\u4ea7\u54c1\u540d\u79f0\uff1aBoc-DL-\u03b2-leucine
\n\u5316\u5b66\u540d\u79f0\uff1aBoc-DL-\u03b2-leucine
\nCAS\u53f7\uff1a248924-39-2
\n\u5206\u5b50\u5f0f\uff1aC11H21NO4
\n\u5206\u5b50\u91cf\uff1a231.289
\n\u7eaf\u5ea6\uff1a>96% <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\nBoc-DL-\u03b2-leucine\u662f\u4e00\u79cd\u4fdd\u62a4\u6027\u6c28\u57fa\u9178\u884d\u751f\u7269\uff0c\u5176\u5316\u5b66\u7ed3\u6784\u4e2d\u5305\u542b\u53d4\u4e01\u6c27\u7fb0\u57fa\uff08Boc\uff09\u4fdd\u62a4\u57fa\u56e2\u548c\u03b2-\u4f4d\u53d6\u4ee3\u7684\u4eae\u6c28\u9178\u6b8b\u57fa\u3002\u8be5\u5316\u5408\u7269\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\uff0c\u5206\u5b50\u91cf\u4e3a231.289\uff0c\u5206\u5b50\u5f0f\u4e3aC11H21NO4\u3002\u5176\u7eaf\u5ea6\u901a\u5e38\u9ad8\u4e8e96%\uff0c\u9002\u7528\u4e8e\u9ad8\u8981\u6c42\u7684\u5408\u6210\u4e0e\u751f\u5316\u7814\u7a76\u3002Boc\u57fa\u56e2\u7684\u5f15\u5165\u589e\u5f3a\u4e86\u5316\u5408\u7269\u7684\u7a33\u5b9a\u6027\uff0c\u4fbf\u4e8e\u5728\u80bd\u5408\u6210\u4e2d\u4f5c\u4e3a\u4e2d\u95f4\u4f53\u4f7f\u7528\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\nBoc-DL-\u03b2-leucine\u5728\u80bd\u94fe\u7ec4\u88c5\u4e2d\u626e\u6f14\u91cd\u8981\u89d2\u8272\uff0c\u5176Boc\u4fdd\u62a4\u57fa\u53ef\u5728\u9178\u6027\u6761\u4ef6\u4e0b\u9009\u62e9\u6027\u8131\u9664\uff0c\u800c\u03b2-\u4f4d\u53d6\u4ee3\u7684\u4eae\u6c28\u9178\u7ed3\u6784\u63d0\u4f9b\u4e86\u72ec\u7279\u7684\u7a7a\u95f4\u4f4d\u963b\u6548\u5e94\uff0c\u6709\u52a9\u4e8e\u7814\u7a76\u975e\u5929\u7136\u6c28\u57fa\u9178\u5bf9\u86cb\u767d\u8d28\u7ed3\u6784\u548c\u529f\u80fd\u7684\u5f71\u54cd\u3002\u8be5\u5316\u5408\u7269\u5728\u63a2\u7d22\u9176\u5e95\u7269\u7279\u5f02\u6027\u3001\u86cb\u767d\u8d28\u6298\u53e0\u673a\u5236\u4ee5\u53ca\u836f\u7269\u8bbe\u8ba1\u7b49\u9886\u57df\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\nBoc-DL-\u03b2-leucine\u5e7f\u6cdb\u5e94\u7528\u4e8e\u591a\u80bd\u5408\u6210\u3001\u836f\u7269\u7814\u53d1\u548c\u751f\u7269\u5316\u5b66\u7814\u7a76\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a\u4f5c\u4e3a\u975e\u5929\u7136\u6c28\u57fa\u9178\u780c\u5757\u7528\u4e8e\u56fa\u76f8\u6216\u6db2\u76f8\u80bd\u5408\u6210\uff1b\u5728\u836f\u7269\u8bbe\u8ba1\u4e2d\u7528\u4e8e\u4fee\u9970\u80bd\u7c7b\u836f\u7269\u7684\u836f\u4ee3\u52a8\u529b\u5b66\u6027\u8d28\uff1b\u4f5c\u4e3a\u751f\u5316\u8bd5\u5242\u7528\u4e8e\u7814\u7a76\u03b2-\u6c28\u57fa\u9178\u7684\u4ee3\u8c22\u9014\u5f84\u548c\u9176\u5b66\u7279\u6027\u3002\u6b64\u5916\uff0c\u5b83\u8fd8\u53ef\u7528\u4e8e\u5236\u5907\u624b\u6027\u50ac\u5316\u5242\u6216\u529f\u80fd\u6750\u6599\u7684\u524d\u4f53\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u672c\u54c1\u5e94\u5bc6\u5c01\u4fdd\u5b58\u4e8e\u5e72\u71e5\u3001\u9634\u51c9\u7684\u73af\u5883\u4e2d\uff0c\u63a8\u8350\u50a8\u5b58\u6e29\u5ea6\u4e3a2-8\u00b0C\uff0c\u907f\u514d\u5149\u7167\u548c\u6f6e\u6e7f\u3002\u4f7f\u7528\u65f6\u9700\u5728\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u4fdd\u62a4\u4e0b\u64cd\u4f5c\uff0c\u4ee5\u9632\u6b62\u964d\u89e3\u3002\u6eb6\u89e3\u5efa\u8bae\u4f7f\u7528\u6781\u6027\u6709\u673a\u6eb6\u5242\uff08\u5982DMF\u3001DMSO\u6216\u7532\u9187\uff09\uff0c\u5e76\u907f\u514d\u4e0e\u5f3a\u9178\u3001\u5f3a\u6c27\u5316\u5242\u76f4\u63a5\u63a5\u89e6\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u7ecfHPLC\u68c0\u6d4b\uff0c\u7eaf\u5ea6>96%\uff0c\u7b26\u5408\u751f\u5316\u8bd5\u5242\u6807\u51c6\u3002\u4f7f\u7528\u65f6\u9700\u7a7f\u6234\u9632\u62a4\u88c5\u5907\uff08\u5982\u624b\u5957\u3001\u62a4\u76ee\u955c\u548c\u5b9e\u9a8c\u670d\uff09\uff0c\u907f\u514d\u5438\u5165\u7c89\u5c18\u6216\u63a5\u89e6\u76ae\u80a4\u3002\u82e5\u4e0d\u614e\u63a5\u89e6\uff0c\u5e94\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5e94\u6309\u7167\u5f53\u5730\u6cd5\u89c4\u5904\u7406\uff0c\u907f\u514d\u73af\u5883\u6c61\u67d3\u3002 <\/p>\n
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