4-O-\u82c4\u57fa 1-O-\u53d4\u4e01\u57fa 4-\u5f02\u4e19\u57fa\u54cc\u5576-1,4-\u4e8c\u7fa7\u9178\u916f\uff08n-boc-4-\u5f02\u4e19\u57fa-4-\u54cc\u5576\u7fa7\u9178\u82c4\u916f\uff09\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\uff0c\u5316\u5b66\u540d\u79f0\u4e3a4-O-benzyl 1-O-tert-butyl 4-propan-2-ylpiperidine-1,4-dicarboxylate\uff0cCAS\u53f71226776-80-2\uff0c\u5206\u5b50\u5f0fC21H31NO4\uff0c\u5206\u5b50\u91cf361.475\u3002\u5176\u7ed3\u6784\u540c\u65f6\u5305\u542b\u53d4\u4e01\u6c27\u7fb0\u57fa\uff08Boc\uff09\u4fdd\u62a4\u57fa\u56e2\u548c\u82c4\u916f\u57fa\u56e2\uff0c\u7eaf\u5ea6\u7ecfHPLC\u9a8c\u8bc1\u226596%\u3002\u8be5\u5316\u5408\u7269\u5728\u5e38\u6e29\u4e0b\u7a33\u5b9a\uff0c\u6613\u6eb6\u4e8e\u6709\u673a\u6eb6\u5242\u5982\u4e8c\u6c2f\u7532\u70f7\u3001\u4e59\u9178\u4e59\u916f\uff0c\u5fae\u6eb6\u4e8e\u6c34\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u54cc\u5576\u7c7b\u884d\u751f\u7269\uff0c\u8be5\u5316\u5408\u7269\u662f\u836f\u7269\u5316\u5b66\u4e2d\u5173\u952e\u7684\u4e2d\u95f4\u4f53\uff0c\u5176Boc\u4fdd\u62a4\u57fa\u53ef\u5728\u9178\u6027\u6761\u4ef6\u4e0b\u9009\u62e9\u6027\u8131\u9664\uff0c\u800c\u82c4\u916f\u57fa\u53ef\u901a\u8fc7\u6c22\u5316\u8fd8\u539f\u88c2\u89e3\u3002\u8fd9\u79cd\u53cc\u91cd\u4fdd\u62a4\u7279\u6027\u4f7f\u5176\u5e7f\u6cdb\u5e94\u7528\u4e8e\u591a\u6b65\u6709\u673a\u5408\u6210\uff0c\u7279\u522b\u662f\u6784\u5efa\u542b\u54cc\u5576\u73af\u7684\u6d3b\u6027\u5206\u5b50\u9aa8\u67b6\uff0c\u5982\u795e\u7ecf\u53d7\u4f53\u8c03\u8282\u5242\u548c\u9176\u6291\u5236\u5242\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u4e3b\u8981\u5e94\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a
\n\uff081\uff09\u533b\u836f\u7814\u53d1\uff1a\u7528\u4e8e\u5408\u6210\u6297\u80bf\u7624\u3001\u6297\u6291\u90c1\u53ca\u9547\u75db\u7c7b\u836f\u7269\u524d\u4f53\uff1b
\n\uff082\uff09\u4e0d\u5bf9\u79f0\u50ac\u5316\uff1a\u4f5c\u4e3a\u624b\u6027\u914d\u4f53\u7684\u5408\u6210\u780c\u5757\uff1b
\n\uff083\uff09\u6750\u6599\u79d1\u5b66\uff1a\u53c2\u4e0e\u5236\u5907\u529f\u80fd\u6027\u9ad8\u5206\u5b50\u5355\u4f53\u3002
\n\u5178\u578b\u7528\u9014\u5305\u62ec\u901a\u8fc7Boc\u8131\u4fdd\u62a4\u540e\u8fdb\u4e00\u6b65\u5b98\u80fd\u56e2\u5316\uff0c\u6216\u7ecf\u6c22\u89e3\u53cd\u5e94\u751f\u6210\u6e38\u79bb\u7fa7\u9178\u884d\u751f\u7269\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5bc6\u5c01\u4fdd\u5b58\u4e8e-20\u2103\u81f34\u2103\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u907f\u514d\u5149\u7167\u53ca\u6f6e\u6e7f\u3002\u5f00\u5c01\u540e\u9700\u5145\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u3002\u4f7f\u7528\u65f6\u5e94\u5728\u901a\u98ce\u6a71\u4e2d\u64cd\u4f5c\uff0c\u4f69\u6234\u9632\u62a4\u624b\u5957\u53ca\u62a4\u76ee\u955c\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u63a8\u8350\u4f18\u5148\u4f7f\u7528\u65e0\u6c34DMF\u6216THF\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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