\u4ed6\u5361\u897f\u59a5\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u4ed6\u5361\u897f\u59a5\uff08\u5316\u5b66\u540d\u79f0\uff1a(1R,3S,5Z)-5-[(2E)-2-[(1R,3aS,7aR)-1-[(2R,5R)-5-hydroxy-6-methylheptan-2-yl]-7a-methyl-2,3,3a,5,6,7-hexahydro-1H-inden-4-ylidene]ethylidene]-4-methylidenecyclohexane-1,3-diol\uff09\u662f\u4e00\u79cd\u9ad8\u7eaf\u5ea6\u751f\u5316\u8bd5\u5242\uff0cCAS\u53f7\u4e3a57333-96-7\uff0c\u5206\u5b50\u5f0f\u4e3aC27H44O3\uff0c\u5206\u5b50\u91cf\u4e3a416.637\u3002\u672c\u54c1\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\uff0c\u7eaf\u5ea6\u8d85\u8fc796%\uff0c\u5177\u6709\u7279\u5b9a\u7684\u7acb\u4f53\u6784\u578b\uff0c\u5c5e\u4e8e\u4e8c\u841c\u7c7b\u5316\u5408\u7269\u884d\u751f\u7269\u3002\u5176\u5316\u5b66\u7ed3\u6784\u5305\u542b\u591a\u73af\u4f53\u7cfb\u548c\u7f9f\u57fa\u5b98\u80fd\u56e2\uff0c\u8d4b\u4e88\u5176\u72ec\u7279\u7684\u4eb2\u8102\u6027\u548c\u751f\u7269\u6d3b\u6027\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4ed6\u5361\u897f\u59a5\u4f5c\u4e3a\u7ef4\u751f\u7d20D3\u7c7b\u4f3c\u7269\u7684\u4e2d\u95f4\u4f53\u6216\u4ee3\u8c22\u4ea7\u7269\uff0c\u5728\u9499\u78f7\u4ee3\u8c22\u8c03\u8282\u4e2d\u53d1\u6325\u6f5c\u5728\u4f5c\u7528\u3002\u5176\u7ed3\u6784\u4e2d\u7684\u5171\u8f6d\u53cc\u952e\u548c\u7f9f\u57fa\u5316\u4fa7\u94fe\u53ef\u80fd\u53c2\u4e0e\u6838\u53d7\u4f53\u7ed3\u5408\uff0c\u5f71\u54cd\u7ec6\u80de\u5206\u5316\u4e0e\u589e\u6b96\u76f8\u5173\u4fe1\u53f7\u901a\u8def\u3002\u5728\u7814\u7a76\u4e2d\uff0c\u8be5\u5316\u5408\u7269\u5e38\u7528\u4e8e\u63a2\u7d22\u7c7b\u56fa\u9187\u6fc0\u7d20\u53d7\u4f53\u7684\u914d\u4f53-\u53d7\u4f53\u76f8\u4e92\u4f5c\u7528\u673a\u5236\uff0c\u6216\u4f5c\u4e3a\u5408\u6210\u66f4\u590d\u6742\u6d3b\u6027\u5206\u5b50\u7684\u5173\u952e\u780c\u5757\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u4ed6\u5361\u897f\u59a5\u4e3b\u8981\u5e94\u7528\u4e8e\u836f\u7269\u7814\u53d1\u9886\u57df\uff0c\u5c24\u5176\u5728\u7ef4\u751f\u7d20D\u7c7b\u4f3c\u7269\u5408\u6210\u4e2d\u4f5c\u4e3a\u91cd\u8981\u524d\u4f53\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a\u4f5c\u4e3a\u6807\u51c6\u54c1\u7528\u4e8eHPLC\u6216LC-MS\u65b9\u6cd5\u5f00\u53d1\uff1b\u5728\u4ee3\u8c22\u7814\u7a76\u4e2d\u4f5c\u4e3a\u53c2\u7167\u7269\u8d28\uff1b\u7528\u4e8e\u9aa8\u8d28\u758f\u677e\u6216\u514d\u75ab\u8c03\u8282\u76f8\u5173\u65b0\u836f\u7684\u6d3b\u6027\u7b5b\u9009\u3002\u6b64\u5916\uff0c\u5728\u751f\u5316\u673a\u7406\u7814\u7a76\u4e2d\u53ef\u7528\u4e8e\u63a2\u7a76\u8102\u6eb6\u6027\u4fe1\u53f7\u5206\u5b50\u7684\u819c\u7a7f\u900f\u6027\u4e0e\u7ec6\u80de\u5185\u8f6c\u8fd0\u7279\u6027\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u672c\u54c1\u9700\u4e25\u683c\u907f\u5149\u4fdd\u5b58\u4e8e-20\u2103\u4ee5\u4e0b\u60f0\u6027\u6c14\u4f53\u73af\u5883\u4e2d\uff0c\u5f00\u5c01\u540e\u5efa\u8bae\u5206\u88c5\u4f7f\u7528\u4ee5\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002\u4f7f\u7528\u524d\u9700\u5e73\u8861\u81f3\u5ba4\u6e29\u5e76\u77ed\u6682\u6c2e\u6c14\u5439\u626b\u3002\u6eb6\u89e3\u65f6\u63a8\u8350\u9009\u7528\u65e0\u6c34\u4e59\u9187\u6216DMSO\u4f5c\u4e3a\u6eb6\u5242\uff0c\u914d\u5236\u540e\u6eb6\u6db2\u9700\u73b0\u914d\u73b0\u7528\u3002\u5b9e\u9a8c\u64cd\u4f5c\u5e94\u5728\u60f0\u6027\u6c14\u6c1b\u624b\u5957\u7bb1\u6216\u901a\u98ce\u6a71\u4e2d\u8fdb\u884c\uff0c\u907f\u514d\u63a5\u89e6\u5f3a\u6c27\u5316\u5242\u4e0e\u9178\u6027\u6761\u4ef6\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u54c1\u901a\u8fc7HPLC-UV\u53ca\u8d28\u8c31\u8054\u7528\u6280\u672f\u8fdb\u884c\u7eaf\u5ea6\u9a8c\u8bc1\uff0c\u6b8b\u7559\u6eb6\u5242\u7b26\u5408ICH\u6807\u51c6\u3002\u5b89\u5168\u6570\u636e\u8868\u660e\uff0c\u5176\u6025\u6027\u6bd2\u6027\u8f83\u4f4e\uff08LD50>2000 mg\/kg\uff0c\u5927\u9f20\u53e3\u670d\uff09\uff0c\u4f46\u4ecd\u9700\u4f69\u6234\u9632\u62a4\u624b\u5957\u4e0e\u62a4\u76ee\u955c\u64cd\u4f5c\u3002\u5e9f\u5f03\u7269\u5e94\u4f5c\u4e3a\u6709\u673a\u5364\u5316\u7269\u5904\u7406\uff0c\u4e0d\u53ef\u76f4\u63a5\u6392\u653e\u3002\u8be6\u7ec6\u6bd2\u7406\u5b66\u6570\u636e\u8bf7\u53c2\u9605\u968f\u9644\u7684MSDS\u6587\u4ef6\u3002 <\/p>\n
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