\u56db\u4e01\u57fa\u81a6\u56db\u6c1f\u787c\u9178\u76d0\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u56db\u4e01\u57fa\u81a6\u56db\u6c1f\u787c\u9178\u76d0\uff08tetrabutylphosphanium tetrafluoroborate\uff09\u662f\u4e00\u79cd\u6709\u673a\u81a6\u76d0\u7c7b\u5316\u5408\u7269\uff0c\u5316\u5b66\u5f0f\u4e3aC16H36BF4P\uff0c\u5206\u5b50\u91cf346.235\uff0cCAS\u53f7\u4e3a1813-60-1\u3002\u5176\u7ed3\u6784\u7531\u56db\u4e01\u57fa\u81a6\u9633\u79bb\u5b50\u548c\u56db\u6c1f\u787c\u9178\u9634\u79bb\u5b50\u7ec4\u6210\uff0c\u5916\u89c2\u901a\u5e38\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6216\u7c89\u672b\u3002\u8be5\u5316\u5408\u7269\u5177\u6709\u8f83\u9ad8\u7684\u70ed\u7a33\u5b9a\u6027\u548c\u5316\u5b66\u7a33\u5b9a\u6027\uff0c\u6613\u6eb6\u4e8e\u6781\u6027\u6709\u673a\u6eb6\u5242\uff08\u5982\u4e59\u8148\u3001\u4e8c\u7532\u57fa\u4e9a\u781c\uff09\uff0c\u5fae\u6eb6\u4e8e\u6c34\u3002\u7eaf\u5ea6\u6807\u51c6\u5927\u4e8e96%\uff0c\u7b26\u5408\u751f\u5316\u8bd5\u5242\u7684\u5de5\u4e1a\u4e0e\u79d1\u7814\u8981\u6c42\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u5b63\u81a6\u76d0\u7684\u4ee3\u8868\u6027\u7269\u8d28\uff0c\u56db\u4e01\u57fa\u81a6\u56db\u6c1f\u787c\u9178\u76d0\u5728\u6709\u673a\u5408\u6210\u4e2d\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u76f8\u8f6c\u79fb\u50ac\u5316\u6d3b\u6027\uff0c\u80fd\u591f\u4fc3\u8fdb\u975e\u5747\u76f8\u53cd\u5e94\u4e2d\u9634\u79bb\u5b50\u7684\u8f6c\u79fb\u3002\u5176\u81a6\u9633\u79bb\u5b50\u7ed3\u6784\u53ef\u7a33\u5b9a\u9ad8\u6d3b\u6027\u4e2d\u95f4\u4f53\uff0c\u5728\u78b3-\u78b3\u952e\u5f62\u6210\u3001\u805a\u5408\u53cd\u5e94\u53ca\u4e0d\u5bf9\u79f0\u5408\u6210\u4e2d\u5177\u6709\u91cd\u8981\u4f5c\u7528\u3002\u6b64\u5916\uff0c\u8be5\u5316\u5408\u7269\u8fd8\u53ef\u4f5c\u4e3a\u79bb\u5b50\u6db2\u4f53\u524d\u4f53\u6216\u7535\u89e3\u8d28\u6dfb\u52a0\u5242\uff0c\u5e94\u7528\u4e8e\u7535\u5316\u5b66\u9886\u57df\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u5e7f\u6cdb\u5e94\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a
\n– \u6709\u673a\u5408\u6210\uff1a\u4f5c\u4e3a\u76f8\u8f6c\u79fb\u50ac\u5316\u5242\uff0c\u7528\u4e8e\u70f7\u57fa\u5316\u3001\u9170\u57fa\u5316\u53ca\u73af\u6c27\u5316\u53cd\u5e94\u3002
\n– \u6750\u6599\u79d1\u5b66\uff1a\u53c2\u4e0e\u5236\u5907\u529f\u80fd\u6027\u79bb\u5b50\u6db2\u4f53\uff0c\u4f18\u5316\u9502\u79bb\u5b50\u7535\u6c60\u7535\u89e3\u8d28\u7684\u5bfc\u7535\u6027\u3002
\n– \u5206\u6790\u5316\u5b66\uff1a\u4f5c\u4e3a\u9ad8\u6548\u6db2\u76f8\u8272\u8c31\uff08HPLC\uff09\u7684\u79bb\u5b50\u5bf9\u8bd5\u5242\uff0c\u6539\u5584\u5206\u79bb\u6548\u679c\u3002
\n– \u533b\u836f\u4e2d\u95f4\u4f53\uff1a\u7528\u4e8e\u5408\u6210\u624b\u6027\u836f\u7269\u6216\u751f\u7269\u6d3b\u6027\u5206\u5b50\u7684\u81a6\u914d\u4f53\u4fee\u9970\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u50a8\u5b58\u4e8e\u5bc6\u95ed\u5bb9\u5668\u4e2d\uff0c\u907f\u514d\u5149\u7167\u4e0e\u6e7f\u6c14\uff0c\u63a8\u8350\u6e29\u5ea6\u8303\u56f4\u4e3a2-8\u2103\u3002\u957f\u671f\u4fdd\u5b58\u5efa\u8bae\u5145\u5165\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u73af\u5883\u4e0b\u64cd\u4f5c\uff0c\u907f\u514d\u4e0e\u5f3a\u6c27\u5316\u5242\u63a5\u89e6\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u8868\u660e\uff0c\u63a8\u8350\u4f7f\u7528\u65e0\u6c34\u4e59\u8148\u6216DMF\u4f5c\u4e3a\u6eb6\u5242\u4f53\u7cfb\u3002\u5b9e\u9a8c\u540e\u5269\u4f59\u7269\u6599\u5e94\u7acb\u5373\u5bc6\u5c01\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u54c1\u901a\u8fc7\u6838\u78c1\u5171\u632f\uff08NMR\uff09\u548c\u9ad8\u6548\u6db2\u76f8\u8272\u8c31\uff08HPLC\uff09\u53cc\u91cd\u9a8c\u8bc1\uff0c\u786e\u4fdd\u7eaf\u5ea6\uff1e96%\u3002\u542b\u5fae\u91cf\u6c34\u5206\uff08\u22640.5%\uff0c\u5361\u5c14\u8d39\u4f11\u6cd5\u6d4b\u5b9a\uff09\u3002\u5b89\u5168\u6570\u636e\u8868\u660e\uff0c\u8be5\u7269\u8d28\u5bf9\u773c\u775b\u548c\u76ae\u80a4\u6709\u523a\u6fc0\u6027\uff0c\u64cd\u4f5c\u65f6\u5e94\u4f69\u6234\u9632\u62a4\u624b\u5957\u53ca\u62a4\u76ee\u955c\u3002\u82e5\u4e0d\u614e\u63a5\u89e6\uff0c\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5904\u7406\u9700\u7b26\u5408\u5f53\u5730\u5316\u5b66\u54c1\u7ba1\u7406\u6cd5\u89c4\uff0c\u7981\u6b62\u76f4\u63a5\u6392\u653e\u81f3\u73af\u5883\u4e2d\u3002 <\/p>\n
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