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\u4ea7\u54c1\u8bf4\u660e <\/p>\n

1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\nFMOC-D-3,4-\u4e8c\u6c2f\u82ef\u4e19\u6c28\u9178\uff08Fmoc-3,4-dichloro-D-phenylalanine\uff09\u662f\u4e00\u79cd\u91cd\u8981\u7684\u6c28\u57fa\u9178\u884d\u751f\u7269\uff0c\u5316\u5b66\u5f0f\u4e3aC24H19Cl2NO4\uff0c\u5206\u5b50\u91cf\u4e3a456.318\uff0cCAS\u53f7\u4e3a177966-58-4\u3002\u8be5\u5316\u5408\u7269\u4ee5Fmoc\uff089-\u82b4\u7532\u6c27\u7fb0\u57fa\uff09\u4e3a\u4fdd\u62a4\u57fa\uff0cD-\u6784\u578b\u7684\u82ef\u4e19\u6c28\u91783,4\u4f4d\u88ab\u6c2f\u539f\u5b50\u53d6\u4ee3\uff0c\u5f62\u6210\u5177\u6709\u7279\u5b9a\u7acb\u4f53\u7ed3\u6784\u7684\u4fee\u9970\u6c28\u57fa\u9178\u3002\u5176\u7eaf\u5ea6\u9ad8\u4e8e96%\uff0c\u9002\u7528\u4e8e\u9ad8\u7cbe\u5ea6\u751f\u7269\u5316\u5b66\u7814\u7a76\u3002 <\/p>\n

2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u8be5\u5316\u5408\u7269\u5728\u80bd\u5408\u6210\u4e2d\u4f5c\u4e3a\u5173\u952e\u780c\u5757\uff0c\u5176D-\u6784\u578b\u53ca\u6c2f\u53d6\u4ee3\u57fa\u8d4b\u4e88\u80bd\u94fe\u72ec\u7279\u7684\u7a7a\u95f4\u4f4d\u963b\u548c\u758f\u6c34\u6027\uff0c\u53ef\u8c03\u8282\u80bd\u7684\u7a33\u5b9a\u6027\u4e0e\u751f\u7269\u6d3b\u6027\u30023,4-\u4e8c\u6c2f\u82ef\u73af\u7ed3\u6784\u589e\u5f3a\u4e86\u5206\u5b50\u4e0e\u9776\u86cb\u767d\u7684\u76f8\u4e92\u4f5c\u7528\uff0c\u5e38\u7528\u4e8e\u8bbe\u8ba1\u9176\u6291\u5236\u5242\u6216\u53d7\u4f53\u62ee\u6297\u5242\uff0c\u5728\u836f\u7269\u5f00\u53d1\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002 <\/p>\n

3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\nFMOC-D-3,4-\u4e8c\u6c2f\u82ef\u4e19\u6c28\u9178\u4e3b\u8981\u7528\u4e8e\u56fa\u76f8\u80bd\u5408\u6210\uff08SPPS\uff09\uff0c\u5c24\u5176\u9002\u7528\u4e8e\u6784\u5efa\u542b\u975e\u5929\u7136\u6c28\u57fa\u9178\u7684\u80bd\u94fe\u3002\u5176\u5e94\u7528\u9886\u57df\u5305\u62ec\uff1a
\n– \u836f\u7269\u7814\u53d1\uff1a\u4f5c\u4e3a\u6297\u80bf\u7624\u3001\u6297\u75c5\u6bd2\u80bd\u7c7b\u836f\u7269\u7684\u4fee\u9970\u5355\u5143
\n– \u7ed3\u6784\u751f\u7269\u5b66\uff1a\u7528\u4e8e\u5236\u5907X\u5c04\u7ebf\u6676\u4f53\u5b66\u6216NMR\u7814\u7a76\u7684\u6a21\u578b\u80bd
\n– \u6750\u6599\u79d1\u5b66\uff1a\u5408\u6210\u529f\u80fd\u6027\u751f\u7269\u9ad8\u5206\u5b50\u6750\u6599 <\/p>\n

4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u3001\u907f\u5149\u3001\u5e72\u71e5\u6761\u4ef6\u4e0b\u50a8\u5b58\uff0c\u957f\u671f\u4fdd\u5b58\u9700\u5145\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u73af\u5883\u4e2d\u64cd\u4f5c\uff0c\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u8868\u660e\uff0c\u8be5\u4ea7\u54c1\u6613\u6eb6\u4e8eDMF\u3001DMSO\u7b49\u6781\u6027\u6709\u673a\u6eb6\u5242\uff0c\u4e0d\u63a8\u8350\u76f4\u63a5\u7528\u6c34\u6eb6\u89e3\u3002 <\/p>\n

5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u7ecfHPLC\u68c0\u6d4b\u7eaf\u5ea6>96%\uff0cMS\u53caNMR\u9a8c\u8bc1\u7ed3\u6784\u51c6\u786e\u6027\u3002\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u9632\u62a4\u624b\u5957\u53ca\u62a4\u76ee\u955c\uff0c\u907f\u514d\u5438\u5165\u6216\u63a5\u89e6\u76ae\u80a4\u3002\u5982\u610f\u5916\u63a5\u89e6\uff0c\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5e94\u4f5c\u4e3a\u6709\u5bb3\u5316\u5b66\u7269\u8d28\u5904\u7406\uff0c\u9075\u5b88\u5f53\u5730\u73af\u4fdd\u6cd5\u89c4\u3002 <\/p>\n

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