\u3002\u5982\u63a5\u89e6\u76ae\u80a4\uff0c\u5e94\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u3002\u5e9f\u5f03\u7269\u5904\u7406\u9700\u9075\u5faa\u5f53\u5730\u5371\u9669\u5316\u5b66\u54c1\u5904\u7f6e\u6cd5\u89c4\u3002 <\/p>\n
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