4-\u53d4\u4e01\u57fa-4-\u6c27\u4ee3\u73af\u620a[C]\u5421\u54af-2-(1\u6c22)-\u7fa7\u9178\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u5316\u5b66\u540d\u79f0\u4e3atert-Butyl 4-oxohexahydrocyclopenta[c]pyrrole-2(1H)-carboxylate\uff0cCAS\u53f7\u4e3a879686-42-7\uff0c\u5206\u5b50\u5f0f\u4e3aC12H19NO3\uff0c\u5206\u5b50\u91cf\u4e3a225.284\u3002\u8be5\u5316\u5408\u7269\u662f\u4e00\u79cd\u9ad8\u7eaf\u5ea6\uff08>96%\uff09\u7684\u6742\u73af\u7fa7\u9178\u884d\u751f\u7269\uff0c\u7ed3\u6784\u4e2d\u542b\u6709\u73af\u620a\u5e76\u5421\u54af\u9aa8\u67b6\u548c\u53d4\u4e01\u6c27\u7fb0\u57fa\u4fdd\u62a4\u57fa\u56e2\uff0c\u5e38\u6e29\u4e0b\u5448\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6216\u7c89\u672b\u72b6\u3002\u5176\u72ec\u7279\u7684\u73af\u72b6\u7ed3\u6784\u4f7f\u5176\u5728\u6709\u673a\u5408\u6210\u4e2d\u8868\u73b0\u51fa\u826f\u597d\u7684\u53cd\u5e94\u6d3b\u6027\uff0c\u5c24\u5176\u5728\u6784\u5efa\u590d\u6742\u6742\u73af\u4f53\u7cfb\u65f6\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u4f5c\u4e3a\u5173\u952e\u4e2d\u95f4\u4f53\uff0c\u5728\u836f\u7269\u5316\u5b66\u548c\u751f\u7269\u6d3b\u6027\u5206\u5b50\u5408\u6210\u4e2d\u5177\u6709\u5e7f\u6cdb\u5e94\u7528\u3002\u5176\u7ed3\u6784\u4e2d\u7684\u73af\u620a\u5e76\u5421\u54af\u5355\u5143\u662f\u591a\u79cd\u751f\u7269\u78b1\u7c7b\u836f\u7269\u7684\u6838\u5fc3\u9aa8\u67b6\uff0c\u800c\u53d4\u4e01\u6c27\u7fb0\u57fa\uff08Boc\uff09\u4fdd\u62a4\u57fa\u7684\u5b58\u5728\u589e\u5f3a\u4e86\u5316\u5408\u7269\u7684\u7a33\u5b9a\u6027\uff0c\u4fbf\u4e8e\u540e\u7eed\u8131\u4fdd\u62a4\u53cd\u5e94\u3002\u5728\u86cb\u767d\u9176\u6291\u5236\u5242\u3001\u6297\u708e\u836f\u7269\u53ca\u795e\u7ecf\u6d3b\u6027\u5206\u5b50\u7684\u7814\u53d1\u4e2d\uff0c\u8be5\u5206\u5b50\u5e38\u88ab\u7528\u4e8e\u6784\u6548\u5173\u7cfb\u7814\u7a76\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a\u533b\u836f\u7814\u53d1\u4e2d\u4f5c\u4e3a\u6fc0\u9176\u6291\u5236\u5242\u6216GPCR\u914d\u4f53\u7684\u5408\u6210\u524d\u4f53\uff1b\u6750\u6599\u79d1\u5b66\u4e2d\u7528\u4e8e\u5236\u5907\u529f\u80fd\u6027\u9ad8\u5206\u5b50\u5355\u4f53\uff1b\u5b66\u672f\u7814\u7a76\u4e2d\u4f5c\u4e3a\u624b\u6027\u5408\u6210\u780c\u5757\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\u4f46\u4e0d\u9650\u4e8e\uff1a\u901a\u8fc7\u9170\u80fa\u5316\u53cd\u5e94\u6784\u5efa\u80bd\u7c7b\u884d\u751f\u7269\u3001\u53c2\u4e0e\u94af\u50ac\u5316\u4ea4\u53c9\u5076\u8054\u53cd\u5e94\u3001\u4f5c\u4e3a\u4e0d\u5bf9\u79f0\u6c22\u5316\u53cd\u5e94\u7684\u5e95\u7269\u7b49\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c29\u6c14\uff09\u73af\u5883\u4e0b\u907f\u5149\u4fdd\u5b58\uff0c\u5f00\u5c01\u540e\u9700\u5145\u6c2e\u5bc6\u5c01\u3002\u4f7f\u7528\u524d\u9700\u6062\u590d\u81f3\u5ba4\u6e29\u4ee5\u907f\u514d\u7ed3\u9732\uff0c\u79f0\u91cf\u5e94\u5728\u5e72\u71e5\u73af\u5883\u4e2d\u8fdb\u884c\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u8868\u660e\uff0c\u8be5\u5316\u5408\u7269\u6613\u6eb6\u4e8e\u4e8c\u6c2f\u7532\u70f7\u3001THF\u7b49\u6709\u673a\u6eb6\u5242\uff0c\u5fae\u6eb6\u4e8e\u9187\u7c7b\uff0c\u4e0d\u63a8\u8350\u76f4\u63a5\u7528\u4e8e\u6c34\u76f8\u53cd\u5e94\u4f53\u7cfb\u3002\u5b9e\u9a8c\u64cd\u4f5c\u5efa\u8bae\u5728\u901a\u98ce\u6a71\u4e2d\u8fdb\u884c\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u7ecfHPLC\u68c0\u6d4b\u7eaf\u5ea6>96%\uff0c\u6279\u6b21\u95f4\u4e00\u81f4\u6027\u8bef\u5dee\u63a7\u5236\u5728\u00b11%\u4ee5\u5185\u3002\u5b89\u5168\u6570\u636e\u8868\u660e\uff0c\u8be5\u7269\u8d28\u53ef\u80fd\u5f15\u8d77\u773c\u775b\u548c\u76ae\u80a4\u523a\u6fc0\uff0c\u64cd\u4f5c\u65f6\u5e94\u4f69\u6234\u9632\u62a4\u773c\u955c\u53ca\u4e01\u8148\u624b\u5957\u3002\u5982\u53d1\u751f\u63a5\u89e6\uff0c\u9700\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d1715\u5206\u949f\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5904\u7406\u9700\u7b26\u5408\u5f53\u5730\u5371\u9669\u5316\u5b66\u54c1\u7ba1\u7406\u6761\u4f8b\uff0c\u5efa\u8bae\u901a\u8fc7\u4e13\u4e1a\u673a\u6784\u8fdb\u884c\u711a\u5316\u5904\u7f6e\u3002 <\/p>\n
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