1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\nFmoc-L-\u812f\u6c28\u9178\u4e94\u6c1f\u82ef\u916f\uff08\u5316\u5b66\u540d\u79f0\uff1a1-O-(9H-fluoren-9-ylmethyl) 2-O-(2,3,4,5,6-pentafluorophenyl) (2S)-pyrrolidine-1,2-dicarboxylate\uff09\u662f\u4e00\u79cd\u9ad8\u7eaf\u5ea6\u6709\u673a\u5316\u5408\u7269\uff0cCAS\u53f7\u4e3a86060-90-4\uff0c\u5206\u5b50\u5f0f\u4e3aC26H18F5NO4\uff0c\u5206\u5b50\u91cf\u4e3a503.417\u3002\u8be5\u5316\u5408\u7269\u7531Fmoc\uff089-\u82b4\u7532\u6c27\u7fb0\u57fa\uff09\u4fdd\u62a4\u57fa\u56e2\u4e0eL-\u812f\u6c28\u9178\u4e94\u6c1f\u82ef\u916f\u7ed3\u5408\u800c\u6210\uff0c\u7eaf\u5ea6\u8d85\u8fc796%\uff0c\u5177\u6709\u4f18\u5f02\u7684\u5316\u5b66\u7a33\u5b9a\u6027\u548c\u53cd\u5e94\u6d3b\u6027\u3002\u5176\u7ed3\u6784\u4e2d\u4e94\u6c1f\u82ef\u916f\u57fa\u56e2\u8d4b\u4e88\u5176\u9ad8\u53cd\u5e94\u6027\uff0c\u9002\u7528\u4e8e\u591a\u79cd\u5076\u8054\u53cd\u5e94\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\nFmoc-L-\u812f\u6c28\u9178\u4e94\u6c1f\u82ef\u916f\u5728\u80bd\u5408\u6210\u4e2d\u5177\u6709\u91cd\u8981\u4f5c\u7528\uff0c\u5c24\u5176\u662f\u56fa\u76f8\u80bd\u5408\u6210\uff08SPPS\uff09\u9886\u57df\u3002Fmoc\u57fa\u56e2\u4f5c\u4e3a\u4e34\u65f6\u4fdd\u62a4\u57fa\u56e2\uff0c\u53ef\u5728\u78b1\u6027\u6761\u4ef6\u4e0b\u9009\u62e9\u6027\u8131\u9664\uff0c\u800c\u4e94\u6c1f\u82ef\u916f\u57fa\u56e2\u4f5c\u4e3a\u6d3b\u5316\u916f\uff0c\u80fd\u591f\u9ad8\u6548\u4e0e\u6c28\u57fa\u57fa\u56e2\u53cd\u5e94\u5f62\u6210\u9170\u80fa\u952e\u3002\u8fd9\u79cd\u7279\u6027\u4f7f\u5176\u6210\u4e3a\u6784\u5efa\u590d\u6742\u591a\u80bd\u94fe\u7684\u5173\u952e\u8bd5\u5242\uff0c\u5e7f\u6cdb\u5e94\u7528\u4e8e\u86cb\u767d\u8d28\u5de5\u7a0b\u548c\u836f\u7269\u7814\u53d1\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u8bd5\u5242\u4e3b\u8981\u7528\u4e8e\u591a\u80bd\u5408\u6210\u3001\u86cb\u767d\u8d28\u4fee\u9970\u548c\u751f\u7269\u5171\u8f6d\u5316\u5b66\u3002\u5728\u836f\u7269\u7814\u53d1\u4e2d\uff0c\u5e38\u7528\u4e8e\u5408\u6210\u542b\u6709\u812f\u6c28\u9178\u6b8b\u57fa\u7684\u80bd\u7c7b\u5316\u5408\u7269\uff0c\u5982\u6297\u80bf\u7624\u80bd\u3001\u6297\u83cc\u80bd\u548c\u6fc0\u7d20\u7c7b\u4f3c\u7269\u3002\u6b64\u5916\uff0c\u5176\u9ad8\u53cd\u5e94\u6027\u4e5f\u9002\u7528\u4e8e\u5236\u5907\u8367\u5149\u6807\u8bb0\u63a2\u9488\u548c\u751f\u7269\u4f20\u611f\u5668\uff0c\u4e3a\u5206\u5b50\u751f\u7269\u5b66\u7814\u7a76\u63d0\u4f9b\u91cd\u8981\u5de5\u5177\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\nFmoc-L-\u812f\u6c28\u9178\u4e94\u6c1f\u82ef\u916f\u9700\u5728-20\u00b0C\u4e0b\u907f\u5149\u4fdd\u5b58\uff0c\u5e72\u71e5\u73af\u5883\u4e2d\u5bc6\u5c01\u5b58\u653e\uff0c\u4ee5\u907f\u514d\u5438\u6e7f\u548c\u964d\u89e3\u3002\u4f7f\u7528\u524d\u5e94\u6062\u590d\u81f3\u5ba4\u6e29\u5e76\u786e\u4fdd\u73af\u5883\u5e72\u71e5\u3002\u5efa\u8bae\u5728\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\u6216\u6c29\u6c14\uff09\u4fdd\u62a4\u4e0b\u64cd\u4f5c\uff0c\u4ee5\u5ef6\u957f\u8bd5\u5242\u7a33\u5b9a\u6027\u3002\u6eb6\u89e3\u65f6\u63a8\u8350\u4f7f\u7528\u65e0\u6c34\u4e8c\u7532\u57fa\u7532\u9170\u80fa\uff08DMF\uff09\u6216\u4e8c\u6c2f\u7532\u70f7\uff08DCM\uff09\u7b49\u975e\u8d28\u5b50\u6027\u6eb6\u5242\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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