2-\u6c28\u57fa-5-Cbz-4,5,6,7-\u56db\u6c22\u567b\u5511\u5e76[5,4-c]\u5421\u5576\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\uff0c\u5316\u5b66\u540d\u79f02-Amino-5-Cbz-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine\uff0cCAS\u53f71141669-69-3\uff0c\u5206\u5b50\u5f0fC14H15N3O2S\uff0c\u5206\u5b50\u91cf289.353\u3002\u5176\u7ed3\u6784\u5305\u542b\u567b\u5511\u5e76\u5421\u5576\u9aa8\u67b6\u548cCbz\u4fdd\u62a4\u57fa\u56e2\uff0c\u7eaf\u5ea6\u7ecfHPLC\u9a8c\u8bc1\u226596%\u3002\u8be5\u5316\u5408\u7269\u5728\u6709\u673a\u6eb6\u5242\u5982DMSO\u3001\u7532\u9187\u4e2d\u5177\u6709\u4e2d\u7b49\u6eb6\u89e3\u6027\uff0c\u9700\u907f\u5149\u4fdd\u5b58\u4ee5\u9632\u964d\u89e3\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u6742\u73af\u5316\u5408\u7269\uff0c\u5176\u567b\u5511\u5e76\u5421\u5576\u7ed3\u6784\u662f\u836f\u7269\u5316\u5b66\u4e2d\u5e38\u89c1\u7684\u836f\u6548\u56e2\uff0c\u80fd\u591f\u53c2\u4e0e\u591a\u79cd\u751f\u7269\u6d3b\u6027\u5206\u5b50\u7684\u5408\u6210\u3002Cbz\u4fdd\u62a4\u57fa\u56e2\u53ef\u9009\u62e9\u6027\u8131\u9664\uff0c\u4f7f\u5176\u6210\u4e3a\u6784\u5efa\u590d\u6742\u751f\u7269\u78b1\u548c\u86cb\u767d\u9176\u6291\u5236\u5242\u7684\u5173\u952e\u4e2d\u95f4\u4f53\u3002\u8be5\u5206\u5b50\u5728\u8c03\u8282\u7ec6\u80de\u4fe1\u53f7\u901a\u8def\u548c\u9176\u6d3b\u6027\u65b9\u9762\u5177\u6709\u6f5c\u5728\u5e94\u7528\u4ef7\u503c\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u672c\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u533b\u836f\u7814\u53d1\u9886\u57df\uff0c\u5177\u4f53\u5305\u62ec\uff1a1\uff09\u4f5c\u4e3a\u6fc0\u9176\u6291\u5236\u5242\u6216GPCR\u914d\u4f53\u7684\u5408\u6210\u524d\u4f53\uff1b2\uff09\u7528\u4e8e\u6784\u5efa\u6297\u80bf\u7624\u6216\u6297\u611f\u67d3\u836f\u7269\u7684\u6838\u5fc3\u9aa8\u67b6\uff1b3\uff09\u5728\u5316\u5b66\u751f\u7269\u5b66\u7814\u7a76\u4e2d\u7528\u4e8e\u63a2\u9488\u5206\u5b50\u5f00\u53d1\u3002\u5176\u9ad8\u7eaf\u5ea6\u7279\u6027\u7279\u522b\u9002\u5408\u5c0f\u5206\u5b50\u5e93\u6784\u5efa\u548c\u9ad8\u901a\u91cf\u7b5b\u9009\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u63a8\u8350\u50a8\u5b58\u4e8e-20\u00b0C\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u5145\u6c2e\u5bc6\u5c01\u4fdd\u5b58\uff0c\u6709\u6548\u671f24\u4e2a\u6708\u3002\u4f7f\u7528\u524d\u9700\u6062\u590d\u81f3\u5ba4\u6e29\u5e76\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002\u5b9e\u9a8c\u64cd\u4f5c\u5e94\u5728\u901a\u98ce\u6a71\u4e2d\u8fdb\u884c\uff0c\u5efa\u8bae\u4f69\u6234\u9632\u62a4\u624b\u5957\u548c\u62a4\u76ee\u955c\u3002\u6eb6\u89e3\u65f6\u4f18\u5148\u9009\u7528\u65e0\u6c34DMSO\uff0c\u914d\u5236\u6210\u6bcd\u6db2\u540e\u9700\u5206\u88c5\u4fdd\u5b58\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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