1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u54cc\u6cca\u6eb4\u70f7\uff081,1′-(Piperazine-1,4-diyl)bis(3-bromopropan-1-one)\uff0cCAS\u53f754-91-1\uff09\u662f\u4e00\u79cd\u6709\u673a\u6eb4\u5316\u7269\uff0c\u5206\u5b50\u5f0f\u4e3aC10H16Br2N2O2\uff0c\u5206\u5b50\u91cf356.054\u3002\u8be5\u5316\u5408\u7269\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u7c89\u672b\uff0c\u7eaf\u5ea6\u901a\u5e38\u9ad8\u4e8e96%\u3002\u5176\u7ed3\u6784\u4e2d\u542b\u6709\u54cc\u55ea\u73af\u548c\u4e24\u4e2a\u6eb4\u4e19\u9170\u57fa\uff0c\u8d4b\u4e88\u5176\u72ec\u7279\u7684\u53cd\u5e94\u6d3b\u6027\u548c\u751f\u7269\u5316\u5b66\u529f\u80fd\u3002\u54cc\u6cca\u6eb4\u70f7\u5728\u5e38\u6e29\u4e0b\u7a33\u5b9a\uff0c\u4f46\u9700\u907f\u5149\u4fdd\u5b58\uff0c\u56e0\u5176\u6eb4\u4ee3\u70f7\u57fa\u7ed3\u6784\u53ef\u80fd\u5bf9\u5149\u654f\u611f\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u54cc\u6cca\u6eb4\u70f7\u4f5c\u4e3a\u4e00\u79cd\u53cc\u529f\u80fd\u70f7\u57fa\u5316\u8bd5\u5242\uff0c\u80fd\u591f\u4e0e\u751f\u7269\u5927\u5206\u5b50\uff08\u5982\u86cb\u767d\u8d28\u3001\u6838\u9178\uff09\u4e2d\u7684\u4eb2\u6838\u57fa\u56e2\uff08\u5982\u6c28\u57fa\u3001\u5def\u57fa\uff09\u53d1\u751f\u5171\u4ef7\u7ed3\u5408\u3002\u8fd9\u4e00\u7279\u6027\u4f7f\u5176\u5728\u751f\u7269\u5316\u5b66\u7814\u7a76\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\uff0c\u5c24\u5176\u5728\u86cb\u767d\u8d28\u4ea4\u8054\u3001\u9176\u6d3b\u6027\u6291\u5236\u548c\u836f\u7269\u8f7d\u4f53\u4fee\u9970\u7b49\u9886\u57df\u3002\u5176\u54cc\u55ea\u73af\u7ed3\u6784\u8fd8\u63d0\u4f9b\u4e86\u826f\u597d\u7684\u6c34\u6eb6\u6027\u548c\u5206\u5b50\u53ef\u5851\u6027\uff0c\u9002\u5408\u7528\u4e8e\u8bbe\u8ba1\u9776\u5411\u9012\u9001\u7cfb\u7edf\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u54cc\u6cca\u6eb4\u70f7\u5e7f\u6cdb\u5e94\u7528\u4e8e\u836f\u7269\u7814\u53d1\u548c\u751f\u7269\u6807\u8bb0\u9886\u57df\u3002\u5728\u6297\u764c\u836f\u7269\u5f00\u53d1\u4e2d\uff0c\u5b83\u53ef\u4f5c\u4e3a\u4ea4\u8054\u5242\u7528\u4e8e\u6784\u5efa\u6297\u4f53-\u836f\u7269\u5076\u8054\u7269\uff08ADC\uff09\uff0c\u589e\u5f3a\u836f\u7269\u7684\u9776\u5411\u6027\u3002\u6b64\u5916\uff0c\u8be5\u5316\u5408\u7269\u8fd8\u53ef\u7528\u4e8e\u86cb\u767d\u8d28\u56fa\u5b9a\u5316\u3001\u6838\u9178\u4fee\u9970\u4ee5\u53ca\u9ad8\u5206\u5b50\u6750\u6599\u7684\u5408\u6210\u3002\u5728\u5b9e\u9a8c\u5ba4\u7814\u7a76\u4e2d\uff0c\u54cc\u6cca\u6eb4\u70f7\u5e38\u7528\u4e8e\u63a2\u7d22\u86cb\u767d\u8d28-\u86cb\u767d\u8d28\u76f8\u4e92\u4f5c\u7528\u6216\u9176\u6d3b\u6027\u8c03\u63a7\u673a\u5236\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u672c\u54c1\u5e94\u5bc6\u5c01\u4fdd\u5b58\u4e8e2-8\u2103\u7684\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u907f\u514d\u4e0e\u6e7f\u6c14\u6216\u5f3a\u6c27\u5316\u5242\u63a5\u89e6\u3002\u4f7f\u7528\u65f6\u9700\u5728\u901a\u98ce\u6a71\u4e2d\u64cd\u4f5c\uff0c\u4f69\u6234\u9632\u62a4\u624b\u5957\u548c\u62a4\u76ee\u955c\u3002\u5efa\u8bae\u73b0\u914d\u73b0\u7528\uff0c\u6eb6\u89e3\u65f6\u53ef\u9009\u62e9\u6781\u6027\u6eb6\u5242\u5982DMSO\u6216\u4e59\u9187\u3002\u957f\u671f\u50a8\u5b58\u53ef\u80fd\u5bfc\u81f4\u90e8\u5206\u964d\u89e3\uff0c\u4f7f\u7528\u524d\u9700\u901a\u8fc7HPLC\u6216TLC\u9a8c\u8bc1\u7eaf\u5ea6\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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