2-\u6c30\u57fa-3-(2-\u6eb4\u82ef\u57fa)\u4e19\u70ef\u9178\u4e59\u8102\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u5316\u5b66\u540d\u79f0\u4e3a\u03b1-Cyan-o-bromzimtsaeureaethylester\uff0cCAS\u53f7\u4e3a59803-32-6\uff0c\u5206\u5b50\u5f0f\u4e3aC12H10BrNO2\uff0c\u5206\u5b50\u91cf280.117\uff0c\u662f\u4e00\u79cd\u9ad8\u7eaf\u5ea6\uff08>96%\uff09\u7684\u6eb4\u82ef\u57fa\u4e19\u70ef\u9178\u916f\u884d\u751f\u7269\u3002\u5176\u7ed3\u6784\u4e2d\u7684\u6c30\u57fa\u548c\u6eb4\u82ef\u57fa\u8d4b\u4e88\u8be5\u5316\u5408\u7269\u72ec\u7279\u7684\u7535\u5b50\u6548\u5e94\u4e0e\u7a7a\u95f4\u4f4d\u963b\uff0c\u4f7f\u5176\u5728\u6781\u6027\u6709\u673a\u6eb6\u5242\uff08\u5982DMF\u3001\u4e59\u8148\uff09\u4e2d\u5177\u6709\u826f\u597d\u7684\u6eb6\u89e3\u6027\uff0c\u800c\u5728\u6c34\u4e2d\u6eb6\u89e3\u5ea6\u8f83\u4f4e\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u03b1,\u03b2-\u4e0d\u9971\u548c\u7fb0\u57fa\u5316\u5408\u7269\uff0c\u8be5\u5206\u5b50\u53ef\u901a\u8fc7\u8fc8\u514b\u5c14\u52a0\u6210\u53cd\u5e94\u4e0e\u751f\u7269\u5927\u5206\u5b50\u4e2d\u7684\u4eb2\u6838\u57fa\u56e2\uff08\u5982\u5def\u57fa\u3001\u6c28\u57fa\uff09\u7ed3\u5408\uff0c\u5728\u6291\u5236\u5242\u8bbe\u8ba1\u548c\u86cb\u767d\u8d28\u6807\u8bb0\u9886\u57df\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002\u6eb4\u539f\u5b50\u7684\u5f15\u5165\u8fdb\u4e00\u6b65\u589e\u5f3a\u4e86\u5176\u4f5c\u4e3a\u4eb2\u7535\u8bd5\u5242\u7684\u6d3b\u6027\uff0c\u4f7f\u5176\u6210\u4e3a\u5408\u6210\u542b\u6eb4\u6742\u73af\u5316\u5408\u7269\u7684\u5173\u952e\u4e2d\u95f4\u4f53\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u4ea7\u54c1\u5e7f\u6cdb\u5e94\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a
\n3.1 \u836f\u7269\u5316\u5b66\uff1a\u7528\u4e8e\u6784\u5efa\u6297\u80bf\u7624\u548c\u6297\u708e\u836f\u7269\u7684\u6838\u5fc3\u9aa8\u67b6\uff0c\u5982\u4f5c\u4e3a\u6fc0\u9176\u6291\u5236\u5242\u7684\u5408\u6210\u524d\u4f53\u3002
\n3.2 \u6750\u6599\u79d1\u5b66\uff1a\u53c2\u4e0e\u5236\u5907\u5149\u7535\u529f\u80fd\u6750\u6599\uff0c\u7279\u522b\u662f\u542b\u6eb4\u5171\u8f6d\u805a\u5408\u7269\u3002
\n3.3 \u751f\u7269\u6807\u8bb0\uff1a\u901a\u8fc7\u6eb4\u539f\u5b50\u7684\u7279\u5f02\u6027\u53d6\u4ee3\u53cd\u5e94\uff0c\u53ef\u7528\u4e8e\u8367\u5149\u63a2\u9488\u7684\u4fee\u9970\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5728\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c29\u6c14\uff09\u4fdd\u62a4\u4e0b\u5bc6\u5c01\u4fdd\u5b58\uff0c\u50a8\u5b58\u6e29\u5ea6-20\u00b0C\uff0c\u907f\u5149\u9632\u6f6e\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u73af\u5883\u4e0b\u64cd\u4f5c\uff0c\u907f\u514d\u4e0e\u5f3a\u6c27\u5316\u5242\u6216\u8fd8\u539f\u5242\u63a5\u89e6\u3002\u6eb6\u89e3\u63a8\u8350\u4f7f\u7528\u65e0\u6c34\u7ea7\u6709\u673a\u6eb6\u5242\uff0c\u5e76\u5efa\u8bae\u73b0\u914d\u73b0\u7528\u4ee5\u4fdd\u8bc1\u53cd\u5e94\u6d3b\u6027\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u7ecfHPLC\u68c0\u6d4b\u7eaf\u5ea6>96%\uff0cMS\u548cNMR\u9a8c\u8bc1\u7ed3\u6784\u3002\u5b89\u5168\u6570\u636e\u5982\u4e0b\uff1a
\n5.1 \u5371\u5bb3\u6027\uff1a\u53ef\u80fd\u5f15\u8d77\u76ae\u80a4\u523a\u6fc0\u548c\u4e25\u91cd\u773c\u775b\u635f\u4f24\uff0c\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u62a4\u76ee\u955c\u548c\u9632\u5316\u624b\u5957\u3002
\n5.2 \u5e94\u6025\u5904\u7406\uff1a\u63a5\u89e6\u76ae\u80a4\u540e\u7acb\u5373\u7528\u5927\u91cf\u6e05\u6c34\u51b2\u6d17\uff0c\u82e5\u5438\u5165\u9700\u8f6c\u79fb\u81f3\u7a7a\u6c14\u65b0\u9c9c\u5904\u3002
\n5.3 \u5e9f\u5f03\u7269\u5904\u7f6e\uff1a\u6309\u5371\u9669\u5316\u5b66\u54c1\u89c4\u8303\u5904\u7406\uff0c\u4e0d\u53ef\u76f4\u63a5\u6392\u5165\u4e0b\u6c34\u9053\u3002 <\/p>\n
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