3-(3,4-\u4e8c\u7f9f\u57fa\u82ef\u57fa-2,5,6-d3)-L-\u4e19\u6c28\u9178\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n\u672c\u4ea7\u54c1\u4e3a\u6c18\u4ee3L-\u591a\u5df4\u884d\u751f\u7269\uff0c\u5316\u5b66\u540d\u79f0\u4e3a(2S)-2-\u6c28\u57fa-3-(2,3,6-\u4e09\u6c18\u4ee3-4,5-\u4e8c\u7f9f\u57fa\u82ef\u57fa)\u4e19\u9178\uff0c\u5206\u5b50\u5f0fC9H8D3NO4\uff0c\u5206\u5b50\u91cf200.206\u3002CAS\u767b\u8bb0\u53f753587-29-4\u660e\u786e\u6807\u8bc6\u5176\u552f\u4e00\u5316\u5b66\u7ed3\u6784\u3002\u8be5\u5316\u5408\u7269\u5728\u82ef\u73af2,5,6\u4f4d\u70b9\u5f15\u5165\u4e09\u4e2a\u6c18\u539f\u5b50\uff0c\u5f62\u6210\u7a33\u5b9a\u540c\u4f4d\u7d20\u6807\u8bb0\u7269\uff0c\u7eaf\u5ea6\u7ecfHPLC\u9a8c\u8bc1>96%\uff0c\u8868\u73b0\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u7c89\u672b\uff0c\u53ef\u6eb6\u4e8e\u7a00\u9178\u53ca\u78b1\u6027\u6eb6\u6db2\uff0c\u5fae\u6eb6\u4e8e\u6c34\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u795e\u7ecf\u9012\u8d28\u591a\u5df4\u80fa\u7684\u524d\u4f53\u5206\u5b50\uff0c\u8be5\u6c18\u4ee3\u5316\u5408\u7269\u4fdd\u7559\u4e86L-\u591a\u5df4\u7684\u7acb\u4f53\u4e13\u4e00\u6027\u751f\u7269\u6d3b\u6027\u3002\u6c18\u539f\u5b50\u53d6\u4ee3\u663e\u8457\u964d\u4f4e\u78b3-\u6c18\u952e\u65ad\u88c2\u901f\u7387\uff0c\u4f7f\u5176\u6210\u4e3a\u7814\u7a76\u591a\u5df4\u4ee3\u8c22\u52a8\u529b\u5b66\u7684\u7406\u60f3\u793a\u8e2a\u5242\u3002\u5728\u5e15\u91d1\u68ee\u75c5\u7814\u7a76\u4e2d\uff0c\u6c18\u6807\u8bb0\u53ef\u5ef6\u957f\u5206\u5b50\u534a\u8870\u671f\uff0c\u7528\u4e8e\u8ffd\u8e2a\u8840\u8111\u5c4f\u969c\u7a7f\u900f\u6548\u7387\u53ca\u591a\u5df4\u8131\u7fa7\u9176\u4ee3\u8c22\u9014\u5f84\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n3.1 \u795e\u7ecf\u836f\u7406\u5b66\u7814\u7a76\uff1a\u7528\u4e8e\u540c\u4f4d\u7d20\u7a00\u91ca\u8d28\u8c31\u6cd5\u7cbe\u786e\u91cf\u5316\u8111\u7ec4\u7ec7\u4e2d\u591a\u5df4\u80fa\u4ee3\u8c22\u901a\u91cf
\n3.2 \u836f\u7269\u5f00\u53d1\uff1a\u4f5c\u4e3a\u6c18\u4ee3\u836f\u7269\u5019\u9009\u5206\u5b50\uff0c\u8bc4\u4f30\u540c\u4f4d\u7d20\u6548\u5e94\u5bf9\u836f\u4ee3\u52a8\u529b\u5b66\u53c2\u6570\u7684\u6539\u5584
\n3.3 \u4e34\u5e8a\u8bca\u65ad\uff1a\u4f5c\u4e3a\u5185\u6807\u7269\u8d28\u5e94\u7528\u4e8e\u8111\u810a\u6db2\u4e2d\u513f\u8336\u915a\u80fa\u7c7b\u7269\u8d28\u7684LC-MS\/MS\u68c0\u6d4b
\n3.4 \u540c\u4f4d\u7d20\u6807\u8bb0\u5b9e\u9a8c\uff1a\u7814\u7a76\u916a\u6c28\u9178\u7f9f\u5316\u9176\u6d3b\u6027\u53ca\u9ed1\u8272\u7d20\u5408\u6210\u9014\u5f84 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u4ea7\u54c1\u9700\u907f\u5149\u4fdd\u5b58\u4e8e-20\u2103\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u5f00\u5c01\u540e\u5efa\u8bae\u5145\u6c2e\u5bc6\u5c01\u3002\u4f7f\u7528\u524d\u9700\u5e73\u8861\u81f3\u5ba4\u6e29\u4ee5\u907f\u514d\u5438\u6e7f\uff0c\u914d\u5236\u6eb6\u6db2\u65f6\u5e94\u4f7f\u7528\u8131\u6c27\u7f13\u51b2\u6db2\uff08\u59820.1M HCl\u542b0.1%\u6297\u574f\u8840\u9178\uff09\u3002\u5de5\u4f5c\u6d53\u5ea6\u901a\u5e38\u4e3a10-100\u03bcM\uff0c\u5177\u4f53\u5b9e\u9a8c\u6761\u4ef6\u9700\u6839\u636e\u7814\u7a76\u4f53\u7cfb\u4f18\u5316\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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