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1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n(3R)-3-(4-cyanophenyl)-3-[(2-methylpropan-2-yl)oxycarbonylamino]propanoic acid\uff0c\u4e2d\u6587\u540d\u79f0\u4e3a(R)-Boc-4-\u6c30\u57fa-\u03b2-Phe-OH\uff0c\u662f\u4e00\u79cd\u5177\u6709\u7279\u5b9a\u7acb\u4f53\u6784\u578b\u7684\u975e\u5929\u7136\u6c28\u57fa\u9178\u884d\u751f\u7269\u3002\u5176\u5206\u5b50\u5f0f\u4e3aC15H18N2O4\uff0c\u5206\u5b50\u91cf\u4e3a290.314\uff0cCAS\u53f7\u4e3a501015-22-1\u3002\u8be5\u5316\u5408\u7269\u4ee5\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u7c89\u672b\u5f62\u5f0f\u5b58\u5728\uff0c\u7eaf\u5ea6\u9ad8\u4e8e96%\u3002\u5176\u7ed3\u6784\u7279\u5f81\u5305\u62ec\u4e00\u4e2a\u6c30\u57fa\u82ef\u57fa\u56e2\u3001Boc\u4fdd\u62a4\u7684\u6c28\u57fa\u4ee5\u53ca\u7fa7\u9178\u5b98\u80fd\u56e2\uff0c\u8fd9\u4e9b\u57fa\u56e2\u8d4b\u4e88\u5176\u72ec\u7279\u7684\u5316\u5b66\u53cd\u5e94\u6027\u548c\u6eb6\u89e3\u6027\uff08\u6613\u6eb6\u4e8e\u6709\u673a\u6eb6\u5242\u5982DMSO\u548c\u7532\u9187\uff0c\u5fae\u6eb6\u4e8e\u6c34\uff09\u3002<\/p>\n

2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u03b2-\u6c28\u57fa\u9178\u7684\u884d\u751f\u7269\uff0c\u8be5\u5316\u5408\u7269\u5728\u80bd\u94fe\u4fee\u9970\u4e2d\u8868\u73b0\u51fa\u663e\u8457\u7684\u7a7a\u95f4\u4f4d\u963b\u6548\u5e94\u548c\u6784\u8c61\u7a33\u5b9a\u6027\uff0c\u80fd\u591f\u5e72\u6270\u5929\u7136\u80bd\u94fe\u7684\u6298\u53e0\u884c\u4e3a\uff0c\u4ece\u800c\u7528\u4e8e\u7814\u7a76\u86cb\u767d\u8d28\u7ed3\u6784\u548c\u529f\u80fd\u5173\u7cfb\u3002Boc\u4fdd\u62a4\u57fa\u7684\u5b58\u5728\u4f7f\u5176\u5728\u56fa\u76f8\u80bd\u5408\u6210\uff08SPPS\uff09\u4e2d\u5177\u6709\u9009\u62e9\u6027\u8131\u4fdd\u62a4\u7684\u4f18\u52bf\uff0c\u800c\u6c30\u57fa\u7684\u5f3a\u5438\u7535\u5b50\u7279\u6027\u53ef\u589e\u5f3a\u5176\u4f5c\u4e3a\u9176\u6291\u5236\u5242\u6216\u53d7\u4f53\u62ee\u6297\u5242\u7684\u6d3b\u6027\u3002\u8fd9\u4e9b\u7279\u6027\u4f7f\u5176\u6210\u4e3a\u836f\u7269\u5316\u5b66\u548c\u751f\u7269\u5316\u5b66\u7814\u7a76\u4e2d\u7684\u91cd\u8981\u4e2d\u95f4\u4f53\u3002<\/p>\n

3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u4ea7\u54c1\u5e7f\u6cdb\u5e94\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a
\n– \u836f\u7269\u7814\u53d1\uff1a\u4f5c\u4e3a\u6784\u5efa\u975e\u5929\u7136\u80bd\u7c7b\u836f\u7269\u7684\u5173\u952e\u6a21\u5757\uff0c\u7528\u4e8e\u5f00\u53d1\u6297\u80bf\u7624\u3001\u6297\u75c5\u6bd2\u6216\u795e\u7ecf\u8c03\u8282\u5242\u3002
\n– \u5316\u5b66\u751f\u7269\u5b66\uff1a\u901a\u8fc7\u5f15\u5165\u03b2-\u6c28\u57fa\u9178\u7ed3\u6784\u63a2\u9488\uff0c\u7814\u7a76\u86cb\u767d\u8d28-\u914d\u4f53\u76f8\u4e92\u4f5c\u7528\u673a\u5236\u3002
\n– \u6750\u6599\u79d1\u5b66\uff1a\u4f5c\u4e3a\u624b\u6027\u6e90\u5408\u6210\u529f\u80fd\u6027\u9ad8\u5206\u5b50\u6750\u6599\u3002
\n\u5178\u578b\u5e94\u7528\u6848\u4f8b\u5305\u62ec\u4f5c\u4e3a\u6fc0\u9176\u6291\u5236\u5242\u7684\u6838\u5fc3\u7247\u6bb5\uff0c\u6216\u7528\u4e8e\u6784\u5efa\u7a33\u5b9a\u80bd\u7c7b\u4f3c\u7269\u4ee5\u589e\u5f3a\u4ee3\u8c22\u7a33\u5b9a\u6027\u3002<\/p>\n

4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u3001\u5e72\u71e5\u907f\u5149\u6761\u4ef6\u4e0b\u957f\u671f\u50a8\u5b58\uff0c\u77ed\u671f\u4f7f\u7528\u53ef\u7f6e\u4e8e4\u00b0C\u73af\u5883\u3002\u5f00\u5c01\u540e\u9700\u5145\u5165\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u5bc6\u5c01\u4fdd\u5b58\uff0c\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u73af\u5883\u4e0b\u64cd\u4f5c\uff0c\u6eb6\u89e3\u63a8\u8350\u4f7f\u7528\u65e0\u6c34DMSO\uff08\u6d53\u5ea6\u226410 mM\uff09\uff0c\u540e\u7eed\u53ef\u7528\u7f13\u51b2\u6db2\u7a00\u91ca\u3002\u6ce8\u610f\u907f\u514d\u4e0e\u5f3a\u6c27\u5316\u5242\u6216\u9178\u78b1\u76f4\u63a5\u63a5\u89e6\u3002<\/p>\n

5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u901a\u8fc7HPLC\u548cNMR\u53cc\u91cd\u9a8c\u8bc1\uff0c\u786e\u4fdd\u5316\u5b66\u7eaf\u5ea6\u548c\u7acb\u4f53\u6784\u578b\u51c6\u786e\u6027\u3002MSDS\u6570\u636e\u663e\u793a\u5176\u5177\u6709\u523a\u6fc0\u6027\uff0c\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u9632\u62a4\u624b\u5957\u3001\u62a4\u76ee\u955c\u53ca\u5b9e\u9a8c\u670d\u3002\u82e5\u63a5\u89e6\u76ae\u80a4\u6216\u773c\u775b\uff0c\u5e94\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5904\u7f6e\u9700\u7b26\u5408\u6709\u673a\u6709\u5bb3\u5316\u5b66\u54c1\u89c4\u8303\uff0c\u7981\u6b62\u76f4\u63a5\u6392\u653e\u81f3\u73af\u5883\u4e2d\u3002 <\/p>\n

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