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6-\u6eb4\u5421\u5576-2-\u787c\u9178\u9891\u54ea\u916f\uff086-Bromopyridine-2-boronic acid pinacol ester\uff09\u662f\u4e00\u79cd\u91cd\u8981\u7684\u6709\u673a\u787c\u5316\u5408\u7269\uff0cCAS\u53f7\u4e3a651358-83-7\uff0c\u5206\u5b50\u5f0f\u4e3aC11H15BBrNO2\uff0c\u5206\u5b50\u91cf\u4e3a283.957\u3002\u8be5\u5316\u5408\u7269\u4ee5\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6216\u7c89\u672b\u5f62\u5f0f\u5b58\u5728\uff0c\u7eaf\u5ea6\u901a\u5e38\u9ad8\u4e8e96%\u3002\u5176\u7ed3\u6784\u4e2d\u5305\u542b\u6eb4\u539f\u5b50\u548c\u787c\u9178\u9891\u54ea\u916f\u57fa\u56e2\uff0c\u4f7f\u5176\u5728\u6709\u673a\u5408\u6210\u4e2d\u5177\u6709\u8f83\u9ad8\u7684\u53cd\u5e94\u6d3b\u6027\uff0c\u5c24\u5176\u9002\u7528\u4e8eSuzuki-Miyaura\u5076\u8054\u53cd\u5e94\u3002<\/p>\n

1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n6-\u6eb4\u5421\u5576-2-\u787c\u9178\u9891\u54ea\u916f\u662f\u4e00\u79cd\u5421\u5576\u884d\u751f\u7269\uff0c\u517c\u5177\u6eb4\u4ee3\u548c\u787c\u9178\u916f\u5b98\u80fd\u56e2\u3002\u5176\u9891\u54ea\u9187\u916f\u7ed3\u6784\u589e\u5f3a\u4e86\u787c\u539f\u5b50\u7684\u7a33\u5b9a\u6027\uff0c\u4fbf\u4e8e\u50a8\u5b58\u548c\u8fd0\u8f93\u3002\u8be5\u5316\u5408\u7269\u5728\u5e38\u6e29\u4e0b\u7a33\u5b9a\uff0c\u4f46\u9700\u907f\u514d\u4e0e\u5f3a\u6c27\u5316\u5242\u6216\u6f6e\u6e7f\u73af\u5883\u63a5\u89e6\u3002\u5176\u7194\u70b9\u548c\u6cb8\u70b9\u6570\u636e\u9700\u53c2\u8003\u5177\u4f53\u5b9e\u9a8c\u6761\u4ef6\uff0c\u6eb6\u89e3\u6027\u65b9\u9762\u6613\u6eb6\u4e8e\u5e38\u89c1\u6709\u673a\u6eb6\u5242\u5982\u4e8c\u6c2f\u7532\u70f7\u3001\u56db\u6c22\u544b\u5583\u7b49\u3002<\/p>\n

2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u6709\u673a\u787c\u8bd5\u5242\uff0c\u8be5\u5316\u5408\u7269\u5728\u836f\u7269\u5316\u5b66\u548c\u6750\u6599\u79d1\u5b66\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002\u5176\u5421\u5576\u9aa8\u67b6\u662f\u8bb8\u591a\u751f\u7269\u6d3b\u6027\u5206\u5b50\u7684\u6838\u5fc3\u7ed3\u6784\uff0c\u800c\u787c\u9178\u916f\u57fa\u56e2\u53ef\u901a\u8fc7\u5076\u8054\u53cd\u5e94\u9ad8\u6548\u6784\u5efa\u78b3-\u78b3\u952e\u3002\u8fd9\u79cd\u53cc\u91cd\u529f\u80fd\u6027\u4f7f\u5176\u6210\u4e3a\u5408\u6210\u590d\u6742\u6742\u73af\u5316\u5408\u7269\u7684\u5173\u952e\u4e2d\u95f4\u4f53\uff0c\u5c24\u5176\u5728\u6297\u80bf\u7624\u3001\u6297\u611f\u67d3\u836f\u7269\u7814\u53d1\u4e2d\u5e94\u7528\u5e7f\u6cdb\u3002<\/p>\n

3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a
\n– \u533b\u836f\u4e2d\u95f4\u4f53\uff1a\u7528\u4e8e\u5408\u6210\u9776\u5411\u836f\u7269\u5206\u5b50\uff0c\u5982\u6fc0\u9176\u6291\u5236\u5242\uff1b
\n– \u6750\u6599\u79d1\u5b66\uff1a\u5236\u5907\u6709\u673a\u5149\u7535\u6750\u6599\u53ca\u914d\u4f4d\u805a\u5408\u7269\uff1b
\n– \u519c\u4e1a\u5316\u5b66\uff1a\u5408\u6210\u5177\u6709\u751f\u7269\u6d3b\u6027\u7684\u519c\u836f\u5316\u5408\u7269\uff1b
\n– \u5b66\u672f\u7814\u7a76\uff1a\u4f5c\u4e3aSuzuki\u5076\u8054\u53cd\u5e94\u7684\u6807\u51c6\u5e95\u7269\u7528\u4e8e\u65b9\u6cd5\u5b66\u5f00\u53d1\u3002 <\/p>\n

4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c29\u6c14\uff09\u4fdd\u62a4\u4e0b\u5bc6\u5c01\u4fdd\u5b58\uff0c\u50a8\u5b58\u6e29\u5ea6\u4e3a2-8\u00b0C\uff0c\u907f\u514d\u5149\u7167\u548c\u6f6e\u6e7f\u73af\u5883\u3002\u4f7f\u7528\u524d\u9700\u5728\u5e72\u71e5\u73af\u5883\u4e0b\u6062\u590d\u81f3\u5ba4\u6e29\uff0c\u5f00\u5c01\u540e\u5efa\u8bae\u4e00\u6b21\u6027\u7528\u5b8c\u3002\u64cd\u4f5c\u65f6\u5e94\u4f69\u6234\u9632\u62a4\u624b\u5957\u3001\u62a4\u76ee\u955c\uff0c\u5e76\u5728\u901a\u98ce\u6a71\u4e2d\u8fdb\u884c\u3002<\/p>\n

5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u901a\u8fc7HPLC\u68c0\u6d4b\u7eaf\u5ea6\u226596%\uff0c\u5e76\u63d0\u4f9b\u8be6\u7ec6\u7684\u6838\u78c1\u5171\u632f\uff08NMR\uff09\u548c\u8d28\u8c31\uff08MS\uff09\u5206\u6790\u62a5\u544a\u3002\u5b89\u5168\u65b9\u9762\uff0c\u8be5\u5316\u5408\u7269\u53ef\u80fd\u5bf9\u773c\u775b\u3001\u76ae\u80a4\u548c\u547c\u5438\u7cfb\u7edf\u9020\u6210\u523a\u6fc0\uff0c\u64cd\u4f5c\u65f6\u9700\u9075\u5b88GHS\u6807\u51c6\uff0c\u5371\u9669\u8bf4\u660e\u4ee3\u7801\u5305\u62ecH315-H319-H335\u3002\u5e9f\u5f03\u7269\u5904\u7406\u5e94\u9075\u5faa\u5f53\u5730\u5316\u5b66\u54c1\u5904\u7f6e\u6cd5\u89c4\uff0c\u4e0d\u53ef\u76f4\u63a5\u6392\u5165\u4e0b\u6c34\u9053\u3002 <\/p>\n

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