3-\u6eb4-2,6-\u4e8c\u6c1f\u82ef\u787c\u9178\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n3-\u6eb4-2,6-\u4e8c\u6c1f\u82ef\u787c\u9178\uff08\u82f1\u6587\u540d\uff1a(3-bromo-2,6-difluorophenyl)boronic acid\uff09\u662f\u4e00\u79cd\u6709\u673a\u787c\u9178\u884d\u751f\u7269\uff0c\u5316\u5b66\u5f0f\u4e3aC6H4BBrF2O2\uff0c\u5206\u5b50\u91cf236.807\uff0cCAS\u53f7\u4e3a352535-84-3\u3002\u8be5\u5316\u5408\u7269\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b\uff0c\u7eaf\u5ea6>96%\uff0c\u5177\u6709\u82ef\u73af\u4e0a\u6eb4\u539f\u5b50\u548c\u6c1f\u539f\u5b50\u7684\u53cc\u91cd\u53d6\u4ee3\u7279\u6027\uff0c\u540c\u65f6\u542b\u6709\u787c\u9178\u57fa\u56e2\uff0c\u4f7f\u5176\u5728\u4ea4\u53c9\u5076\u8054\u53cd\u5e94\u4e2d\u8868\u73b0\u51fa\u9ad8\u53cd\u5e94\u6d3b\u6027\u3002\u5176\u7ed3\u6784\u4e2d\u7684\u5364\u7d20\u548c\u787c\u9178\u57fa\u56e2\u4e3a\u540e\u7eed\u5b98\u80fd\u56e2\u5316\u63d0\u4f9b\u4e86\u91cd\u8981\u4f4d\u70b9\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a Suzuki-Miyaura \u5076\u8054\u53cd\u5e94\u7684\u5173\u952e\u4e2d\u95f4\u4f53\uff0c\u8be5\u5316\u5408\u7269\u80fd\u591f\u4e0e\u82b3\u57fa\u5364\u5316\u7269\u6216\u70ef\u70c3\u5364\u5316\u7269\u5728\u94af\u50ac\u5316\u5242\u4f5c\u7528\u4e0b\u5f62\u6210\u78b3-\u78b3\u952e\uff0c\u5e7f\u6cdb\u5e94\u7528\u4e8e\u590d\u6742\u5206\u5b50\u6784\u5efa\u3002\u5176\u5206\u5b50\u4e2d\u7684\u6eb4\u539f\u5b50\u53ef\u8fdb\u4e00\u6b65\u53c2\u4e0e\u4eb2\u6838\u53d6\u4ee3\u53cd\u5e94\uff0c\u800c\u787c\u9178\u57fa\u56e2\u5219\u8d4b\u4e88\u5176\u4e0e\u591a\u79cd electrophiles \u53cd\u5e94\u7684\u80fd\u529b\uff0c\u5728\u836f\u7269\u5316\u5b66\u548c\u6750\u6599\u79d1\u5b66\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u533b\u836f\u4e2d\u95f4\u4f53\u5408\u6210\u3001\u6709\u673a\u5149\u7535\u6750\u6599\u5f00\u53d1\u53ca\u914d\u4f53\u8bbe\u8ba1\u3002\u5728\u6297\u80bf\u7624\u836f\u7269\u548c\u6297\u83cc\u5242\u7814\u53d1\u4e2d\uff0c\u53ef\u4f5c\u4e3a\u6784\u5efa\u542b\u4e8c\u6c1f\u82ef\u57fa\u7ed3\u6784\u5355\u5143\u7684\u780c\u5757\uff1b\u5728OLED\u6750\u6599\u9886\u57df\uff0c\u7528\u4e8e\u5408\u6210\u5177\u6709\u7279\u5b9a\u53d1\u5149\u6027\u80fd\u7684\u5171\u8f6d\u5206\u5b50\u3002\u6b64\u5916\uff0c\u5176\u8fd8\u53ef\u4f5c\u4e3a\u91d1\u5c5e\u6709\u673a\u6846\u67b6\uff08MOF\uff09\u6216\u5171\u4ef7\u6709\u673a\u6846\u67b6\uff08COF\uff09\u7684\u4fee\u9970\u524d\u4f53\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5bc6\u5c01\u4fdd\u5b58\u4e8e-20\u00b0C\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c29\u6c14\uff09\u73af\u5883\u4e2d\uff0c\u907f\u514d\u5149\u7167\u548c\u6e7f\u6c14\u3002\u5f00\u5c01\u540e\u9700\u5728\u5e72\u71e5\u7bb1\u4e2d\u64cd\u4f5c\uff0c\u9632\u6b62\u787c\u9178\u57fa\u56e2\u6c34\u89e3\u3002\u53cd\u5e94\u4f53\u7cfb\u4e2d\u9700\u4e25\u683c\u9664\u6c27\uff0c\u5efa\u8bae\u642d\u914d\u94af\u50ac\u5316\u5242\uff08\u5982Pd(PPh3)4\uff09\u53ca\u78b1\u6027\u6761\u4ef6\uff08\u5982Na2CO3\uff09\u4f7f\u7528\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u8868\u660e\u5176\u5728THF\u3001DMSO\u4e2d\u6eb6\u89e3\u6027\u826f\u597d\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u7ecfHPLC\u68c0\u6d4b\u7eaf\u5ea6>96%\uff0c\u6b8b\u7559\u6eb6\u5242\u7b26\u5408ICH\u6807\u51c6\u3002\u64cd\u4f5c\u65f6\u9700\u4f69\u6234\u9632\u62a4\u624b\u5957\u53ca\u62a4\u76ee\u955c\uff0c\u907f\u514d\u5438\u5165\u7c89\u5c18\u6216\u63a5\u89e6\u76ae\u80a4\u3002MSDS\u6570\u636e\u663e\u793a\u5176\u5177\u6709\u523a\u6fc0\u6027\uff0c\u9047\u660e\u706b\u53ef\u80fd\u91ca\u653e\u6709\u6bd2\u6c14\u4f53\uff08\u5982HBr\u3001HF\uff09\u3002\u5e9f\u5f03\u7269\u5e94\u6309\u7167\u5371\u9669\u5316\u5b66\u54c1\u89c4\u8303\u5904\u7f6e\u3002 <\/p>\n
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