3-\u6eb4-4-\u7f9f\u57fa\u82ef\u7532\u9178\u7532\u916f\u4ea7\u54c1\u8bf4\u660e\u4e66 <\/p>\n
1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n3-\u6eb4-4-\u7f9f\u57fa\u82ef\u7532\u9178\u7532\u916f\uff08Methyl 3-bromo-4-hydroxybenzoate\uff09\u662f\u4e00\u79cd\u6709\u673a\u6eb4\u5316\u7269\uff0c\u5316\u5b66\u5f0f\u4e3aC8H7BrO3\uff0c\u5206\u5b50\u91cf231.043\u3002\u8be5\u5316\u5408\u7269\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u7ed3\u6676\u7c89\u672b\uff0cCAS\u53f7\u4e3a29415-97-2\uff0c\u7eaf\u5ea6\u901a\u5e38\u9ad8\u4e8e96%\u3002\u5176\u7ed3\u6784\u5305\u542b\u82ef\u7532\u9178\u7532\u916f\u9aa8\u67b6\uff0c\u57283\u4f4d\u548c4\u4f4d\u5206\u522b\u88ab\u6eb4\u539f\u5b50\u548c\u7f9f\u57fa\u53d6\u4ee3\uff0c\u8d4b\u4e88\u5176\u72ec\u7279\u7684\u53cd\u5e94\u6d3b\u6027\u3002\u8be5\u7269\u8d28\u6613\u6eb6\u4e8e\u6709\u673a\u6eb6\u5242\u5982\u7532\u9187\u3001\u4e59\u9187\u548c\u4e59\u919a\uff0c\u4f46\u5728\u6c34\u4e2d\u6eb6\u89e3\u5ea6\u8f83\u4f4e\u3002 <\/p>\n
2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n\u4f5c\u4e3a\u82b3\u9999\u65cf\u5316\u5408\u7269\u7684\u884d\u751f\u7269\uff0c3-\u6eb4-4-\u7f9f\u57fa\u82ef\u7532\u9178\u7532\u916f\u5728\u6709\u673a\u5408\u6210\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002\u6eb4\u539f\u5b50\u7684\u5b58\u5728\u4f7f\u5176\u6210\u4e3a Suzuki\u5076\u8054\u3001Buchwald-Hartwig\u80fa\u5316\u7b49\u4ea4\u53c9\u5076\u8054\u53cd\u5e94\u7684\u7406\u60f3\u5e95\u7269\u3002\u7f9f\u57fa\u548c\u916f\u57fa\u7684\u5171\u5b58\u63d0\u4f9b\u4e86\u8fdb\u4e00\u6b65\u7684\u5b98\u80fd\u56e2\u5316\u53ef\u80fd\u6027\uff0c\u4f8b\u5982\u901a\u8fc7\u916f\u6c34\u89e3\u6216\u7f9f\u57fa\u7684\u919a\u5316\u53cd\u5e94\u8fdb\u884c\u7ed3\u6784\u4fee\u9970\u3002\u8fd9\u4e9b\u7279\u6027\u4f7f\u5176\u5728\u836f\u7269\u5316\u5b66\u548c\u6750\u6599\u79d1\u5b66\u4e2d\u5177\u6709\u5e7f\u6cdb\u7684\u5e94\u7528\u6f5c\u529b\u3002 <\/p>\n
3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u5316\u5408\u7269\u4e3b\u8981\u7528\u4e8e\u533b\u836f\u4e2d\u95f4\u4f53\u548c\u7cbe\u7ec6\u5316\u5b66\u54c1\u7684\u5408\u6210\u3002\u5728\u836f\u7269\u7814\u53d1\u4e2d\uff0c\u5b83\u662f\u6784\u5efa\u6297\u83cc\u5242\u3001\u6297\u708e\u836f\u548c\u6297\u764c\u836f\u7269\u7684\u91cd\u8981\u780c\u5757\u3002\u6b64\u5916\uff0c\u5728\u6750\u6599\u79d1\u5b66\u9886\u57df\uff0c\u5b83\u53ef\u4f5c\u4e3a\u6db2\u6676\u6750\u6599\u6216\u9ad8\u5206\u5b50\u5355\u4f53\u7684\u524d\u4f53\u3002\u5b9e\u9a8c\u5ba4\u4e2d\u5e38\u7528\u4e8e\u7814\u7a76\u82b3\u9999\u65cf\u4eb2\u7535\u53d6\u4ee3\u53cd\u5e94\u7684\u673a\u7406\uff0c\u4ee5\u53ca\u4f5c\u4e3a\u6807\u51c6\u54c1\u7528\u4e8e\u5206\u6790\u65b9\u6cd5\u7684\u5f00\u53d1\u4e0e\u9a8c\u8bc1\u3002 <\/p>\n
4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u57282-8\u2103\u7684\u5e72\u71e5\u73af\u5883\u4e2d\u907f\u5149\u4fdd\u5b58\uff0c\u957f\u671f\u50a8\u5b58\u9700\u5145\u5165\u60f0\u6027\u6c14\u4f53\u4fdd\u62a4\u3002\u5f00\u5c01\u540e\u5e94\u5c3d\u5feb\u4f7f\u7528\uff0c\u907f\u514d\u53cd\u590d\u51bb\u878d\u3002\u4f7f\u7528\u65f6\u9700\u5728\u901a\u98ce\u6a71\u4e2d\u64cd\u4f5c\uff0c\u4f69\u6234\u9632\u62a4\u624b\u5957\u548c\u62a4\u76ee\u955c\u3002\u6eb6\u89e3\u6027\u6d4b\u8bd5\u8868\u660e\uff0c\u63a8\u8350\u4f7f\u7528\u4e8c\u7532\u57fa\u4e9a\u781c\uff08DMSO\uff09\u6216\u4e8c\u6c2f\u7532\u70f7\u4f5c\u4e3a\u6eb6\u5242\u4f53\u7cfb\u3002 <\/p>\n
5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
\n\u672c\u4ea7\u54c1\u901a\u8fc7HPLC\u68c0\u6d4b\uff0c\u7eaf\u5ea6\u226596%\uff08\u9762\u79ef\u5f52\u4e00\u5316\u6cd5\uff09\u3002MS\u548cNMR\u8c31\u56fe\u6570\u636e\u53ef\u5e94\u8981\u6c42\u63d0\u4f9b\u3002\u5b89\u5168\u6570\u636e\u8868\u660e\uff0c\u8be5\u5316\u5408\u7269\u53ef\u80fd\u5f15\u8d77\u76ae\u80a4\u548c\u773c\u775b\u523a\u6fc0\uff0c\u64cd\u4f5c\u65f6\u5e94\u907f\u514d\u76f4\u63a5\u63a5\u89e6\u3002\u5e9f\u5f03\u7269\u5904\u7f6e\u9700\u7b26\u5408\u5f53\u5730\u73af\u4fdd\u6cd5\u89c4\uff0c\u4e0d\u53ef\u968f\u610f\u6392\u653e\u3002\u8be6\u7ec6\u6bd2\u7406\u5b66\u6570\u636e\u53c2\u8003SDS\u7b2c11\u8282\uff08\u6025\u6027\u6bd2\u6027\uff1aLD50\u5927\u9f20\u7ecf\u53e3>2000 mg\/kg\uff09\u3002 <\/p>\n
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