\u4ea7\u54c1\u8bf4\u660e <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u5316\u5b66\u540d\u79f0\u4e3a(1S),3(R)-bis<(tert-butyldimethylsilyl)oxy>-20(S)-(hydroxymethyl)-9,10-secopregna-5(E),7(E),10(19)-triene\uff0c\u4e2d\u6587\u540d\u79f0\u4e3a(1S),3(R)-\u53cc<(\u53d4\u4e01\u57fa\u4e8c\u7532\u57fa\u7845\u6c27\u57fa)>-20(S)-(\u7f9f\u7532\u57fa)-9,10-\u5f00\u73af\u5b55\u753e-5(E),7(E),10(19)-\u4e09\u70ef\uff0cCAS\u53f7\u4e3a128387-35-9\u3002\u5176\u5206\u5b50\u5f0f\u4e3aC34H62O3Si2\uff0c\u5206\u5b50\u91cf\u4e3a575.025\uff0c\u7eaf\u5ea6\u9ad8\u4e8e96%\u3002\u8be5\u5316\u5408\u7269\u662f\u4e00\u79cd\u7ecf\u8fc7\u7845\u70f7\u5316\u4fee\u9970\u7684\u7ef4\u751f\u7d20D3\u884d\u751f\u7269\uff0c\u5177\u6709\u7279\u5b9a\u7684\u7acb\u4f53\u6784\u578b\uff081S,3R,20S\uff09\u548c\u5171\u8f6d\u4e09\u70ef\u7ed3\u6784\uff085E,7E,10(19)\uff09\uff0c\u5176\u53d4\u4e01\u57fa\u4e8c\u7532\u57fa\u7845\u57fa\uff08TBS\uff09\u4fdd\u62a4\u57fa\u56e2\u589e\u5f3a\u4e86\u5206\u5b50\u7684\u7a33\u5b9a\u6027\u548c\u8102\u6eb6\u6027\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u662f\u7ef4\u751f\u7d20D3\u4ee3\u8c22\u9014\u5f84\u4e2d\u7684\u5173\u952e\u4e2d\u95f4\u4f53\uff0c\u5c24\u5176\u5728\u5408\u6210\u6d3b\u6027\u7ef4\u751f\u7d20D\u7c7b\u4f3c\u7269\uff08\u5982\u9aa8\u5316\u4e09\u9187\u53ca\u5176\u884d\u751f\u7269\uff09\u4e2d\u5177\u6709\u91cd\u8981\u4f5c\u7528\u3002\u5176\u7ed3\u6784\u4e2d\u7684\u7f9f\u57fa\u7ecf\u7845\u70f7\u5316\u4fdd\u62a4\u540e\uff0c\u53ef\u9009\u62e9\u6027\u53c2\u4e0e\u540e\u7eed\u5316\u5b66\u53cd\u5e94\uff0c\u4e3a\u5408\u6210\u5177\u6709\u7279\u5b9a\u751f\u7269\u6d3b\u6027\u7684\u7ef4\u751f\u7d20D\u7c7b\u5316\u5408\u7269\u63d0\u4f9b\u91cd\u8981\u524d\u4f53\u3002\u8fd9\u7c7b\u5316\u5408\u7269\u5728\u8c03\u8282\u9499\u78f7\u4ee3\u8c22\u3001\u7ec6\u80de\u5206\u5316\u548c\u514d\u75ab\u8c03\u8282\u7b49\u65b9\u9762\u5177\u6709\u5e7f\u6cdb\u751f\u7406\u529f\u80fd\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u533b\u836f\u7814\u53d1\u548c\u751f\u5316\u7814\u7a76\u9886\u57df\uff0c\u5177\u4f53\u5305\u62ec\uff1a
\n– \u4f5c\u4e3a\u5408\u6210\u6d3b\u6027\u7ef4\u751f\u7d20D\u7c7b\u4f3c\u7269\u7684\u5173\u952e\u4e2d\u95f4\u4f53\uff0c\u7528\u4e8e\u5f00\u53d1\u6cbb\u7597\u9aa8\u8d28\u758f\u677e\u3001\u94f6\u5c51\u75c5\u53ca\u7532\u72b6\u65c1\u817a\u529f\u80fd\u5f02\u5e38\u7684\u836f\u7269\uff1b
\n– \u7528\u4e8e\u7814\u7a76\u7ef4\u751f\u7d20D\u53d7\u4f53\u7684\u914d\u4f53\u7ed3\u5408\u7279\u6027\u53ca\u4fe1\u53f7\u8f6c\u5bfc\u673a\u5236\uff1b
\n– \u5728\u6709\u673a\u5408\u6210\u4e2d\u4f5c\u4e3a\u9ad8\u4ef7\u503c\u624b\u6027\u780c\u5757\uff0c\u7528\u4e8e\u6784\u5efa\u590d\u6742\u753e\u4f53\u9aa8\u67b6\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u4ee5\u4e0b\u907f\u5149\u4fdd\u5b58\uff0c\u957f\u671f\u50a8\u5b58\u9700\u7f6e\u4e8e\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u73af\u5883\u4e2d\u4ee5\u51cf\u7f13\u6c27\u5316\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u60f0\u6027\u6c1b\u56f4\uff08\u5982\u6c29\u6c14\u624b\u5957\u7bb1\uff09\u4e2d\u64cd\u4f5c\uff0c\u907f\u514d\u63a5\u89e6\u6c34\u5206\u6216\u5f3a\u9178\u5f3a\u78b1\u3002\u6eb6\u89e3\u63a8\u8350\u4f7f\u7528\u65e0\u6c34\u6709\u673a\u6eb6\u5242\uff08\u5982\u4e8c\u6c2f\u7532\u70f7\u3001\u56db\u6c22\u544b\u5583\uff09\u3002\u5f00\u5c01\u540e\u5efa\u8bae\u4e00\u6b21\u6027\u7528\u5b8c\uff0c\u6216\u5206\u88c5\u540e\u5bc6\u5c01\u4fdd\u5b58\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u901a\u8fc7HPLC\u68c0\u6d4b\u786e\u8ba4\u7eaf\u5ea6>96%\uff0c\u5e76\u63d0\u4f9bCOA\uff08\u8d28\u91cf\u5206\u6790\u8bc1\u4e66\uff09\u3002\u9700\u6ce8\u610f\u5176\u53ef\u80fd\u5bf9\u773c\u775b\u3001\u76ae\u80a4\u548c\u547c\u5438\u7cfb\u7edf\u4ea7\u751f\u523a\u6fc0\uff0c\u64cd\u4f5c\u65f6\u5e94\u7a7f\u6234\u9632\u62a4\u88c5\u5907\uff08\u624b\u5957\u3001\u62a4\u76ee\u955c\u53ca\u9632\u5c18\u53e3\u7f69\uff09\u3002\u82e5\u610f\u5916\u63a5\u89e6\uff0c\u9700\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5e94\u4f5c\u4e3a\u6709\u5bb3\u5316\u5b66\u54c1\u5904\u7f6e\uff0c\u9075\u5b88\u5f53\u5730\u73af\u4fdd\u6cd5\u89c4\u3002 <\/p>\n
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