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\u4ea7\u54c1\u8bf4\u660e
\n\u4ea7\u54c1\u8bf4\u660e
\n1. \u4ea7\u54c1\u6982\u8ff0\u4e0e\u5316\u5b66\u7279\u6027
\n(S)-tert-Butyl 3-ethylpiperazine-1-carboxylate\uff0c\u4e2d\u6587\u540d\u79f0\u4e3a(S)1-BOC-3-\u4e59\u57fa\u54cc\u55ea\uff0cCAS\u53f7\u4e3a928025-56-3\uff0c\u662f\u4e00\u79cd\u624b\u6027\u54cc\u55ea\u884d\u751f\u7269\u3002\u5176\u5206\u5b50\u5f0f\u4e3aC11H22N2O2\uff0c\u5206\u5b50\u91cf\u4e3a214.305\uff0c\u7eaf\u5ea6\u9ad8\u4e8e96%\u3002\u8be5\u5316\u5408\u7269\u4e3a\u767d\u8272\u81f3\u7c7b\u767d\u8272\u56fa\u4f53\uff0c\u5177\u6709BOC\u4fdd\u62a4\u57fa\u56e2\uff0c\u53ef\u589e\u5f3a\u5176\u5728\u5316\u5b66\u53cd\u5e94\u4e2d\u7684\u7a33\u5b9a\u6027\u3002\u5176\u624b\u6027\u4e2d\u5fc3\u4f4d\u4e8e\u54cc\u55ea\u73af\u76843\u4f4d\uff0c\u4f7f\u5176\u5728\u4e0d\u5bf9\u79f0\u5408\u6210\u4e2d\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002
\n2. \u751f\u7269\u5316\u5b66\u529f\u80fd\u4e0e\u91cd\u8981\u6027
\n(S)1-BOC-3-\u4e59\u57fa\u54cc\u55ea\u662f\u533b\u836f\u4e2d\u95f4\u4f53\u548c\u6709\u673a\u5408\u6210\u4e2d\u7684\u91cd\u8981\u780c\u5757\u3002\u5176\u54cc\u55ea\u7ed3\u6784\u5e7f\u6cdb\u5b58\u5728\u4e8e\u751f\u7269\u6d3b\u6027\u5206\u5b50\u4e2d\uff0c\u5982\u836f\u7269\u5206\u5b50\u4e2d\u7684\u914d\u4f53\u6216\u836f\u6548\u56e2\u3002BOC\u4fdd\u62a4\u57fa\u56e2\u53ef\u5728\u9178\u6027\u6761\u4ef6\u4e0b\u8131\u9664\uff0c\u4fbf\u4e8e\u540e\u7eed\u5b98\u80fd\u56e2\u4fee\u9970\u3002\u8be5\u5316\u5408\u7269\u7684\u624b\u6027\u7279\u6027\u4f7f\u5176\u5728\u4e0d\u5bf9\u79f0\u50ac\u5316\u3001\u624b\u6027\u836f\u7269\u5408\u6210\u7b49\u9886\u57df\u5177\u6709\u72ec\u7279\u4f18\u52bf\uff0c\u5c24\u5176\u5728\u795e\u7ecf\u7c7b\u836f\u7269\u548c\u6297\u611f\u67d3\u836f\u7269\u7684\u7814\u53d1\u4e2d\u5e94\u7528\u5e7f\u6cdb\u3002
\n3. \u4e3b\u8981\u5e94\u7528\u9886\u57df\u4e0e\u5177\u4f53\u7528\u9014
\n\u8be5\u4ea7\u54c1\u4e3b\u8981\u7528\u4e8e\u4ee5\u4e0b\u9886\u57df\uff1a
\n– \u533b\u836f\u4e2d\u95f4\u4f53\uff1a\u4f5c\u4e3a\u624b\u6027\u54cc\u55ea\u9aa8\u67b6\uff0c\u7528\u4e8e\u5408\u6210\u6297\u6291\u90c1\u3001\u6297\u7cbe\u795e\u75c5\u53ca\u6297\u611f\u67d3\u836f\u7269\u3002
\n– \u4e0d\u5bf9\u79f0\u5408\u6210\uff1a\u4f5c\u4e3a\u624b\u6027\u52a9\u5242\u6216\u914d\u4f53\uff0c\u53c2\u4e0e\u50ac\u5316\u4e0d\u5bf9\u79f0\u53cd\u5e94\u3002
\n– \u6709\u673a\u5408\u6210\uff1a\u7528\u4e8e\u6784\u5efa\u590d\u6742\u6742\u73af\u5316\u5408\u7269\u6216\u529f\u80fd\u5316\u54cc\u55ea\u884d\u751f\u7269\u3002
\n4. \u50a8\u5b58\u6761\u4ef6\u4e0e\u4f7f\u7528\u5efa\u8bae
\n\u5efa\u8bae\u5c06\u4ea7\u54c1\u5bc6\u5c01\u4fdd\u5b58\u4e8e2-8\u2103\u7684\u5e72\u71e5\u73af\u5883\u4e2d\uff0c\u907f\u514d\u5149\u7167\u548c\u6f6e\u6e7f\u3002\u5f00\u5c01\u540e\u9700\u5145\u5165\u60f0\u6027\u6c14\u4f53\uff08\u5982\u6c2e\u6c14\uff09\u4ee5\u5ef6\u957f\u7a33\u5b9a\u6027\u3002\u4f7f\u7528\u65f6\u9700\u5728\u5e72\u71e5\u73af\u5883\u4e0b\u64cd\u4f5c\uff0c\u907f\u514d\u4e0e\u5f3a\u9178\u3001\u5f3a\u6c27\u5316\u5242\u63a5\u89e6\u3002BOC\u4fdd\u62a4\u57fa\u7684\u8131\u9664\u9700\u5728\u9178\u6027\u6761\u4ef6\u4e0b\u8fdb\u884c\uff08\u5982\u4e09\u6c1f\u4e59\u9178\u6216\u76d0\u9178\uff09\u3002
\n5. \u8d28\u91cf\u63a7\u5236\u4e0e\u5b89\u5168\u4fe1\u606f
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