3-(9-\u82b4\u7532\u6c27\u57fa\u7fb0\u57fa)\u6c28\u57fa-3-(2-\u785d\u57fa\u82ef\u57fa)\u4e19\u9178\uff08CAS\u53f7\uff1a171778-06-6\uff09\u662f\u4e00\u79cd\u5177\u6709\u7279\u5b9a\u4fdd\u62a4\u57fa\u56e2\u7684\u6c28\u57fa\u9178\u884d\u751f\u7269\uff0c\u5206\u5b50\u5f0f\u4e3aC24H20N2O6\uff0c\u5206\u5b50\u91cf\u4e3a432.425\u3002\u8be5\u5316\u5408\u7269\u5728\u5e38\u6e29\u4e0b\u4e3a\u767d\u8272\u81f3\u6de1\u9ec4\u8272\u56fa\u4f53\uff0c\u7eaf\u5ea6\u901a\u5e38\u9ad8\u4e8e96%\u3002\u5176\u7ed3\u6784\u4e2d\u7684\u82b4\u7532\u6c27\u57fa\u7fb0\u57fa\uff08Fmoc\uff09\u548c\u785d\u57fa\u82ef\u57fa\u8d4b\u4e88\u5176\u72ec\u7279\u7684\u5149\u654f\u6027\u548c\u4fdd\u62a4\u57fa\u7279\u6027\uff0c\u9002\u7528\u4e8e\u591a\u80bd\u5408\u6210\u4e2d\u7684\u9009\u62e9\u6027\u4fdd\u62a4\u4e0e\u8131\u4fdd\u62a4\u53cd\u5e94\u3002<\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u8be5\u5316\u5408\u7269\u5c5e\u4e8eFmoc\u4fdd\u62a4\u7684\u6c28\u57fa\u9178\u884d\u751f\u7269\uff0c\u5176\u5206\u5b50\u7ed3\u6784\u5305\u542bFmoc\u4fdd\u62a4\u57fa\u56e2\u548c2-\u785d\u57fa\u82ef\u57fa\u4fee\u9970\u7684\u4e19\u9178\u9aa8\u67b6\u3002Fmoc\u57fa\u56e2\u5728\u78b1\u6027\u6761\u4ef6\u4e0b\u53ef\u88ab\u8131\u9664\uff0c\u800c\u785d\u57fa\u82ef\u57fa\u7684\u5b58\u5728\u4f7f\u5176\u5bf9\u5149\u654f\u611f\uff0c\u9002\u7528\u4e8e\u5149\u5316\u5b66\u8c03\u63a7\u53cd\u5e94\u3002\u5176\u5316\u5b66\u7a33\u5b9a\u6027\u8f83\u9ad8\uff0c\u4f46\u5728\u5f3a\u9178\u6216\u5f3a\u78b1\u6761\u4ef6\u4e0b\u53ef\u80fd\u53d1\u751f\u5206\u89e3\u3002<\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u591a\u80bd\u56fa\u76f8\u5408\u6210\u7684\u91cd\u8981\u4e2d\u95f4\u4f53\uff0c\u8be5\u5316\u5408\u7269\u80fd\u591f\u901a\u8fc7Fmoc\u4fdd\u62a4\u57fa\u5b9e\u73b0\u6c28\u57fa\u7684\u9009\u62e9\u6027\u4fdd\u62a4\uff0c\u907f\u514d\u526f\u53cd\u5e94\u7684\u53d1\u751f\u3002\u785d\u57fa\u82ef\u57fa\u7684\u5f15\u5165\u8fdb\u4e00\u6b65\u6269\u5c55\u4e86\u5176\u5728\u5149\u63a7\u91ca\u653e\u7cfb\u7edf\u4e2d\u7684\u5e94\u7528\uff0c\u4f8b\u5982\u5149\u89e6\u53d1\u836f\u7269\u9012\u9001\u6216\u5149\u5316\u5b66\u6807\u8bb0\u7814\u7a76\u3002\u5176\u5728\u751f\u7269\u5171\u8f6d\u5316\u5b66\u548c\u86cb\u767d\u8d28\u5de5\u7a0b\u9886\u57df\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002<\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u591a\u80bd\u5408\u6210\u3001\u836f\u7269\u5f00\u53d1\u53ca\u751f\u7269\u6807\u8bb0\u7814\u7a76\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a
\n– \u4f5c\u4e3aFmoc\u4fdd\u62a4\u7684\u6c28\u57fa\u9178\u6784\u5efa\u5757\uff0c\u7528\u4e8e\u56fa\u76f8\u591a\u80bd\u5408\u6210\u3002
\n– \u5149\u654f\u4fdd\u62a4\u57fa\u56e2\u7684\u7814\u7a76\uff0c\u7528\u4e8e\u5f00\u53d1\u5149\u54cd\u5e94\u578b\u836f\u7269\u6216\u63a2\u9488\u3002
\n– \u751f\u7269\u5171\u8f6d\u5316\u5b66\u4e2d\uff0c\u4f5c\u4e3a\u8fde\u63a5\u5206\u5b50\u6216\u529f\u80fd\u5316\u8bd5\u5242\u3002<\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u3001\u907f\u5149\u3001\u5e72\u71e5\u7684\u6761\u4ef6\u4e0b\u50a8\u5b58\uff0c\u4ee5\u4fdd\u6301\u5176\u7a33\u5b9a\u6027\u3002\u4f7f\u7528\u65f6\u9700\u907f\u514d\u5f3a\u5149\u76f4\u5c04\uff0c\u5e76\u5728\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u73af\u5883\u4e0b\u64cd\u4f5c\u4ee5\u51cf\u5c11\u964d\u89e3\u98ce\u9669\u3002\u6eb6\u89e3\u65f6\u63a8\u8350\u4f7f\u7528\u4e8c\u7532\u57fa\u7532\u9170\u80fa\uff08DMF\uff09\u6216\u4e8c\u6c2f\u7532\u70f7\u7b49\u6709\u673a\u6eb6\u5242\u3002<\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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