7-\u6eb4-3,4-\u4e8c\u6c22-2H-\u5f02\u55b9\u5549-1-\u916e\u4ea7\u54c1\u8bf4\u660e <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n7-\u6eb4-3,4-\u4e8c\u6c22-2H-\u5f02\u55b9\u5549-1-\u916e\uff08\u82f1\u6587\u540d\u79f0\uff1a7-bromo-3,4-dihydro-2h-isoquinolin-1-one\uff09\u662f\u4e00\u79cd\u6709\u673a\u6eb4\u5316\u7269\uff0cCAS\u53f7\u4e3a891782-60-8\uff0c\u5206\u5b50\u5f0f\u4e3aC9H8BrNO\uff0c\u5206\u5b50\u91cf\u4e3a226.07\u3002\u8be5\u5316\u5408\u7269\u4e3a\u767d\u8272\u81f3\u6de1\u9ec4\u8272\u7ed3\u6676\u6216\u7c89\u672b\uff0c\u7eaf\u5ea6\u9ad8\u4e8e96%\uff0c\u5177\u6709\u5178\u578b\u7684\u5f02\u55b9\u5549\u916e\u9aa8\u67b6\u7ed3\u6784\uff0c\u51767\u4f4d\u6eb4\u53d6\u4ee3\u57fa\u8d4b\u4e88\u5176\u72ec\u7279\u7684\u53cd\u5e94\u6d3b\u6027\u3002\u8be5\u7269\u8d28\u53ef\u6eb6\u4e8e\u5e38\u89c1\u6709\u673a\u6eb6\u5242\u5982\u4e8c\u7532\u57fa\u4e9a\u781c\uff08DMSO\uff09\u3001\u7532\u9187\u548c\u6c2f\u4eff\uff0c\u4f46\u5728\u6c34\u4e2d\u6eb6\u89e3\u5ea6\u8f83\u4f4e\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u5f02\u55b9\u5549\u916e\u7c7b\u884d\u751f\u7269\uff0c\u8be5\u5316\u5408\u7269\u5728\u751f\u7269\u5316\u5b66\u7814\u7a76\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002\u5176\u7ed3\u6784\u4e2d\u7684\u6eb4\u539f\u5b50\u53ef\u4f5c\u4e3a\u6d3b\u6027\u4f4d\u70b9\u53c2\u4e0e\u5076\u8054\u53cd\u5e94\uff0c\u5e38\u7528\u4e8e\u6784\u5efa\u66f4\u590d\u6742\u7684\u6742\u73af\u5316\u5408\u7269\u3002\u6b64\u5916\uff0c\u5f02\u55b9\u5549\u916e\u9aa8\u67b6\u662f\u591a\u79cd\u751f\u7269\u6d3b\u6027\u5206\u5b50\u7684\u6838\u5fc3\u7ed3\u6784\uff0c\u5728\u836f\u7269\u7814\u53d1\u4e2d\u5e38\u7528\u4e8e\u63a2\u7d22\u795e\u7ecf\u8c03\u8282\u3001\u6297\u708e\u6216\u6297\u80bf\u7624\u6d3b\u6027\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u4ea7\u54c1\u4e3b\u8981\u5e94\u7528\u4e8e\u533b\u836f\u4e2d\u95f4\u4f53\u5408\u6210\u548c\u6709\u673a\u5316\u5b66\u7814\u7a76\u9886\u57df\u3002\u5177\u4f53\u7528\u9014\u5305\u62ec\uff1a\u4f5c\u4e3a\u5173\u952e\u4e2d\u95f4\u4f53\u7528\u4e8e\u5408\u6210\u5c0f\u5206\u5b50\u6291\u5236\u5242\u6216\u53d7\u4f53\u914d\u4f53\uff1b\u5728\u836f\u7269\u53d1\u73b0\u4e2d\u7528\u4e8e\u7ed3\u6784\u4fee\u9970\u4e0e\u6784\u6548\u5173\u7cfb\u7814\u7a76\uff1b\u5728\u6750\u6599\u79d1\u5b66\u4e2d\u7528\u4e8e\u5236\u5907\u529f\u80fd\u6027\u6709\u673a\u5206\u5b50\u3002\u5176\u6eb4\u53d6\u4ee3\u57fa\u53ef\u901a\u8fc7 Suzuki \u6216 Buchwald-Hartwig \u7b49\u5076\u8054\u53cd\u5e94\u8fdb\u4e00\u6b65\u884d\u751f\u5316\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728-20\u00b0C\u4e0b\u907f\u5149\u4fdd\u5b58\uff0c\u957f\u671f\u50a8\u5b58\u9700\u5145\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u3002\u5f00\u5c01\u540e\u5e94\u5bc6\u5c01\u9632\u6f6e\uff0c\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002\u4f7f\u7528\u65f6\u9700\u5728\u901a\u98ce\u6a71\u4e2d\u64cd\u4f5c\uff0c\u4f69\u6234\u9632\u62a4\u624b\u5957\u548c\u62a4\u76ee\u955c\u3002\u6eb6\u89e3\u63a8\u8350\u4f7f\u7528\u65e0\u6c34DMSO\uff0c\u914d\u5236\u6eb6\u6db2\u5efa\u8bae\u73b0\u914d\u73b0\u7528\uff0c\u907f\u514d\u957f\u65f6\u95f4\u66b4\u9732\u4e8e\u7a7a\u6c14\u4e2d\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u901a\u8fc7HPLC\u68c0\u6d4b\u7eaf\u5ea6\u226596%\uff0c\u5e76\u63d0\u4f9b\u8d28\u8c31\u548c\u6838\u78c1\u6570\u636e\u652f\u6301\u3002\u5b89\u5168\u4fe1\u606f\uff1a\u53ef\u80fd\u5bf9\u773c\u775b\u3001\u76ae\u80a4\u548c\u547c\u5438\u7cfb\u7edf\u9020\u6210\u523a\u6fc0\uff0c\u64cd\u4f5c\u65f6\u5e94\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u3002\u5982\u4e0d\u614e\u63a5\u89e6\uff0c\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\u5e76\u5c31\u533b\u3002\u5e9f\u5f03\u7269\u5904\u7406\u9700\u7b26\u5408\u5f53\u5730\u73af\u4fdd\u6cd5\u89c4\u3002\u8fd0\u8f93\u5206\u7c7b\u4e3a\u975e\u5371\u9669\u54c1\uff0c\u4f46\u5efa\u8bae\u6309\u4e00\u822c\u5316\u5b66\u54c1\u89c4\u8303\u8fd0\u8f93\u3002 <\/p>\n
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